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crazytrees金蟲(chóng) (小有名氣)
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[交流]
【求助】XRD測(cè)試中的熒光問(wèn)題 已有1人參與
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小弟最近投一篇文章,被審稿人問(wèn)到XRD中的熒光問(wèn)題,不知道怎么回答 原文如下: “The authors discuss the occurrence of some amount of amorphous material in their samples. The very flat background would be in contradiction to any amorphous contribution, but is probably the result of a subtracted background profile.” 這個(gè)確實(shí)是平滑過(guò)了,采用jade進(jìn)行的平滑和扣背底。但是在平滑前也確實(shí)是看不出。 This requires explanation together with the cut-off of the fluorescence radiation of Fe induced by Cu-radiation. 這里的熒光衍射是什么的?很少看到文獻(xiàn)中提到這個(gè)。 Lattice parameters need to be determined by the Rietveld method and compared with each other. Some small peak shifts indicate small, but significant differences in the lattice parameters of the samples, requiring explanation. 這個(gè)隨后計(jì)算一下就行了。 期待高人出手幫助。謝謝! |
鐵桿木蟲(chóng) (職業(yè)作家)

金蟲(chóng) (小有名氣)
金蟲(chóng) (小有名氣)
金蟲(chóng) (小有名氣)
金蟲(chóng) (小有名氣)
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