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sd71469190木蟲 (著名寫手)
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CryEngComm小修，大家都是多久回復(fù)的。（附有審稿意見） 已有9人參與
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Reviewer(s)' Comments to Author: Referee: 1 Comments to the Author The present manuscript (CrystEngComm CE-ART-××××××) by×××× et al. is an interesting piece of work that deals with the synthesis and detailed description of X-ray crystal structures of the two coordination polymers. The thermal and photoluminescent properties of the obtained materials have been also studied. The work appears to be rather original, the methodology is appropriate and the conclusions made correspond to the obtained results. The graphical material is rather appealing and facilitates the understanding of structural features. In general, this work is lies within the scope of CrystEngComm, and its acceptance can be recommended after the minor revision, which should address the following points. 1. The main criticism concerns some hidden details in the synthetic procedure for compounds 1 and 2. These parameters are very important for the reproducibility of the syntheses and must be clearly described.－－－好解決 2. Providing that the compounds have been only characterized by IR-spectroscopy, X-ray structural and elemental analyses, all the bands in the IR-spectra should be specified in section 2.2. In addition, the IR spectra should be given in supporting information.－－－好解決，但是要指認(rèn)全部紅外的峰太難了 3. Graphical abstract and synopsis are missing.－－－好解決 4. The manuscript contains a number of unclear/incorrect expressions (or typos) that should be corrected (e.g. p. 1, line 28; p. 1, lines 32-36; p. 3, lines 2-3; p. 3, line 21; p. 7; line 3, etc.). －－－好解決 Referee: 2 Comments to the Author The paper of ××× reports interesting coordination system and it is interesting for many reasons, which are associated with the original coordination geometries and topology of the compounds. The paper perfectly matches the area of the Journal. It describes a reasonable number of new crystal structures together with a very proficient presentation and discussion. I am happy to support this publication after a certain revision concerning analysis of interpenetration in the crystal structures and somewhat more intensive chemical discussion. 1 The authors should analyze the terminology and symbology of interpenetration according to the most recent works. See: V.A. Blatov, et al., "Vertex-, face-, point-, Schlfli-, and Delaney-symbols in nets, polyhedra and tilings: recommended terminology" CrystEngComm, 2009, 12, 44-48. I.A. Baburin, et al., Interpenetrated Three-Dimensional Networks of Hydrogen-Bonded Organic Species: A Systematic Analysis of the Cambridge Structural Database, Cryst. Growth Des.; 2008; 8(2); 519-539. I.A. Baburin, et al., Interpenetrated three-dimensional hydrogen-bonded networks from metal-organic molecular and one- or two-dimensional polymeric motifs CrystEngComm, 2008, 10, 1822-1838 關(guān)于拓?fù)浞治�，我的結(jié)構(gòu)是比較簡(jiǎn)單的44格子的穿插，這樣子讓分析拓?fù)浜孟窈芗?br /> 2 Also, considering very subtle functional features of the coordinated aminopyrimidine ligand, it may be important to find more discussion for the role of amino group. Thus, the silver ion coordinating to the pyrimidine N-site together with the adjacent NH2 it total constitute a multiple site for the binding of counter anions or solvate H-bond donating/accepting molecules, which may a special feature of the present system or even its special benefit. Additional short discussion for the related complexes with such N/NH-donating species ( could be very helpful. －－－好解決 大家都積極回復(fù)阿，看看這種情況需要修改后幾天回復(fù)阿，我其實(shí)已經(jīng)修改完畢了，文章又看了3遍了（不是一天看的）。這種中的幾率如何？沒太大信心阿 [ Last edited by lby1258 on 2010-6-4 at 20:55 ] |
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