| 6 | 1/1 | 返回列表 |
| 查看: 2437 | 回復: 5 | |||
dzychem鐵桿木蟲 (正式寫手)
|
[交流]
【求助】審稿意見中碰到的flack參數(shù)相關的問題 已有5人參與
|
|
本人有兩個晶體,解析完了以后flack參數(shù)分別是0.691(18)和0.50(2),platon檢測報告有C類提示,分別是: (1)STRVA01_ALERT_4_C Flack test results are ambiguous. From the CIF: _refine_ls_abs_structure_Flack 0.691 From the CIF: _refine_ls_abs_structure_Flack_su 0.018 (2)STRVA01_ALERT_4_C Flack test results are ambiguous. From the CIF: _refine_ls_abs_structure_Flack 0.500 From the CIF: _refine_ls_abs_structure_Flack_su 0.020 但審稿人提出了如下意見: In the Cc non-centrosymmetric space group with heavy atom like Pb, one should expect to be able to determine reliably the absolute structure, which is not the case in this manuscript. In both structures, the value of the Flack parameter is 0.69 and 0.50 respectively with a rather large su. This large su is certainly related to the merging of reflections in the 2/m point group which is incorrect. The data should have been merged in the 2 point group. In any case, the compounds are obviously twinned by inversion and this important characteristic has been completely missed by the authors. 審稿人認為su值偏大,但我覺得應該是不大啊。另外,按照 審稿人的意見,采用2 點群重新合并數(shù)據(jù)后的flack參數(shù)基本上沒有什么變化,不知道有什么問題? 謝謝指教! |
鐵桿木蟲 (著名寫手)

木蟲 (職業(yè)作家)

鐵桿木蟲 (正式寫手)
銅蟲 (初入文壇)
| 6 | 1/1 | 返回列表 |
| 最具人氣熱帖推薦 [查看全部] | 作者 | 回/看 | 最后發(fā)表 | |
|---|---|---|---|---|
|
[考研] 085600 286分 材料求調(diào)劑 +5 | 麻辣魷魚 2026-03-27 | 6/300 |
|
|---|---|---|---|---|
|
[考研] 331環(huán)境科學與工程求調(diào)劑 +3 | 熠然好運氣 2026-03-27 | 3/150 |
|
|
[考研] 291求調(diào)劑 +7 | 孅華 2026-03-22 | 7/350 |
|
|
[考研] 266分,求材料冶金能源化工等調(diào)劑 +5 | 哇呼哼呼哼 2026-03-27 | 7/350 |
|
|
[考研] 070300化學求調(diào)劑 +4 | 起個名咋這么難 2026-03-27 | 4/200 |
|
|
[考研] 285求調(diào)劑 +4 | AZMK 2026-03-27 | 7/350 |
|
|
[考研] 070300求調(diào)劑306分 +3 | 26要上岸 2026-03-27 | 3/150 |
|
|
[考研] 266分求材料化工冶金礦業(yè)等專業(yè)的調(diào)劑 +4 | 哇呼哼呼哼 2026-03-26 | 4/200 |
|
|
[材料工程] 一志愿C9材料與化工專業(yè)總分300求調(diào)劑 +7 | 曼111 2026-03-24 | 8/400 |
|
|
[考研] 調(diào)劑 +3 | 李嘉圖·S·路 2026-03-27 | 3/150 |
|
|
[考研] 求調(diào)劑 +6 | 林之夕 2026-03-24 | 6/300 |
|
|
[考研] 一志愿北京化工大學材料與化工(085600)296求調(diào)劑 +9 | 稻妻小編 2026-03-26 | 9/450 |
|
|
[考研] 281求調(diào)劑 +6 | Koxui 2026-03-24 | 7/350 |
|
|
[考研] 生物技術與工程 +3 | 1294608413 2026-03-25 | 4/200 |
|
|
[考研] 求調(diào)劑 +3 | 李李不服輸 2026-03-25 | 3/150 |
|
|
[考研] 材料調(diào)劑 +3 | iwinso 2026-03-23 | 3/150 |
|
|
[考研] B區(qū)考研調(diào)劑 +4 | yqdszhdap- 2026-03-22 | 5/250 |
|
|
[考研] 材料專碩找調(diào)劑 +5 | 哈哈哈吼吼吼哈 2026-03-23 | 5/250 |
|
|
[考研] 293求調(diào)劑 +3 | 濤濤Wjt 2026-03-22 | 5/250 |
|
|
[考研] 280分求調(diào)劑 一志愿085802 +4 | PUMPT 2026-03-22 | 7/350 |
|