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sd71469190木蟲 (著名寫手)
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[交流]
Crystal Growth and Design 小修中的兩個棘手問題。 已有6人參與
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今日Crystal Growth and Design審稿意見回來,兩個小修一個大修,三人的評價都算不錯?墒堑谌齻大修的審稿人提到了兩個很棘手的問題: Comments: The paper brings new information regarding the aggregation of water molecules into chains or tapes. The two new coordination polymers are interesting as well. However, before acceptance, the authors should address the following questions: 1. Thermal decompostion of the two complexes: the authors claim that the second steps correspond to the loss of the dicarboxylato anions. This is not possible, because the charge of the Ag(I) ions is not neutralized! If metallic silver is obtained, then no Ag-bipy chains can be formed. 2. The quantum yields for the luminescence spectra should be determined and reported. 強調(diào)一下,本人合成的是Ag-吡啶-草酸的2維配位聚合物。第一個問題我覺得問的很好,但是我無法回答, 因為這個問題確實是個問題,但是很多文獻卻也是像我那樣子描述的TGA曲線。 第二個問題由于實驗條件限制我做不了。 這該如何response呢?請高手指點迷津阿,不勝感激 [ Last edited by 王繼偉 on 2010-8-26 at 13:02 ] |
金蟲 (小有名氣)
木蟲 (著名寫手)
木蟲 (著名寫手)
銅蟲 (正式寫手)
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