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gaoyuan1398版主
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[交流]
【求助】XRD
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那位大俠幫忙給我一個(gè)ErPO4,Er(PO3)3,YbPO4,Yb(PO3)3的XRD衍射標(biāo)準(zhǔn)卡��！ 先謝謝了！��！ Email：mingchengguo1978@163.com [ Last edited by hslining on 2009-9-10 at 17:08 ] |
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Johnsson
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小木蟲(金幣+0.5):給個(gè)紅包，謝謝回帖交流
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Card Information Names: Erbium Phosphate Formula: Er P O4 PDF Number: 9-383 Quality: star Subfiles: inorganic NBS Cell and Symmetry Information System: tetragonal Space Group: I41/amd (no. 141) a: 6.863 c: 6.007 Density (Dx): 6.155 Z: 4 Instrument Information Radiation: CuKa1 Wavelength: 1.5405 Filter: Ni Instrument(d): unknown Instrument(I): diffractometer I type: unknown Comments and Additional Information Colour: Pink Preparation: Sample prepared hydrothermally at 400 C from erbium oxide and dilute phosphoric acid. Analysis: Spectrographic analysis showed no impurities greater than 0.01%. Temperature: Pattern taken at 25 C. Literature References General: Natl. Bur. Stand. (U.S.), Circ. 539 9 31 (1960) PeakList h k l d I 1 0 1 4.5200 55 2 0 0 3.4300 100 2 1 1 2.7330 25 1 1 2 2.5540 65 2 2 0 2.4260 20 2 0 2 2.2610 12 3 0 1 2.1382 25 1 0 3 1.9224 16 3 2 1 1.8144 20 3 1 2 1.7596 45 4 0 0 1.7157 14 2 1 3 1.6771 10 4 1 1 1.6039 6 4 2 0 1.5347 12 3 0 3 1.5063 4 0 0 4 1.5023 6 3 3 2 1.4244 14 3 2 3 1.3792 12 2 0 4 1.3759 1 4 3 1 1.3379 8 4 1 3 1.2802 12 2 2 4 1.2769 1 5 2 1 1.2465 2 5 1 2 1.2283 10 4 4 0 1.2120 4 1 0 5 1.1832 4 6 0 0 1.1438 6 4 3 3 1.1321 1 4 0 4 1.1301 8 2 1 5 1.1189 6 6 1 1 1.1089 4 5 3 2 1.0957 10 6 2 0 1.0851 6 4 2 4 1.0732 10 5 4 1 1.0550 2 3 2 5 1.0161 4 6 3 1 1.0081 4 6 1 3 0.9833 6 1 1 6 0.9808 1 |
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Card Information Names: Erbium Phosphate Formula: Er ( P O3 )3 PDF Number: 35-295 Quality: questionable Subfiles: inorganic Cell and Symmetry Information System: unknown Instrument Information Radiation: Wavelength: Instrument(d): unknown Instrument(I): unknown I type: unknown Comments and Additional Information Quality: O assigned because unindexed. Preparation: Made by heating Er ( P O3 )3 !x H2 O at 900 C. Literature References General: Ezhova, Z. et al. Russ. J. Inorg. Chem. (Engl. Transl.) 26 192 (1981) Peak Data PeakList h k l d I - - - 5.6300 75 - - - 5.0300 30 - - - 4.1000 100 - - - 3.9170 9 - - - 3.8240 60 - - - 3.6630 55 - - - 3.5230 40 - - - 3.2670 8 - - - 2.9980 40 - - - 2.8850 55 - - - 2.5950 25 - - - 2.5710 35 - - - 2.5160 19 - - - 2.4320 20 - - - 2.1810 16 - - - 2.1510 25 - - - 2.0470 17 - - - 2.0140 15 |
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Card Information Names: Ytterbium Phosphate Formula: Yb P O4 PDF Number: 24-1410 Quality: questionable Subfiles: inorganic Cell and Symmetry Information System: tetragonal Space Group: I41/amd (no. 141) a: 6.81 c: 5.97 Instrument Information Radiation: CuKa1 Wavelength: 1.54056 Instrument(d): unknown Instrument(I): unknown I type: unknown Comments and Additional Information Preparation: Obtained on heating Yb P O4 !3 H2 O. Literature References General: Kuznetsov et al. Russ. J. Inorg. Chem. (Engl. Transl.) 14 1449 (1969) Peak Data PeakList h k l d I - - - 4.9900 10 1 0 1 4.5500 20 2 0 0 3.3900 100 - - - 3.0100 5 2 1 1 2.7200 5 1 1 2 2.5200 60 2 2 0 2.4000 20 2 0 2 2.2300 5 3 0 1 2.1100 35 1 0 3 1.9150 35 - - - 1.8760 10 3 2 1 1.7990 20 3 1 2 1.7410 60 4 0 0 1.6970 10 - - - 1.6520 5 4 1 1 1.5910 10 4 2 0 1.5200 20 3 3 2 1.4160 20 2 0 4 1.3660 20 5 0 1 1.3270 20 2 2 4 1.2690 35 5 2 1 1.2410 10 5 1 2 1.2190 20 |
4樓2009-07-20 08:46:12
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小木蟲(金幣+0.5):給個(gè)紅包，謝謝回帖交流
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Card Information Names: Ytterbium Phosphate Formula: Yb ( P O3 )3 PDF Number: 35-356 Quality: calculated Subfiles: inorganic Cell and Symmetry Information System: monoclinic Space Group: P21/c (no. 14) a: 11.219 b: 19.983 c: 9.999 b: 97.30 Instrument Information Radiation: CuKa1 Wavelength: 1.5405981 Instrument(d): calculated Instrument(I): calculated I type: peak heights Comments and Additional Information Pattern: See ICSD 2132 (PDF 01-070-1039). Literature References General: Majling, J. et al. Calc. Powder Diff. Patterns for Anhydrous Phos. 227 (1979) Unit Cell: Hong, H. Acta Crystallogr., Sec. B 30 1857 (1974) Peak Data PeakList h k l d I 0 2 1 7.0308 1 1 3 0 5.7122 4 0 3 1 5.5280 55 0 0 2 4.9569 28 0 1 2 4.8128 1 1 4 0 4.5578 2 2 3 -1 4.0662 100 2 0 -2 3.9588 5 1 3 -2 3.8737 4 2 3 1 3.7890 29 1 3 2 3.6275 17 1 5 -1 3.5702 4 2 0 2 3.4876 20 1 4 -2 3.4478 2 2 4 1 3.3859 1 0 6 0 3.3287 5 3 3 0 3.2408 4 0 2 3 3.1380 2 1 6 1 3.0056 3 0 3 3 2.9608 22 2 6 0 2.8573 19 2 5 -2 2.8135 2 4 0 0 2.7811 6 0 6 2 2.7643 9 2 3 -3 2.7462 8 1 7 -1 2.6853 2 4 2 -1 2.6713 1 1 7 1 2.6422 1 2 5 2 2.6287 1 4 0 -2 2.5687 11 4 3 -1 2.5588 13 2 6 -2 2.5489 17 2 3 3 2.4981 9 0 0 4 2.4794 7 0 1 4 2.4610 2 1 8 0 2.4365 2 4 3 1 2.4176 9 2 6 2 2.4100 9 2 0 -4 2.3793 5 2 1 -4 2.3624 2 3 6 1 2.3577 2 1 6 -3 2.3388 3 2 7 -2 2.3156 1 4 0 2 2.3042 4 |
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