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dali112金蟲 (小有名氣)
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[求助]
求助pdf：32-0711的標準譜圖對應 的晶面指數(shù)
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| 急求pdf：32-0711（ Nb2O5）的標準譜圖對應 的晶面指數(shù)及a，b，c的值。 |
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xhtangxh
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drg1984(金幣+1): 感謝回帖交流！ 2011-07-18 08:35:51
drg1984(金幣+1): 感謝回帖交流！ 2011-07-18 08:35:51
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你可以把數(shù)據傳上來。建議你拿下面這個卡片試試。 PDF#72-1484: QM=Calculated(C); d=Calculated; I=Calculated Niobium Oxide Nb2 O5 Radiation=CuKa1 Lambda=1.54060 Filter= Calibration= 2T=6.110-89.306 I/Ic(RIR)=4.70 Ref: Calculated from ICSD using POWD-12++ (1997) Tetragonal - (Unknown), I4/mmm (139) Z=16 mp= CELL: 20.44 x 20.44 x 3.832 <90.0 x 90.0 x 90.0> P.S=tI112 (?) Density(c)=4.410 Density(m)=4.350 Mwt=265.81 Vol=1600.99 F(30)=999.9(.0000,33/0) Ref: Mertin, W., Andersson, S., Gruehn, R. J. Solid State Chem., v1 p419 (1970) Strong Lines: 3.61/X 2.80/5 3.77/5 4.82/4 14.5/4 2.06/3 7.23/2 1.59/2 1.72/2 1.69/2 FIZ=017027: At least one TF missing. Calc. density unusual but tolerable. Ueber die Kristallstruktur von M - Nb2 O5 l4 j2 i2 h2 (I4/MMM) A2X5 High-temperature form. 2-Theta d(?) I(f) ( h k l ) Theta 1/(2d) 2pi/d n^2 6.110 14.4533 38.6 ( 1 1 0) 3.055 0.0346 0.4347 8.645 10.2200 0.2 ( 2 0 0) 4.322 0.0489 0.6148 12.237 7.2266 23.0 ( 2 2 0) 6.119 0.0692 0.8694 13.688 6.4637 0.4 ( 3 1 0) 6.844 0.0774 0.9721 17.340 5.1100 0.1 ( 4 0 0) 8.670 0.0978 1.2296 18.400 4.8177 41.0 ( 3 3 0) 9.200 0.1038 1.3042 19.405 4.5705 0.1 ( 4 2 0) 9.702 0.1094 1.3747 22.157 4.0086 0.6 ( 5 1 0) 11.079 0.1247 1.5674 23.602 3.7664 50.6 ( 1 0 1) 11.801 0.1328 1.6682 24.617 3.6133 100.0 ( 4 4 0) 12.309 0.1384 1.7389 25.179 3.5340 11.7 ( 2 1 1) 12.589 0.1415 1.7779 25.387 3.5054 2.7 ( 5 3 0) 12.694 0.1426 1.7924 26.136 3.4067 0.8 ( 6 0 0) 13.068 0.1468 1.8444 26.668 3.3400 1.9 ( 3 0 1) 13.334 0.1497 1.8812 27.577 3.2318 2.0 ( 6 2 0) 13.789 0.1547 1.9441 28.083 3.1748 10.9 ( 3 2 1) 14.042 0.1575 1.9791 29.436 3.0318 1.3 ( 4 1 1) 14.718 0.1649 2.0724 30.909 2.8907 8.5 ( 7 1 0) 