可以考慮將六水三氯化鐵晶體在氯化氫氣體中脫水，麻煩著呢。如果是就用一點的話，最好采用純氯在低濃度和惰性氣體充斥的條件下氧化還原鐵粉（反應(yīng)劇烈）

學(xué)習(xí)了。好牛，什么都有人知道��！

it is very simple. It was refluxed in SOCl2 overnight, and then solvent was removed and dried under vacuum. You'd better use a vacuum line. (you can find the exact procedure in Inorganic Synthesis, sorry, I can't remember which volume.) I hope it will be helpful for you.

謝謝了，在氯氣中和Fe粉反應(yīng)比較麻煩吧，也不好控制把，謝謝，現(xiàn)在我這里有很多六水的三氯化鐵，希望還有更簡單一點的辦法，再次辛苦大家了！

二樓的能說得詳細點嗎？能把文獻傳過來嗎？謝謝！

好的，我試一下哦！謝謝！