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virture木蟲 (小有名氣)
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[求助]
求助PCN-222的cif文件 已有1人參與
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| 求助PCN-222的cif文件,急用,謝謝 |
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data_e:\xray\2-14-4\nodoub~1\2 _audit_creation_method SHELXL-97 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C48 H24 Cl Fe N4 O16 Zr3' _chemical_formula_weight 1277.67 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Fe' 'Fe' 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Zr' 'Zr' -2.9673 0.5597 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting ? _symmetry_space_group_name_H-M ? loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x-y, x, z' '-y, x-y, z' '-x, -y, z' '-x+y, -x, z' 'y, -x+y, z' 'x-y, -y, -z' '-x, -x+y, -z' 'y, x, -z' '-y, -x, -z' '-x+y, y, -z' 'x, x-y, -z' '-x, -y, -z' '-x+y, -x, -z' 'y, -x+y, -z' 'x, y, -z' 'x-y, x, -z' '-y, x-y, -z' '-x+y, y, z' 'x, x-y, z' '-y, -x, z' 'y, x, z' 'x-y, -y, z' '-x, -x+y, z' _cell_length_a 41.968(7) _cell_length_b 41.968(7) _cell_length_c 17.143(2) _cell_angle_alpha 90.00 _cell_angle_beta 90.00 _cell_angle_gamma 120.00 _cell_volume 26149(7) _cell_formula_units_Z 6 _cell_measurement_temperature 173(2) _cell_measurement_reflns_used ? _cell_measurement_theta_min ? _cell_measurement_theta_max ? _exptl_crystal_description ? _exptl_crystal_colour ? _exptl_crystal_size_max ? _exptl_crystal_size_mid ? _exptl_crystal_size_min ? _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 0.487 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 3786 _exptl_absorpt_coefficient_mu 0.292 _exptl_absorpt_correction_type ? _exptl_absorpt_correction_T_min ? _exptl_absorpt_correction_T_max ? _exptl_absorpt_process_details ? _exptl_special_details ; ? ; _diffrn_ambient_temperature 173(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type ? _diffrn_measurement_method ? _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 125544 _diffrn_reflns_av_R_equivalents 0.1398 _diffrn_reflns_av_sigmaI/netI 0.0488 _diffrn_reflns_limit_h_min -44 _diffrn_reflns_limit_h_max 44 _diffrn_reflns_limit_k_min -44 _diffrn_reflns_limit_k_max 44 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_theta_min 1.31 _diffrn_reflns_theta_max 22.05 _reflns_number_total 6038 _reflns_number_gt 4741 _reflns_threshold_expression >2sigma(I) _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution 'SHELXS-97 (Sheldrick, 2008)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 2008)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details ; calc [1.00000+0.00000exp(0.00(sin\q/\l)^2^)]/ [\s^2^(Fo^2^)+0.0000+0.0000*P+(0.1008P)^2^+0.0000sin\q/\l] where P = 0.00000Fo^2^ + 1.00000Fc^2^ ; _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_number_reflns 6038 _refine_ls_number_parameters 181 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0821 _refine_ls_R_factor_gt 0.0551 _refine_ls_wR_factor_ref 0.1582 _refine_ls_wR_factor_gt 0.1438 _refine_ls_goodness_of_fit_ref 1.045 _refine_ls_restrained_S_all 1.045 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Zr1 Zr 0.457975(13) 0.0000 0.10266(3) 0.0331(2) Uani 1 2 d S . . Zr2 Zr 0.533821(9) 0.067643(18) 0.0000 0.0274(2) Uani 1 4 d S . . Fe1 Fe 0.51200(7) 0.25600(3) 0.5000 0.1073(8) Uani 1 4 d S . . O3 O 0.51645(6) 0.03289(11) 0.1031(3) 0.0678(14) Uani 1 2 d S . . O4 O 0.47404(12) 0.03385(11) 0.0000 0.0602(13) Uani 1 2 d S . . O2 O 0.51760(8) 0.09873(7) 0.07892(15) 0.0443(7) Uani 1 1 d . . . O1 O 0.46905(9) 0.05532(8) 0.14348(18) 0.0640(9) Uani 1 1 d . . . N1 N 0.50405(19) 0.25202(9) 0.3824(3) 0.073(2) Uani 1 2 d S . . N2 N 0.50293(19) 0.20432(14) 0.5000 0.076(2) Uani 1 2 d S . . C8 C 0.50226(17) 0.19348(13) 0.3581(2) 0.0770(17) Uani 1 1 d . . . C11 C 0.50287(17) 0.18392(13) 0.4354(2) 0.0750(17) Uani 1 1 d . . . C3 C 0.52665(14) 0.15019(12) 0.1919(2) 0.0604(13) Uani 1 1 d . . . H3 H 0.5468 0.1564 0.1577 0.072 Uiso 1 1 calc R . . C10 C 0.49969(17) 0.23415(13) 0.2536(2) 0.087(2) Uani 1 1 d . . . H10 H 0.4981 0.2201 0.2089 0.104 Uiso 1 1 calc R . . C2 C 0.49592(14) 0.11662(12) 0.1876(2) 0.0553(12) Uani 1 1 d . . . C1 C 0.49360(14) 0.08768(12) 0.1314(3) 0.0499(12) Uani 1 1 d . . . C7 C 0.46701(16) 0.10779(14) 0.2381(3) 0.0788(17) Uani 1 1 d . . . H7 H 0.4455 0.0842 0.2363 0.095 Uiso 1 1 calc R . . C9 C 0.50258(18) 0.22487(13) 0.3334(2) 0.0771(18) Uani 1 1 d . . . C6 C 0.46991(18) 0.13396(16) 0.2913(3) 0.0841(18) Uani 1 1 d . . . H6 H 0.4496 0.1283 0.3245 0.101 Uiso 1 1 calc R . . C5 C 0.50048(17) 0.16701(13) 0.2975(3) 0.0641(14) Uani 1 1 d . . . C4 C 0.52848(16) 0.17569(13) 0.2472(3) 0.0683(15) Uani 1 1 d . . . H4 H 0.5497 0.1995 0.2494 0.082 Uiso 1 1 calc R . . C12 C 0.5030(2) 0.15141(14) 0.4607(3) 0.110(3) Uani 1 1 d . . . H12 H 0.5031 0.1332 0.4280 0.131 Uiso 1 1 calc R . . O6 O 0.40541(11) 0.0000 0.0918(3) 0.0688(13) Uani 1 2 d S . . O5 O 0.46148(12) 0.0000 0.2309(3) 0.0701(14) Uani 1 2 d S . . Cl1 Cl 0.57704(14) 0.28852(7) 0.5000 0.1544(16) Uani 1 4 d S . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Zr1 0.0475(3) 0.0233(3) 0.0204(3) 0.000 0.0080(2) 0.01165(16) Zr2 0.0434(4) 0.0178(4) 0.0126(4) 0.000 0.000 0.00889(19) Fe1 0.277(3) 0.0878(8) 0.0203(7) 0.000 0.000 0.1384(13) O3 0.078(3) 0.044(3) 0.070(3) 0.046(2) 0.0231(12) 0.0218(13) O4 0.081(3) 0.047(2) 0.0074(19) 0.000 0.000 -0.002(2) O2 0.074(2) 0.0288(15) 0.0251(15) 0.0021(12) 0.0058(15) 0.0222(15) O1 0.091(2) 0.042(2) 0.052(2) -0.0034(16) 0.0283(18) 0.0280(18) N1 0.172(6) 0.061(2) 0.023(3) -0.0007(16) -0.001(3) 0.086(3) N2 0.187(7) 0.058(4) 0.024(3) 0.000 0.000 0.091(4) C8 0.175(6) 0.058(3) 0.025(3) 0.003(2) 0.001(3) 0.079(4) C11 0.169(6) 0.055(3) 0.034(3) -0.005(2) -0.001(3) 0.080(4) C3 0.103(4) 0.040(3) 0.038(3) -0.009(2) 0.009(3) 0.036(3) C10 0.202(6) 0.074(3) 0.020(2) -0.001(2) 0.000(3) 0.096(4) C2 0.092(4) 0.040(3) 0.035(3) -0.004(2) 0.009(3) 0.034(3) C1 0.085(3) 0.031(3) 0.040(3) 0.000(2) 0.013(3) 0.034(3) C7 0.106(4) 0.058(3) 0.060(3) -0.010(3) 0.029(3) 0.032(3) C9 0.175(6) 0.071(3) 0.024(2) -0.003(2) -0.002(3) 0.091(4) C6 0.139(5) 0.081(4) 0.048(3) 0.000(3) 0.038(3) 0.066(4) C5 0.127(5) 0.040(3) 0.034(3) 0.000(2) 0.007(3) 0.048(3) C4 0.118(5) 0.042(3) 0.045(3) -0.006(2) 0.003(3) 0.040(3) C12 0.273(8) 0.079(4) 0.035(2) 0.003(3) 0.010(4) 0.132(5) O6 0.063(2) 0.062(3) 0.081(3) 0.000 0.016(2) 0.0311(15) O5 0.092(3) 0.060(3) 0.047(3) 0.000 0.015(2) 0.0299(15) Cl1 0.197(5) 0.157(3) 0.123(3) 0.000 0.000 0.098(2) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Zr1 O3 2.131(2) 4_655 ? Zr1 O3 2.131(2) . ? Zr1 O4 2.147(2) . ? Zr1 O4 2.148(2) 7 ? Zr1 O5 2.204(5) . ? Zr1 O6 2.214(5) . ? Zr1 O1 2.240(3) . ? Zr1 O1 2.240(3) 23 ? Zr1 Zr2 3.5003(7) . ? Zr1 Zr2 3.5003(7) 13_655 ? Zr1 Zr1 3.5197(11) 16 ? Zr1 Zr1 3.5275(13) 4_655 ? Zr2 O3 2.172(4) . ? Zr2 O3 2.172(4) 16 ? Zr2 O4 2.179(4) 19_655 ? Zr2 O4 2.179(4) . ? Zr2 O2 2.210(3) . ? Zr2 O2 2.210(3) 19_655 ? Zr2 O2 2.210(3) 11_655 ? Zr2 O2 2.210(3) 16 ? Zr2 Zr1 3.5003(7) 13_655 ? Zr2 Zr1 3.5003(7) 4_655 ? Zr2 Zr1 3.5003(7) 16 ? Fe1 N2 2.006(5) . ? Fe1 N2 2.006(5) 20 ? Fe1 N1 2.037(5) 16_556 ? Fe1 N1 2.037(5) . ? Fe1 Cl1 2.364(6) . ? O3 Zr1 2.131(2) 4_655 ? O4 Zr1 2.147(2) 16 ? O2 C1 1.254(5) . ? O1 C1 1.245(5) . ? N1 C9 1.392(5) . ? N1 C9 1.392(5) 20 ? N2 C11 1.399(5) 16_556 ? N2 C11 1.400(5) . ? C8 C9 1.377(6) . ? C8 C11 1.387(6) . ? C8 C5 1.496(6) . ? C11 C12 1.435(6) . ? C3 C2 1.355(6) . ? C3 C4 1.403(6) . ? C10 C10 1.317(9) 20 ? C10 C9 1.444(6) . ? C2 C7 1.382(6) . ? C2 C1 1.515(6) . ? C7 C6 1.386(6) . ? C6 C5 1.342(7) . ? C5 C4 1.352(7) . ? C12 C12 1.347(9) 16_556 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O3 Zr1 O3 68.26(18) 4_655 . ? O3 Zr1 O4 109.77(18) 4_655 . ? O3 Zr1 O4 72.27(15) . . ? O3 Zr1 O4 72.27(15) 4_655 7 ? O3 Zr1 O4 109.77(18) . 7 ? O4 Zr1 O4 69.90(17) . 