15.454 0.1730 2.1736 31.537 2.8345 1.1 ( 6 4 0) 15.768 0.1764 2.2167 31.986 2.7958 52.8 ( 4 3 1) 15.993 0.1788 2.2474 33.194 2.6967 7.9 ( 5 2 1) 16.597 0.1854 2.3300 35.093 2.5550 13.1 ( 8 0 0) 17.546 0.1957 2.4592 35.502 2.5265 6.9 ( 6 1 1) 17.751 0.1979 2.4869 36.210 2.4787 0.1 ( 8 2 0) 18.105 0.2017 2.5349 36.608 2.4527 1.8 ( 5 4 1) 18.304 0.2039 2.5618 37.298 2.4089 3.3 ( 6 6 0) 18.649 0.2076 2.6083 37.832 2.3761 0.1 ( 7 5 0) 18.916 0.2104 2.6443 38.738 2.3226 12.7 ( 7 0 1) 19.369 0.2153 2.7053 39.767 2.2648 0.4 ( 7 2 1) 19.884 0.2208 2.7743 39.906 2.2572 1.9 ( 9 1 0) 19.953 0.2215 2.7836 41.761 2.1612 0.2 ( 6 5 1) 20.880 0.2314 2.9073 41.895 2.1546 0.4 ( 9 3 0) 20.947 0.2321 2.9162 42.729 2.1144 2.5 ( 8 1 1) 21.365 0.2365 2.9716 43.809 2.0647 25.0 ( 7 7 0) 21.905 0.2422 3.0431 44.277 2.0440 1.1 ( 10 0 0) 22.139 0.2446 3.0740 44.615 2.0293 0.9 ( 8 3 1) 22.307 0.2464 3.0962 45.202 2.0043 1.8 ( 10 2 0) 22.601 0.2495 3.1348 45.659 1.9853 0.7 ( 9 5 0) 22.829 0.2518 3.1648 46.439 1.9538 0.2 ( 9 0 1) 23.220 0.2559 3.2160 47.410 1.9160 15.1 ( 0 0 2) 23.705 0.2610 3.2793 47.410 1.9160 15.1 ( 7 6 1) 23.705 0.2610 3.2793 47.892 1.8978 2.6 ( 10 4 0) 23.946 0.2635 3.3108 47.892 1.8978 2.6 ( 1 1 2) 23.946 0.2635 3.3108 48.210 1.8860 0.2 ( 2 0 2) 24.105 0.2651 3.3314 48.210 1.8860 0.2 ( 8 5 1) 24.105 0.2651 3.3314 49.154 1.8520 0.8 ( 2 2 2) 24.577 0.2700 3.3926 49.154 1.8520 0.8 ( 11 1 0) 24.577 0.2700 3.3926 49.583 1.8370 0.1 ( 3 1 2) 24.791 0.2722 3.4204 49.933 1.8249 0.7 ( 9 4 1) 24.967 0.2740 3.4430 50.473 1.8067 2.4 ( 8 8 0) 25.237 0.2768 3.4778 50.894 1.7927 10.5 ( 11 3 0) 25.447 0.2789 3.5049 51.272 1.7804 3.4 ( 3 3 2) 25.636 0.2808 3.5291 52.141 1.7527 0.2 ( 10 6 0) 26.071 0.2853 3.5848 52.440 1.7434 0.1 ( 10 3 1) 26.220 0.2868 3.6039 53.256 1.7186 19.1 ( 8 7 1) 26.628 0.2909 3.6560 54.136 1.6927 16.1 ( 4 4 2) 27.068 0.2954 3.7118 54.136 1.6927 16.1 ( 11 5 0) 27.068 0.2954 3.7118 54.575 1.6802 1.1 ( 12 2 0) 27.288 0.2976 3.7396 54.575 1.6802 1.1 ( 5 3 2) 27.288 0.2976 3.7396 54.935 1.6700 0.2 ( 6 0 2) 27.468 0.2994 3.7624 55.657 1.6500 2.0 ( 6 2 2) 27.828 0.3030 3.8079 55.657 1.6500 2.0 ( 10 5 1) 27.828 0.3030 3.8079 56.938 1.6159 1.6 ( 12 4 