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xianyun414木蟲 (小有名氣)
司令
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[求助]
銅納米線 夏幼南法 已有3人參與
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夏幼南發(fā)表在Angew. Chem. Int. Ed. 2011, 50, 10560 –10564的文章,制備銅納米線是在22.2ml Vial,這在100攝氏度加熱下會(huì)不會(huì)把瓶蓋給沖出來,或者爆了,可以在三口燒瓶里進(jìn)行反應(yīng)嗎,還是說反應(yīng)本身須在一定的壓力下進(jìn)行呢。以下為反應(yīng)條件,謝謝 All the chemicals were obtained from Sigma-Aldrich and used as received. In a standard synthesis of Cu nanowires, 21 mg CuCl2·2H2O, 180 mg HDA, and 50 mg glucose (α or form) were dissolved in 10 mL water in a 22.2-mL vial (borosilicate glass vial, with a black phenolic molded screw cap and polyvinyl-faced pulp liner, VWR International, Radnor, PA) at room temperature. After the vial had been capped, the solution was magnetically stirred at room temperature overnight. The capped vial was then transferred into an oil bath and heated at 100 oC for 6 h under magnetic stirring. |
納米銅 | 納米材料專題 | 金屬納米線 |

木蟲 (正式寫手)

新蟲 (正式寫手)
金蟲 (小有名氣)

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