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帥得無(wú)法呼吸新蟲 (小有名氣)
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[求助]
有一晶體 懇求各路英雄好漢前來(lái)支援 謝謝 已有1人參與
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| 配體等數(shù)據(jù)在壓縮包內(nèi) |
新蟲 (小有名氣)
金蟲 (正式寫手)
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相關(guān)數(shù)據(jù)在壓縮包里 Identification code 20160314_3_0m Empirical formula CHONCoCl Formula weight 137.41 Temperature/K 223.0 Crystal system triclinic Space group P-1 a/Å 7.2857(6) b/Å 13.9446(11) c/Å 19.7447(16) α/° 101.429(2) β/° 99.928(2) γ/° 94.933(2) Volume/Å3 1921.7(3) Z 1 ρcalcg/cm3 0.119 μ/mm‑1 0.247 F(000) 66.0 Crystal size/mm3 ? × ? × ? Radiation MoKα (λ = 0.71076) 2Θ range for data collection/° 5.748 to 63.646 Index ranges -10 ≤ h ≤ 10, -20 ≤ k ≤ 20, -28 ≤ l ≤ 29 Reflections collected 71559 Independent reflections 11738 [Rint = 0.0268, Rsigma = 0.0182] Data/restraints/parameters 11738/0/453 Goodness-of-fit on F2 1.069 Final R indexes [I>=2σ (I)] R1 = 0.0521, wR2 = 0.1247 Final R indexes [all data] R1 = 0.0611, wR2 = 0.1321 Largest diff. peak/hole / e Å-3 1.19/-1.19 |
金蟲 (正式寫手)
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已修改好 見附件 Table 1 Crystal data and structure refinement for 20160314_3_0m. Identification code 20160314_3_0m Empirical formula C39H46Cl6CoN2O2 Formula weight 846.41 Temperature/K 223.0 Crystal system triclinic Space group P-1 a/Å 7.2857(6) b/Å 13.9446(11) c/Å 19.7447(16) α/° 101.429(2) β/° 99.928(2) γ/° 94.933(2) Volume/Å3 1921.7(3) Z 1 ρcalcg/cm3 0.731 μ/mm‑1 0.451 F(000) 439.0 Crystal size/mm3 ? × ? × ? Radiation MoKα (λ = 0.71076) 2Θ range for data collection/° 5.748 to 63.646 Index ranges -10 ≤ h ≤ 10, -20 ≤ k ≤ 20, -28 ≤ l ≤ 29 Reflections collected 71559 Independent reflections 11738 [Rint = 0.0268, Rsigma = 0.0182] Data/restraints/parameters 11738/0/453 Goodness-of-fit on F2 1.071 Final R indexes [I>=2σ (I)] R1 = 0.0518, wR2 = 0.1219 Final R indexes [all data] R1 = 0.0607, wR2 = 0.1291 Largest diff. peak/hole / e Å-3 1.19/-1.19 |
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