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PDF#71-1178: QM=Calculated; d=Calculated; I=(Unknown)
Cobalt Oxide
CoO
Radiation=CuKa1 Lambda=1.5406 Filter=
Calibration= 2T=36.476-77.501 I/Ic(RIR)=4.92
Ref: Level-1 PDF

Cubic,  Fm-3m(225) Z=4 mp=
CELL: 4.263 x 4.263 x 4.263 <90.0 x 90.0 x 90.0> P.S=
Density(c)=6.423 Density(m)= Mwt= Vol=77.5
Ref: Ibid.

Strong Lines: 2.13/X  2.46/7  1.51/5  1.29/2  1.23/1

2-Theta d(?) I(f)  ( h k l) Theta  1/(2d) 2pi/d  n^2
36.476  2.4612 67.6  ( 1 1 1)  18.238  0.2031  2.5529 3
42.370  2.1315  100.0  ( 2 0 0)  21.185  0.2346  2.9478 4
61.470  1.5072 47.5  ( 2 2 0)  30.735  0.3317  4.1688 8
73.637  1.2853 17.7  ( 3 1 1)  36.818  0.3890  4.8883 11
77.501  1.2306 12.0  ( 2 2 2)  38.750  0.4063  5.1057 12

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PDF#02-0925: QM=Uncommon(?); d=Film/Visual; I=(Unknown)
Cobalt Hydroxide
Co(OH)2
Radiation=CuKa1 Lambda=1.5406 Filter=
Calibration= 2T=19.029-98.082 I/Ic(RIR)=
Ref: Level-1 PDF

Z= mp=
P.S=
Density(c)= Density(m)= Mwt= Vol=
Ref: Ibid.

Strong Lines: 2.37/X  2.74/X  2.68/X  4.66/8  4.00/7  1.78/5  1.58/4  2.00/3

2-Theta d(?) I(f)  ( h k l) Theta  1/(2d) 2pi/d  n^2
19.029  4.6600 80.0          9.514  0.1073  1.3483
22.206  4.0000 70.0          11.103  0.1250  1.5708
32.655  2.7400  100.0          16.327  0.1825  2.2931
33.407  2.6800  100.0          16.703  0.1866  2.3445
37.933  2.3700  100.0          18.966  0.2110  2.6511
45.305  2.0000 30.0          22.652  0.2500  3.1416
51.283  1.7800 50.0          25.642  0.2809  3.5299
58.355  1.5800 40.0          29.178  0.3165  3.9767
60.457  1.5300 30.0          30.229  0.3268  4.1067
61.797  1.5000 30.0          30.899  0.3333  4.1888
69.581  1.3500 10.0          34.791  0.3704  4.6542
72.030  1.3100 20.0          36.015  0.3817  4.7963
77.547  1.2300 1.0          38.774  0.4065  5.1083
81.503  1.1800 1.0          40.752  0.4237  5.3247
89.931  1.0900 1.0          44.965  0.4587  5.7644
98.082  1.0200 2.0          49.041  0.4902  6.1600

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2樓2018-05-07 18:56:06

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PDF#15-0806: QM=Star(+); d=(Unknown); I=Diffractometer
Cobalt
Co (Dark gray)
Radiation=CoKa1 Lambda=1.78897 Filter=Fe
Calibration=Internal(W) d-Cutoff= I/Ic(RIR)=
Ref= Natl. Bur. Stand. (U.S.) Monogr. 25, 4 10 (1966)

Cubic - Powder Diffraction,  Fm-3m (225) Z=4 mp=
Cell=3.5447 Pearson=cF4 (Cu)
Density(c)=8.788 Density(m)=8.82A Mwt=58.93 Vol=44.54 F(5)=238.1(.0042,5)
Ref= Ibid.

Strong Line: 2.05/X 1.77/4 1.07/3 1.25/3 1.02/1 0.00/1 0.00/1 0.00/1 0.00/1 0.00/1
NOTE:  Sample prepared by heating cobalt oxalate in H2 for 10 minutes at 300 C.
Spectroscopic analysis: 0.1 to 1.0% each of Ni and Sb; and 0.01 to 0.1% each of Al and Fe.
Pattern taken at 25 C.

d(A)    I(f) I(v)  h  k  l  n^2  2-Theta Theta  1/(2d) 2pi/d
2.046  100.0  100.0  1  1  1 3 44.216  22.108  0.2443  3.0699
1.772 40.0 46.0  2  0  0 4 51.522  25.761  0.2821  3.5452
1.253 25.0 41.0  2  2  0 8 75.853  37.927  0.3990  5.0137
1.068 30.0 57.0  3  1  1 11 92.224  46.112  0.4678  5.8787
1.023 12.0 24.0  2  2  2 12 97.657  48.828  0.4886  6.1401

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3樓2018-05-07 18:56:33

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PDF#73-1701: QM=Calculated; d=Calculated; I=(Unknown)
Cobalt Oxide
Co3O4
Radiation=CuKa1 Lambda=1.5406 Filter=
Calibration= 2T=19.000-85.767 I/Ic(RIR)=4.48
Ref: Level-1 PDF

Cubic,  Fd-3m(227) Z=8 mp=
CELL: 8.0835 x 8.0835 x 8.0835 <90.0 x 90.0 x 90.0> P.S=
Density(c)=6.055 Density(m)= Mwt= Vol=528.2
Ref: Ibid.

Strong Lines: 2.44/X  2.86/3  1.43/3  1.56/3  2.02/2  4.67/2  2.33/1  1.65/1

2-Theta d(?) I(f)  ( h k l) Theta  1/(2d) 2pi/d  n^2
19.000  4.6670 18.1  ( 1 1 1) 9.500  0.1071  1.3463 3
31.272  2.8579 32.4  ( 2 2 0)  15.636  0.1750  2.1985 8
36.847  2.4373  100.0  ( 3 1 1)  18.424  0.2051  2.5780 11
38.549  2.3335 9.3  ( 2 2 2)  19.275  0.2143  2.6926 12
44.811  2.0209 19.4  ( 4 0 0)  22.406  0.2474  3.1091 16
49.084  1.8545 0.1  ( 3 3 1)  24.542  0.2696  3.3881 19
55.657  1.6500 7.6  ( 4 2 2)  27.828  0.3030  3.8079 24
59.358  1.5557 28.8  ( 5 1 1)  29.679  0.3214  4.0389 27
65.237  1.4290 31.4  ( 4 4 0)  32.619  0.3499  4.3970 32
68.631  1.3664 1.2  ( 5 3 1)  34.315  0.3659  4.5985 35
69.744  1.3472 0.1  ( 4 4 2)  34.872  0.3711  4.6637 36
74.123  1.2781 2.0  ( 6 2 0)  37.061  0.3912  4.9160 40
77.344  1.2327 5.9  ( 5 3 3)  38.672  0.4056  5.0970 43
78.409  1.2186 3.3  ( 6 2 2)  39.204  0.4103  5.1559 44
82.629  1.1667 1.7  ( 4 4 4)  41.315  0.4285  5.3852 48
85.767  1.1319 0.7  ( 5 5 1)  42.883  0.4417  5.5509 51

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