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buct_xjq捐助貴賓 (著名寫手)
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[交流]
白色的Fe-mcm-41,能否證明鐵在骨架上
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制備了鐵含量較高的Fe-mcm-41,烘干后樣品為白色,個(gè)人以為這在很大程度上已經(jīng)證明了鐵在分子篩的骨架上,不知道大家是否有這方面的經(jīng)驗(yàn)以供參考,僅就樣品的顏色來判斷金屬的配位情況。 [ Last edited by buct_xjq on 2009-5-29 at 20:25 ] |


捐助貴賓 (著名寫手)

木蟲 (正式寫手)
捐助貴賓 (著名寫手)
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The color of an iron-containing sample may be used as a qualitative indication of the probable components present in the sample.4’ The four as-synthesized samples with varying Si02/Fe203 (A 1,B 1, Cl, Dl) are white, indicating the absence of antiferromagnetic interactions due to Fe-O-Fe bonds arising from an iron-oxide phase. 來源 A. Meagher*, V. Nair and R. Szostak A Mössbauer study of ZSM-5-type ferrisilicates Zeolites,Volume 8, Issue 1, January 1988, Pages 3-11 以前在小木蟲上求助的這篇文獻(xiàn),有興趣的朋友可以下來看看 http://www.gaoyang168.com/bbs/viewthread.php?tid=1320297 [ Last edited by buct_xjq on 2009-5-29 at 20:38 ] |

金蟲 (正式寫手)

木蟲 (正式寫手)
鐵桿木蟲 (著名寫手)
捐助貴賓 (著名寫手)
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做過鐵的含量了,XRF表征表明在10wt%左右,含量還是做的很不錯,最近也查到一篇做Fe-MCM-41的文獻(xiàn)說如果樣品在焙燒前事白色就可以證明樣品種不存在氧化鐵, Journal of Catalysis 209, 186–196 (2002),Characterizations of Iron-Containing MCM-41 and Its Catalytic Properties in Epoxidation of Styrene with Hydrogen Peroxide YeWang,∗,1 Qinghong Zhang,† Tetsuya Shishido,† and Katsuomi Takehira,有這方面經(jīng)驗(yàn)的高手希望能交流一下,鐵的含量提高以后規(guī)整度明顯降低,但有些XRD表征并沒有出峰的樣品在焙燒之前依然是白色的,這點(diǎn)讓我不思其解。 |

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