7 ? O3 Zr1 O5 86.63(16) 4_655 . ? O3 Zr1 O5 86.63(16) . . ? O4 Zr1 O5 144.96(9) . . ? O4 Zr1 O5 144.96(9) 7 . ? O3 Zr1 O6 145.60(9) 4_655 . ? O3 Zr1 O6 145.60(9) . . ? O4 Zr1 O6 85.10(16) . . ? O4 Zr1 O6 85.11(16) 7 . ? O5 Zr1 O6 98.63(18) . . ? O3 Zr1 O1 139.44(13) 4_655 . ? O3 Zr1 O1 75.67(13) . . ? O4 Zr1 O1 74.73(12) . . ? O4 Zr1 O1 139.91(13) 7 . ? O5 Zr1 O1 73.08(9) . . ? O6 Zr1 O1 73.53(10) . . ? O3 Zr1 O1 75.67(13) 4_655 23 ? O3 Zr1 O1 139.44(13) . 23 ? O4 Zr1 O1 139.91(13) . 23 ? O4 Zr1 O1 74.73(12) 7 23 ? O5 Zr1 O1 73.08(9) . 23 ? O6 Zr1 O1 73.53(10) . 23 ? O1 Zr1 O1 127.71(15) . 23 ? O3 Zr1 Zr2 88.78(11) 4_655 . ? O3 Zr1 Zr2 35.96(10) . . ? O4 Zr1 Zr2 36.30(11) . . ? O4 Zr1 Zr2 89.93(11) 7 . ? O5 Zr1 Zr2 117.91(8) . . ? O6 Zr1 Zr2 117.39(7) . . ? O1 Zr1 Zr2 71.53(8) . . ? O1 Zr1 Zr2 160.76(8) 23 . ? O3 Zr1 Zr2 35.97(10) 4_655 13_655 ? O3 Zr1 Zr2 88.78(11) . 13_655 ? O4 Zr1 Zr2 89.93(11) . 13_655 ? O4 Zr1 Zr2 36.30(11) 7 13_655 ? O5 Zr1 Zr2 117.91(8) . 13_655 ? O6 Zr1 Zr2 117.39(7) . 13_655 ? O1 Zr1 Zr2 160.76(8) . 13_655 ? O1 Zr1 Zr2 71.53(8) 23 13_655 ? Zr2 Zr1 Zr2 89.24(2) . 13_655 ? O3 Zr1 Zr1 90.21(12) 4_655 16 ? O3 Zr1 Zr1 90.21(12) . 16 ? O4 Zr1 Zr1 34.97(9) . 16 ? O4 Zr1 Zr1 34.97(9) 7 16 ? O5 Zr1 Zr1 176.18(13) . 16 ? O6 Zr1 Zr1 85.19(12) . 16 ? O1 Zr1 Zr1 108.21(8) . 16 ? O1 Zr1 Zr1 108.21(8) 23 16 ? Zr2 Zr1 Zr1 59.817(10) . 16 ? Zr2 Zr1 Zr1 59.818(10) 13_655 16 ? O3 Zr1 Zr1 34.13(9) 4_655 4_655 ? O3 Zr1 Zr1 34.13(9) . 4_655 ? O4 Zr1 Zr1 90.96(13) . 4_655 ? O4 Zr1 Zr1 90.96(13) 7 4_655 ? O5 Zr1 Zr1 86.18(13) . 4_655 ? O6 Zr1 Zr1 175.20(12) . 4_655 ? O1 Zr1 Zr1 108.10(9) . 4_655 ? O1 Zr1 Zr1 108.11(9) 23 4_655 ? Zr2 Zr1 Zr1 59.743(10) . 4_655 ? Zr2 Zr1 Zr1 59.744(10) 13_655 4_655 ? Zr1 Zr1 Zr1 90.0 16 4_655 ? O3 Zr2 O3 108.9(3) . 16 ? O3 Zr2 O4 70.87(9) . 19_655 ? O3 Zr2 O4 70.87(9) 16 19_655 ? O3 Zr2 O4 70.87(9) . . ? O3 Zr2 O4 70.87(9) 16 . ? O4 Zr2 O4 111.4(2) 19_655 . ? O3 Zr2 O2 78.42(12) . . ? O3 Zr2 O2 142.68(7) 16 . ? O4 Zr2 O2 141.86(7) 19_655 . ? O4 Zr2 O2 77.87(12) . . ? O3 Zr2 O2 78.42(12) . 19_655 ? O3 Zr2 O2 142.68(7) 16 19_655 ? O4 Zr2 O2 77.88(12) 19_655 19_655 ? O4 Zr2 O2 141.86(7) . 19_655 ? O2 Zr2 O2 74.20(15) . 19_655 ? O3 Zr2 O2 142.68(7) . 11_655 ? O3 Zr2 O2 78.42(12) 16 11_655 ? O4 Zr2 O2 77.88(12) 19_655 11_655 ? O4 Zr2 O2 141.86(7) . 11_655 ? O2 Zr2 O2 118.50(14) . 11_655 ? O2 Zr2 O2 75.49(13) 19_655 11_655 ? O3 Zr2 O2 142.68(7) . 16 ? O3 Zr2 O2 78.42(12) 16 16 ? O4 Zr2 O2 141.86(7) 19_655 16 ? O4 Zr2 O2 77.87(12) . 16 ? O2 Zr2 O2 75.49(13) . 16 ? O2 Zr2 O2 118.50(14) 19_655 16 ? O2 Zr2 O2 74.20(15) 11_655 16 ? O3 Zr2 Zr1 35.17(6) . . ? O3 Zr2 Zr1 90.04(11) 16 . ? O4 Zr2 Zr1 91.16(11) 19_655 . ? O4 Zr2 Zr1 35.70(6) . . ? O2 Zr2 Zr1 75.37(7) . . ? O2 Zr2 Zr1 110.81(7) 19_655 . ? O2 Zr2 Zr1 166.13(7) 11_655 . ? O2 Zr2 Zr1 111.28(7) 16 . ? O3 Zr2 Zr1 90.04(11) . 