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zhangyu164新蟲(chóng) (正式寫(xiě)手)
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[求助]
關(guān)于飛灰的XRD分析 已有1人參與
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各位大神，求助�。。。。�！審稿意見(jiàn)不會(huì)回答。。。。。。。。關(guān)于XRD的半定量分析垃圾焚燒飛灰中的非晶體含量及組成。 我文中有一段話(huà)是對(duì)城市生活垃圾焚燒飛灰XRD檢測(cè)結(jié)果（如下圖）的描述：“According to X-ray diffraction (XRD) analysis, the investigated fly ash sample had a highly complex mineralogy. As shown in Fig. 3, the main crystalline compounds were calcite (CaCO3), halite (NaCl) and sylvite (KCl). In addition, the presence of crystal structures, such as calcium chlorite hydroxide (CaClOH), silicon chloride (SiCl4), calcium chloride hydrate (Ca(ClO)2•4H2O), iron sulfide (FeS) and portlandite (Ca(OH)2) were also verified. According to the diffraction pattern obtained by XRD, the main components of this sample include calcium chloride hydroxide, halite, silver aluminum sulfide, silicon chloride, stannite and sylvite, which confirms the results of XRF.” 這是審稿人的意見(jiàn)：“Authors used XRD analysis for identification of the crystalline compounds of fly ash. Unfortunately, the analysis is only qualitative. The semi quantitative analysis could give better information about material composition. Moreover, it is well known that materials treated in high temperatures usually contain high amounts of amorphous phase. I would recommend to perform XRD analysis with some standard and to determine semi quantitative composition and content of amorphous phase, if possible.” 他說(shuō)：我這個(gè)XRD分析只是 定性分析，半定量分析可以更好的體現(xiàn)材料的組成。 并且材料在高溫下會(huì)有非晶體產(chǎn)生，所以審稿人認(rèn)為，應(yīng)該用某種標(biāo)準(zhǔn)來(lái)進(jìn)行XRD的半定量分析飛灰中非晶體的組成和含量。 至今我看到的關(guān)于對(duì)飛灰的XRD結(jié)果的描述都是定性分析飛灰中的結(jié)晶相物質(zhì)，還沒(méi)有看到XRD半定量分析的，而且還是關(guān)于非晶體的。。。。。我看到有文章中提到說(shuō)，XRD衍射圖譜上呈現(xiàn)出較多小的、波紋狀的峰，說(shuō)明飛灰中含有大量的非晶態(tài)的玻璃類(lèi)物質(zhì)，大多數(shù)情況下，飛灰中的重金屬富集在非結(jié)晶相中，在晶體相中分布很少。 這個(gè)XRD的半定量分析飛灰中的非晶體，該怎么弄？或者 我可以用一個(gè)很好的理由去反駁這個(gè)審稿人的意見(jiàn)？？？？？？？？  1491786327(1).jpg |
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