0) 28.469 0.3094 3.8883 57.325 1.6059 0.2 ( 9 9 0) 28.663 0.3113 3.9125 57.674 1.5970 2.7 ( 7 1 2) 28.837 0.3131 3.9343 57.674 1.5970 2.7 ( 10 8 0) 28.837 0.3131 3.9343 57.990 1.5891 21.0 ( 6 4 2) 28.995 0.3146 3.9540 57.990 1.5891 21.0 ( 11 4 1) 28.995 0.3146 3.9540 58.859 1.5677 0.9 ( 13 1 0) 29.429 0.3189 4.0080 59.513 1.5520 0.5 ( 12 1 1) 29.756 0.3222 4.0484 60.332 1.5329 4.5 ( 13 3 0) 30.166 0.3262 4.0990 60.332 1.5329 4.5 ( 8 0 2) 30.166 0.3262 4.0990 61.012 1.5174 1.0 ( 8 2 2) 30.506 0.3295 4.1408 61.012 1.5174 1.0 ( 12 3 1) 30.506 0.3295 4.1408 61.820 1.4995 1.1 ( 11 6 1) 30.910 0.3334 4.1902 61.820 1.4995 1.1 ( 6 6 2) 30.910 0.3334 4.1902 63.322 1.4675 0.2 ( 13 5 0) 31.661 0.3407 4.2815 63.322 1.4675 0.2 ( 8 4 2) 31.661 0.3407 4.2815 63.685 1.4600 4.0 ( 14 0 0) 31.843 0.3425 4.3036 63.685 1.4600 4.0 ( 9 1 2) 31.843 0.3425 4.3036 64.409 1.4453 0.4 ( 14 2 0) 32.205 0.3459 4.3472 64.671 1.4401 0.2 ( 13 2 1) 32.335 0.3472 4.3630 65.095 1.4318 0.2 ( 9 3 2) 32.547 0.3492 4.3884 66.103 1.4123 1.3 ( 10 9 1) 33.052 0.3540 4.4488 66.522 1.4045 9.7 ( 7 7 2) 33.261 0.3560 4.4737 66.522 1.4045 9.7 ( 14 4 0) 33.261 0.3560 4.4737 67.582 1.3850 0.9 ( 13 7 0) 33.791 0.3610 4.5367 67.582 1.3850 0.9 ( 10 2 2) 33.791 0.3610 4.5367 67.934 1.3787 0.3 ( 9 5 2) 33.967 0.3627 4.5574 68.222 1.3735 0.3 ( 12 7 1) 34.111 0.3640 4.5744 69.017 1.3597 0.7 ( 15 1 0) 34.508 0.3677 4.6212 69.679 1.3483 1.1 ( 10 4 2) 34.840 0.3708 4.6599 70.059 1.3420 0.3 ( 14 6 0) 35.030 0.3726 4.6821 70.311 1.3378 0.9 ( 13 6 1) 35.155 0.3738 4.6968 71.781 1.3139 4.2 ( 8 8 2) 35.891 0.3805 4.7820 71.781 1.3139 4.2 ( 11 11 0) 35.891 0.3805 4.7820 72.091 1.3090 5.8 ( 12 10 0) 36.045 0.3820 4.7998 72.091 1.3090 5.8 ( 11 3 2) 36.045 0.3820 4.7998 73.053 1.2942 1.2 ( 13 9 0) 36.527 0.3864 4.8550 73.053 1.2942 1.2 ( 11 10 1) 36.527 0.3864 4.8550 73.732 1.2839 6.7 ( 15 0 1) 36.866 0.3894 4.8938 74.164 1.2775 0.3 ( 16 0 0) 37.082 0.3914 4.9183 74.344 1.2749 1.1 ( 15 2 1) 37.172 0.3922 4.9286 74.344 1.2749 1.1 ( 1 0 3) 37.172 0.3922 4.9286 74.840 1.2676 0.5 ( 14 8 0) 37.420 0.3944 4.9566 75.020 1.2650 0.6 ( 13 8 1) 37.510 0.3952 4.9668 75.020 1.2650 0.6 ( 2 1 3) 37.510 0.3952 4.9668 75.144 