13_655 ? O3 Zr2 Zr1 35.17(6) 16 13_655 ? O4 Zr2 Zr1 35.69(6) 19_655 13_655 ? O4 Zr2 Zr1 91.16(11) . 13_655 ? O2 Zr2 Zr1 166.12(7) . 13_655 ? O2 Zr2 Zr1 111.28(7) 19_655 13_655 ? O2 Zr2 Zr1 75.37(7) 11_655 13_655 ? O2 Zr2 Zr1 110.81(7) 16 13_655 ? Zr1 Zr2 Zr1 90.77(2) . 13_655 ? O3 Zr2 Zr1 35.17(6) . 4_655 ? O3 Zr2 Zr1 90.04(11) 16 4_655 ? O4 Zr2 Zr1 35.69(6) 19_655 4_655 ? O4 Zr2 Zr1 91.16(11) . 4_655 ? O2 Zr2 Zr1 110.81(7) . 4_655 ? O2 Zr2 Zr1 75.37(7) 19_655 4_655 ? O2 Zr2 Zr1 111.28(7) 11_655 4_655 ? O2 Zr2 Zr1 166.13(7) 16 4_655 ? Zr1 Zr2 Zr1 60.515(19) . 4_655 ? Zr1 Zr2 Zr1 60.37(2) 13_655 4_655 ? O3 Zr2 Zr1 90.04(11) . 16 ? O3 Zr2 Zr1 35.17(6) 16 16 ? O4 Zr2 Zr1 91.16(11) 19_655 16 ? O4 Zr2 Zr1 35.70(6) . 16 ? O2 Zr2 Zr1 111.28(7) . 16 ? O2 Zr2 Zr1 166.13(7) 19_655 16 ? O2 Zr2 Zr1 110.81(7) 11_655 16 ? O2 Zr2 Zr1 75.37(7) 16 16 ? Zr1 Zr2 Zr1 60.37(2) . 16 ? Zr1 Zr2 Zr1 60.517(19) 13_655 16 ? Zr1 Zr2 Zr1 90.77(2) 4_655 16 ? N2 Fe1 N2 161.1(4) . 20 ? N2 Fe1 N1 88.67(5) . 16_556 ? N2 Fe1 N1 88.66(5) 20 16_556 ? N2 Fe1 N1 88.66(5) . . ? N2 Fe1 N1 88.66(5) 20 . ? N1 Fe1 N1 163.7(4) 16_556 . ? N2 Fe1 Cl1 99.5(2) . . ? N2 Fe1 Cl1 99.5(2) 20 . ? N1 Fe1 Cl1 98.2(2) 16_556 . ? N1 Fe1 Cl1 98.2(2) . . ? Zr1 O3 Zr1 111.74(18) 4_655 . ? Zr1 O3 Zr2 108.86(14) 4_655 . ? Zr1 O3 Zr2 108.86(14) . . ? Zr1 O4 Zr1 110.07(17) . 16 ? Zr1 O4 Zr2 108.00(15) . . ? Zr1 O4 Zr2 108.00(15) 16 . ? C1 O2 Zr2 130.4(2) . . ? C1 O1 Zr1 135.1(3) . . ? C9 N1 C9 105.6(5) . 20 ? C9 N1 Fe1 127.1(2) . . ? C9 N1 Fe1 127.1(2) 20 . ? C11 N2 C11 104.7(5) 16_556 . ? C11 N2 Fe1 127.1(2) 16_556 . ? C11 N2 Fe1 127.1(2) . . ? C9 C8 C11 125.3(4) . . ? C9 C8 C5 118.0(4) . . ? C11 C8 C5 116.7(4) . . ? C8 C11 N2 125.0(4) . . ? C8 C11 C12 125.0(4) . . ? N2 C11 C12 110.0(4) . . ? C2 C3 C4 119.3(5) . . ? C10 C10 C9 108.2(2) 20 . ? C3 C2 C7 119.8(4) . . ? C3 C2 C1 120.9(4) . . ? C7 C2 C1 119.2(4) . . ? O1 C1 O2 126.6(4) . . ? O1 C1 C2 117.1(4) . . ? O2 C1 C2 116.3(4) . . ? C2 C7 C6 118.8(5) . . ? C8 C9 N1 124.9(4) . . ? C8 C9 C10 126.0(4) . . ? N1 C9 C10 109.0(4) . . ? C5 C6 C7 122.0(5) . . ? C6 C5 C4 118.8(4) . . ? C6 C5 C8 119.3(5) . . ? C4 C5 C8 121.9(5) . . ? C5 C4 C3 121.1(5) . . ? C12 C12 C11 107.6(3) 16_556 . ? _diffrn_measured_fraction_theta_max 0.997 _diffrn_reflns_theta_full 22.05 _diffrn_measured_fraction_theta_full 0.997 _refine_diff_density_max 1.104 _refine_diff_density_min -1.186 _refine_diff_density_rms 0.060 |

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