| 5 | 1/1 | 返回列表 |
| 查看: 1070 | 回復: 4 | |||
[求助]
Au、Ag納米粒子制備時如何避光? 已有1人參與
|
|
以兩篇文章為例 甲:Ag-modified zeolite (Ag/HZSM-5) was prepared by ion-exchange of 2.5 g of H-ZSM-5 with 25 mL of 0.15 M AgNO3 aqueous solution overnight at 25°C in the dark with subsequent filtration,19 washing with distilled water, drying at 393 K for 14 h, and further calcination at 673 K for 4 h in a flow of air calcination at 673 K for 4 h 乙:All the preparations were performed in the absence of light, which is known to decompose the gold precursors ( deposition–precipitation ) 1.兩篇文章皆提及,沉積沉淀法制備Au NP,離子交換法制備Ag粒子,需避光制備。文中所言避光指的是什么光?太陽光?燈光?具體避光實驗操作應該如何進行呢? ![]() 2. Ag粒子也可由AgNO3熱分解而來?無需H2還原? 【unexchanged silver exists as metallic species formed by thermal decomposition of AgNO3 during calcination】?Au可從Au2O3任何氣氛下高溫分解而來【干燥樣品(As prepared),金以+3價氧化態(tài)存在。Au2O3不穩(wěn)定,任何氣體下加熱都可還原得到Au0,但是不一定保證所有Au物種都變成Au0,部分陽離子物種也可能存在。通常在373K條件下,Au前提開始分解并還原為Au0】。 |
榮譽版主 (文壇精英)
山濤
![]() |
專家經(jīng)驗: +925 |

榮譽版主 (文壇精英)
山濤
![]() |
專家經(jīng)驗: +925 |

| 5 | 1/1 | 返回列表 |
| 最具人氣熱帖推薦 [查看全部] | 作者 | 回/看 | 最后發(fā)表 | |
|---|---|---|---|---|
|
[考研] 【考研調(diào)劑】化學專業(yè) 281分,一志愿四川大學,誠心求調(diào)劑 +15 | 吃吃吃才有意義 2026-03-19 | 16/800 |
|
|---|---|---|---|---|
|
[考研] 0854人工智能方向招收調(diào)劑 +3 | 章小魚567 2026-03-24 | 3/150 |
|
|
[考研] 調(diào)劑 +4 | 13853210211 2026-03-24 | 4/200 |
|
|
[考研] 材料學碩333求調(diào)劑 +3 | 北道巷 2026-03-24 | 3/150 |
|
|
[考研] 292求調(diào)劑 +4 | 鵝鵝鵝額額額額?/a> 2026-03-24 | 4/200 |
|
|
[考研] 材料專碩331求調(diào)劑 +4 | 鮮當牛 2026-03-24 | 4/200 |
|
|
[考研] 一志愿武理材料工程348求調(diào)劑 +6 |  ̄^ ̄゜汗 2026-03-19 | 9/450 |
|
|
[考研] 333求調(diào)劑 +3 | ALULU4408 2026-03-23 | 3/150 |
|
|
[考研] 工科0856求調(diào)劑 +5 | 沐析汀汀 2026-03-21 | 5/250 |
|
|
[考研] 323求調(diào)劑 +6 | 洼小桶 2026-03-18 | 6/300 |
|
|
[考研] 317求調(diào)劑 +12 | 申子申申 2026-03-19 | 18/900 |
|
|
[考研] 材料與化工085600,總分304,本科有兩篇sci參與,求調(diào)劑 +4 | 幸運的醬醬 2026-03-22 | 5/250 |
|
|
[考研] 319求調(diào)劑 +4 | 小力氣珂珂 2026-03-20 | 4/200 |
|
|
[考研] 303求調(diào)劑 +5 | 安憶靈 2026-03-22 | 6/300 |
|
|
[考研] 考研調(diào)劑 +3 | 呼呼?~+123456 2026-03-21 | 3/150 |
|
|
[考研]
|
Grand777 2026-03-21 | 3/150 |
|
|
[考研] 一志愿重慶大學085700資源與環(huán)境總分308求調(diào)劑 +7 | 墨墨漠 2026-03-20 | 7/350 |
|
|
[考研] 求調(diào)劑 +3 | .m.. 2026-03-21 | 4/200 |
|
|
[考研] 一志愿 西北大學 ,070300化學學碩,總分287,雙非一本,求調(diào)劑。 +3 | 晨昏線與星海 2026-03-18 | 3/150 |
|
|
[考研] 一志愿西南交通 專碩 材料355 本科雙非 求調(diào)劑 +5 | 西南交通專材355 2026-03-19 | 5/250 |
|