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laiwandefeng銀蟲 (小有名氣)
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[交流]
【求助】求ZnSe PDF卡片 已有2人參與
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本人的Jade 出現(xiàn)了點(diǎn)的小問題，原先能搜索到的ZnSe PDF現(xiàn)在只剩下1個(gè)了(37-1463)。請(qǐng)各位大俠幫我找出其他的PDF 以下面的形式粘貼出來就ok了。 PDF#37-1463: QM=Star(+); d=Diffractometer; I=Diffractometer Stilleite, syn Zn Se (Yellow) d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d 3.272 100.0 94.0 1 1 1 3 27.224 13.612 0.1528 1.9197 2.834 1.0 1.0 2 0 0 4 31.532 15.766 0.1764 2.2163 2.004 65.0 100.0 2 2 0 8 45.195 22.597 0.2494 3.1344 1.709 37.0 67.0 3 1 1 11 53.568 26.784 0.2925 3.6758 1.636 1.0 2.0 2 2 2 12 56.153 28.077 0.3055 3.8391 1.417 8.0 17.0 4 0 0 16 65.858 32.929 0.3529 4.4341 1.300 12.0 28.0 3 3 1 19 72.632 36.316 0.3844 4.8309 1.267 1.0 2.0 4 2 0 20 74.832 37.416 0.3944 4.9562 1.157 13.0 35.0 4 2 2 24 83.463 41.732 0.4321 5.4296 1.091 7.0 20.0 5 1 1 27 89.824 44.912 0.4583 5.7590 1.002 4.0 12.0 4 4 0 32 100.463 50.231 0.4989 6.2698 0.958 7.0 23.0 5 3 1 35 107.001 53.501 0.5218 6.5571 0.944 1.0 3.0 6 0 0 36 109.237 54.618 0.5292 6.6505 0.896 5.0 17.0 6 2 0 40 118.500 59.250 0.5579 7.0102 0.864 2.0 7.0 5 3 3 43 126.002 63.001 0.5784 7.2680 0.854 1.0 4.0 6 2 2 44 128.662 64.331 0.5851 7.3520 0.818 1.0 4.0 4 4 4 48 140.574 70.287 0.6111 7.6790 0.793 3.0 12.0 5 5 1 51 152.049 76.024 0.6299 7.9156 |
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jacy_cheyn
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小木蟲(金幣+0.5):給個(gè)紅包，謝謝回帖
wsht212(金幣+1): 2011-05-30 14:35:40
wsht212(金幣+1): 2011-05-30 14:35:45
小木蟲(金幣+0.5):給個(gè)紅包，謝謝回帖
wsht212(金幣+1): 2011-05-30 14:35:40
wsht212(金幣+1): 2011-05-30 14:35:45
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PDF#37-1463: QM=Star(+); d=Diffractometer; I=Diffractometer Stilleite, syn Zn Se (Yellow) Radiation=CuKa1 Lambda=1.5405981 Filter=Graph Calibration=Internal(W) d-Cutoff=17.7 I/Ic(RIR)= Ref= McMurdie, H., Morris, M., Evans, E., Paretzkin, B., Wong-Ng, W., Zhang, Y. Powder Diffraction, 1 345 (1986) Cubic - Powder Diffraction, F-43m (216) Z=4 mp= Cell=5.6688 Pearson=cF8 (S Zn) Density(c)=5.263 Density(m)=5.92A Mwt=144.34 Vol=182.17 F(18)=171.0(.0058,18) Ref= (1) Zachariasen, W. Z. Phys. Chem. (Leipzig), 124 436 (1926) Strong Line: 3.27/X 2.00/7 1.71/4 1.16/1 1.30/1 1.42/1 1.09/1 0.96/1 0.90/1 1.00/1 NOTE: The sample was obtained from Aesar, a branch of Johnson Matthey, Inc., Seabrook, NH, USA. It was labelled as 99.9% pure. The structure was determined by Zachariasen (1). A metastable hexagonal polymorphic form was found by Pashinkin et