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| 本帖產(chǎn)生 1 個 翻譯EPI ，點(diǎn)擊這里進(jìn)行查看 | |||
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caixian木蟲 (正式寫手)
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[求助]
摘要
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| 本文通過一步反應(yīng)合成了配合物二氯(五甲基環(huán)戊二烯基)合釕(III)聚合物 [C_5 Me_5 RuCl_2 ]_n，并對制備方法進(jìn)行了改進(jìn)和優(yōu)化，使產(chǎn)率達(dá)到80%，高于文獻(xiàn)報道值。采用元素分析、紅外光譜（IR）、核磁共振（1H-NMR）等結(jié)構(gòu)分析方法對配合物的結(jié)構(gòu)進(jìn)行了表征，確定了它們的化學(xué)結(jié)構(gòu)。 |
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本帖內(nèi)容被屏蔽 |
3樓2016-06-25 17:26:03
【答案】應(yīng)助回帖
★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★
caixian: 金幣+20, 翻譯EPI+1 2016-06-27 15:40:46
caixian: 金幣+20, 翻譯EPI+1 2016-06-27 15:40:46
| In this paper, [C_5 Me_5 RuCl_2 ]_n has been synthesized through one-step reaction. Preparation method has been improved and optimized,thus the productivity was up to 80%, which was higher than reproted values of literature. Structure of the complexes have been represented by the structural analytical methods like elemental analysis, IR, 1H-NMR,then their chemical construction was confirmed finally. |
2樓2016-06-25 17:02:03
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