求教各位大神圖中反應(yīng)的催化劑
這是一片國外專利的反應(yīng),文獻中只說了需要催化劑,但是沒有說明催化劑是什么?求教各位大神,途中反應(yīng)的催化劑應(yīng)該是什么,原文這樣說的:The synthesis is based on catalytic dehydration of glycerine. The glycerine, placed in a retort connected with refrigerator, is heated over inoculum catalyst to the temperature of 220-250 degrees С (Fig 1). After 20-25 minutes, the distillation of water vapor begins. The quantity of the catalyst is 0.02-0.05%. Such a minimum quantity of the catalyst is reasoned by the fact that with the production of first synthesis products, the process transits to the auto-catalytic mode. In such a way, the initial catalyst is only an inoculum for the start of the dehydration process in the auto-catalytic mode. For example, for the process of dehydration of 200 ml (252 g) of glycerine, only 50-100 mg of catalyst is needed.
返回小木蟲查看更多
京公網(wǎng)安備 11010802022153號