al. (2). The mean temperature of data collection was 25.2 C. To replace 5-522, Swanson et al. (3). References to other early patterns will be found in Swanson et al., (3). d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d 3.2729 100.0 94.0 1 1 1 3 27.224 13.612 0.1528 1.9197 2.8349 1.0 1.0 2 0 0 4 31.532 15.766 0.1764 2.2163 2.0046 65.0 100.0 2 2 0 8 45.195 22.597 0.2494 3.1344 1.7094 37.0 67.0 3 1 1 11 53.568 26.784 0.2925 3.6758 1.6366 1.0 2.0 2 2 2 12 56.153 28.077 0.3055 3.8391 1.4170 8.0 17.0 4 0 0 16 65.858 32.929 0.3529 4.4341 1.3006 12.0 28.0 3 3 1 19 72.632 36.316 0.3844 4.8309 1.2678 1.0 2.0 4 2 0 20 74.832 37.416 0.3944 4.9562 1.1572 13.0 35.0 4 2 2 24 83.463 41.732 0.4321 5.4296 1.0910 7.0 20.0 5 1 1 27 89.824 44.912 0.4583 5.7590 1.0021 4.0 12.0 4 4 0 32 100.463 50.231 0.4989 6.2698 0.9582 7.0 23.0 5 3 1 35 107.001 53.501 0.5218 6.5571 0.9448 1.0 3.0 6 0 0 36 109.237 54.618 0.5292 6.6505 0.8963 5.0 17.0 6 2 0 40 118.500 59.250 0.5579 7.0102 0.8645 2.0 7.0 5 3 3 43 126.002 63.001 0.5784 7.2680 0.8546 1.0 4.0 6 2 2 44 128.662 64.331 0.5851 7.3520 0.8182 1.0 4.0 4 4 4 48 140.574 70.287 0.6111 7.6790 0.7938 3.0 12.0 5 5 1 51 152.049 76.024 0.6299 7.9156 |
4樓2011-05-28 21:12:40
linhua0402313
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wsht212(金幣+2):謝謝交流，希望常來！ 2010-07-07 22:12:43
wsht212(金幣+2):謝謝交流，希望常來！ 2010-07-07 22:12:43
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你自己看下面的了： PDF#15-0105: QM=Intermediate; d=(Unknown); I=Film/Visual Zinc Selenide Zn Se Radiation=CuKa1 Lambda=1.5406 Filter= Calibration= d-Cutoff= I/Ic(RIR)= Ref= Korneeva. Sov. Phys. Crystallogr. (Engl. Transl.), 6 505 (1962) Hexagonal - Powder Diffraction, P63mc (186) Z=2 mp= Cell=3.996x6.55 Pearson=hP4 (S Zn) Density(c)=5.230 Density(m)=5.92A Mwt=144.34 Vol=90.58 F(20)=3.5(0.137,42) Ref= Ibid. Strong Line: 3.43/X 2.00/X 3.25/9 1.84/8 3.05/7 1.70/7 2.37/6 1.35/6 1.12/6 0.96/5 NOTE: See 5-522 for pattern of cubic modification. Wurtzite type obtained by decomposing Zn Se ! N2 H4 at 480(20) C. Vapor grown crystals have a=4.003, c=6.540, C=1.634. d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d 3.430 100.0 54.0 1 0 0 25.955 12.978 0.1458 1.8318 3.250 90.0 52.0 0 0 2 27.420 13.710 0.1538 1.9333 3.050 70.0 43.0 1 0 1 29.257 14.629 0.1639 2.0601 2.368 60.0 47.0 1 0 2 37.966 18.983 0.2111 2.6534 1.997 100.0 93.0 1 1 0 45.377 22.688 0.2504 3.1463 1.840 80.0 81.0 1 0 3 49.496 24.748 0.2717 3.4148 1.703 70.0 77.0 1 1 2 53.784 26.892 0.2936 3.6895 1.527 10.0 12.0 2 0 2 60.588 30.294 0.3274 4.1147 1.353 60.0 83.0 2 0 3 69.405 34.702 0.3695 4.6439 1.308 30.0 43.0 2 1 0 72.158 36.079 0.3823 