1.2632 0.6 ( 12 2 2) 37.572 0.3958 4.9738 75.692 1.2555 0.1 ( 3 0 3) 37.846 0.3983 5.0047 76.363 1.2461 0.3 ( 15 4 1) 38.182 0.4013 5.0423 76.363 1.2461 0.3 ( 3 2 3) 38.182 0.4013 5.0423 77.188 1.2348 3.1 ( 15 7 0) 38.594 0.4049 5.0883 77.188 1.2348 3.1 ( 12 4 2) 38.594 0.4049 5.0883 77.490 1.2308 1.6 ( 9 9 2) 38.745 0.4062 5.1051 77.823 1.2263 0.2 ( 10 8 2) 38.911 0.4077 5.1236 78.365 1.2192 2.5 ( 4 3 3) 39.182 0.4101 5.1535 78.820 1.2133 0.6 ( 13 1 2) 39.410 0.4121 5.1786 79.028 1.2106 0.8 ( 16 1 1) 39.514 0.4130 5.1901 79.028 1.2106 0.8 ( 5 2 3) 39.514 0.4130 5.1901 79.755 1.2014 0.1 ( 13 11 0) 39.877 0.4162 5.2298 79.755 1.2014 0.1 ( 15 6 1) 39.877 0.4162 5.2298 80.176 1.1962 0.4 ( 13 3 2) 40.088 0.4180 5.2528 80.176 1.1962 0.4 ( 16 6 0) 40.088 0.4180 5.2528 80.415 1.1932 2.1 ( 16 3 1) 40.208 0.4190 5.2658 81.075 1.1852 0.3 ( 17 3 0) 40.537 0.4219 5.3016 81.075 1.1852 0.3 ( 13 10 1) 40.537 0.4219 5.3016 82.327 1.1703 1.4 ( 14 9 1) 41.164 0.4273 5.3691 82.327 1.1703 1.4 ( 7 0 3) 41.164 0.4273 5.3691 82.777 1.1650 0.2 ( 13 5 2) 41.389 0.4292 5.3931 83.105 1.1613 2.5 ( 14 0 2) 41.553 0.4306 5.4106 83.105 1.1613 2.5 ( 16 5 1) 41.553 0.4306 5.4106 83.791 1.1535 0.6 ( 10 10 2) 41.896 0.4335 5.4471 83.791 1.1535 0.6 ( 17 5 0) 41.896 0.4335 5.4471 84.088 1.1502 0.3 ( 11 9 2) 42.044 0.4347 5.4627 84.356 1.1472 2.8 ( 17 0 1) 42.178 0.4358 5.4769 85.010 1.1401 0.7 ( 17 2 1) 42.505 0.4386 5.5113 85.010 1.1401 0.7 ( 8 1 3) 42.505 0.4386 5.5113 85.426 1.1356 0.1 ( 18 0 0) 42.713 0.4403 5.5331 85.722 1.1324 0.3 ( 14 4 2) 42.861 0.4415 5.5486 86.079 1.1286 0.2 ( 18 2 0) 43.040 0.4430 5.5672 86.253 1.1268 0.1 ( 8 3 3) 43.127 0.4437 5.5762 86.700 1.1221 0.1 ( 13 7 2) 43.350 0.4456 5.5994 86.968 1.1193 0.1 ( 16 7 1) 43.484 0.4467 5.6132 87.709 1.1118 0.1 ( 17 7 0) 43.854 0.4497 5.6514 88.035 1.1085 2.3 ( 18 4 0) 44.018 0.4511 5.6681 88.271 1.1062 1.2 ( 13 12 1) 44.135 0.4520 5.6802 88.271 1.1062 1.2 ( 7 6 3) 44.135 0.4520 5.6802 88.922 1.0997 0.4 ( 14 6 2) 44.461 0.4547 5.7134 88.922 1.0997 0.4 ( 14 11 1) 44.461 0.4547 5.7134 89.306 1.0960 0.2 ( 15 3 2) 44.653 0.4562 5.7328 |
4樓2011-07-18 08:33:10
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