4.8037 1.222 40.0 61.0 1 0 5 78.151 39.075 0.4092 5.1417 1.153 40.0 65.0 3 0 0 83.836 41.918 0.4337 5.4494 1.119 60.0 100.0 2 1 3 87.002 43.501 0.4468 5.6150 1.087 40.0 69.0 3 0 2 90.247 45.123 0.4600 5.7803 1.042 20.0 36.0 1 0 6 95.332 47.666 0.4798 6.0299 1.000 30.0 56.0 2 2 0 100.758 50.379 0.5000 6.2832 0.956 50.0 98.0 2 2 2 107.362 53.681 0.5230 6.5724 0.923 20.0 40.0 2 0 6 113.136 56.568 0.5417 6.8074 0.878 20.0 42.0 3 1 3 122.640 61.320 0.5695 7.1562 0.857 10.0 22.0 4 0 1 128.004 64.002 0.5834 7.3316 |
2樓2010-07-07 17:45:26
laiwandefeng
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jacy_cheyn
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wsht212(金幣+1): 2011-05-30 14:35:51
wsht212(金幣+1): 2011-05-30 14:35:55
wsht212(金幣+1): 2011-05-30 14:35:51
wsht212(金幣+1): 2011-05-30 14:35:55
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PDF#05-0522(Deleted Card): QM=Indexed; d=(Unknown); I=Diffractometer Stilleite, syn Zn Se Radiation=CuKa1 Lambda=1.5405 Filter=Ni Calibration= d-Cutoff= I/Ic(RIR)= Ref= Swanson, Fuyat. Natl. Bur. Stand. (U.S.), Circ. 539, 3 23 (1954) Cubic - Powder Diffraction, F-43m (216) Z=4 mp= Cell=5.667 Pearson=cF8 (S Zn) Density(c)=5.267 Density(m)=5.420 Mwt=144.34 Vol=182.00 F(17)=29.1(0.034,17) Ref= Ibid. Strong Line: 3.27/X 2.00/7 1.71/4 1.16/2 1.30/1 1.42/1 1.09/1 0.96/1 1.00/1 0.90/1 NOTE: Color on specimen from Shinkelobwe, Zaire. Spectroscopic analysis: <0.01% Ba, K, Mo, Na; <0.001% Al, Ca, Fe, Mg, Ni, Pd, Si; <0.0001% Ag, Bi, Cd, Cu, Mn. X-ray pattern at 25 C. Also hexagonal form. To replace 1-690. Deleted by 37-1463. d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d 3.2730 100.0 87.0 1 1 1 3 27.224 13.612 0.1528 1.9197 2.8350 1.0 1.0 2 0 0 4 31.531 15.766 0.1764 2.2163 2.0030 70.0 100.0 2 2 0 8 45.233 22.617 0.2496 3.1369 1.7070 44.0 74.0 3 1 1 11 53.648 26.824 0.2929 3.6808 1.6350 1.0 2.0 2 2 2 12 56.214 28.107 0.3058 3.8429 1.4160 9.0 18.0 4 0 0 16 65.910 32.955 0.3531 4.4373 1.2990 13.0 29.0 3 3 1 19 72.737 36.369 0.3849 4.8369 1.2670 1.0 2.0 4 2 0 20 74.884 37.442 0.3946 4.9591 1.1561 15.0 37.0 4 2 2 24 83.560 41.780 0.4325 5.4348 1.0901 8.0 21.0 5 1 1 27 89.920 44.960 0.4587 5.7639 1.0018 4.0 11.0 4 4 0 32 100.510 50.255 0.4991 6.2719 0.9577 8.0 24.0 5 3 1 35 107.086 53.543 0.5221 6.5607 0.9441 1.0 3.0 6 0 0 36 109.351 54.675 0.5296 6.6552 0.8958 4.0 13.0 6 2 0 40 118.606 59.303 0.5582 7.0141 0.8642 2.0 7.0 5 3 3 43 126.080 63.040 0.5786 7.2705 0.8545 1.0 3.0 6 2 2 44 128.696 64.348 0.5851 7.3531 0.8180 2.0 7.0 4 4 4 48 140.665 70.333 0.6112 7.6812 |
5樓2011-05-28 21:13:31
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