 |
 |
 |
 |
 |
 |
||
 |
 |
 |
 |
 |
| 5 | 1/1 | 返回列表 |
| 查看: 1647 | 回復(fù): 8 | ||
| 當(dāng)前只顯示滿足指定條件的回帖，點(diǎn)擊這里查看本話題的所有回帖 | ||
[求助]
acta e 審稿意見回來，請(qǐng)教！！如何修改和回復(fù)@~~~~~~~~~~~~~
|
||
|
Your paper can be accepted after taking into account the following comments: 1. Abstract: plural in first sentence ..... oxazole goups. second sentence: The complex is six-coordinate ... geometry. or better: The six-coordinate complex displays a distorted octahedral geometry. 2. last sentence: the Cg...Cg distance and symmetry operations must be given. However, the two oxazole units have two five-membered and six six-membered rings. this implies a lot of work defining the centres of gravity (Cg's) for the rings and calculating the distances between Cg's and average perpendicular distances between the ring systems. Moreover, your Fig. 2 does not show the inversion related \p--\p interaction clearly, and the symmetry operators for molecule A and molecule B should also be provided in the caption of Figure 2. You need a programme like PLATON which can help analize this problem by using the "cal all" option. It will also be seen that the complexes are held together by a combination of different \p--\p interactions and a C---H...\p contact when PLATON is applied. (see point 9) The best was to delete the sentence in Abstract ... exhibits obvious intermolecular \p--\p interactions and also delete Fig. 2. Otherwise, details must be calculated, which needs time ... IMPORTANT: all numerical measured values need standard uncertainties (s.u.), which will be described for the Comment section. 3. Computing details: the SHELXS97 and SHELXL97 reference must refer to a new reference: Sheldrick, G. M. (2008). Acta Cryst. A64, 112--122. please use this reference instead of the Sheldrick G. M. (2001). reference please download and read this article which will show you that the Bruker AXS SHELXTL programme should be cited with the new Sheldrick (2008) reference. 3. in the computing details block it should be corrected like: _computing_structure_solution 'SHELXS97 (Sheldrick, 2008)' _computing_structure_refinement 'SHELXL97 (Sheldrick, 2008)' _computing_molecular_graphics 'SHELXTL (Sheldrick, 2008)' _computing_publication_material 'SHELXL97 ' 4. References: Abbady M. A. (1979). .... there is only one author, delete the Assiut ... Assiut E. part there 5. Comment, please short: ... has been reported (Lamansky et l., 2001), among ... please write the trivial names for the ligands (bo) and (bon) in the long introductory sentence, as they appear only once in the text. 6. Comment: please think of having two oxazol ligands, so the average deviation of Ir1 C18 C23 C24 N2 and the dihedral angles as for molecule 1 (average is 0.0628 and 0.0719 (typo mol. 1, please check, and mol. 2) the s.u.'s for dihedral angles in parentheses: 6.5(2)\% (6.9(1)\% for mol.2), 9.2(1)\% (11.4(1)\% for mol. 2). please check with MPLA in SHELXL97. 7. Comment: please shorten the text by using just one sentence which refers to Table 1. two values each averaged not necessary. (Relevant coordination distances shown in Table 1.) 8. Table 1: please show only the six Ir---C/N/O bond distances and omit other distances and angles by replacement of yes with ? in the cif tables. The values are kept with the Supplementary materials. 9. Fig. 2: delete in Text in the Comment or you may download the programme PLATON and chose two inversion related \p--\p interactions with details as proposed in point 2, and the weak C26---H26...Cg9 contact. Cg9 is the centroid of ring C18 - C23, symmetry operation -x, y, 3/2 - z for the \p--\p interactions please chose two examples Cg3...Cg3i and Cg3...Cg6i (there are many others) the rings are parallel and inversion related. symmetry code i (7_556) is 1/2 - x, 1/2 - y, 1 - z -------------------------------------------------------- PLATON download is recommended via http://www.cryst.chem.uu.nl/platon/p1000000.html help-files are also available there for Windows systems download WinPLATON via http://www.chem.gla.ac.uk/~louis/software/platon/ A short PLATON tutorial is offered by Lachlan Cranswick at http://www.ccp14.ac.uk/tutorial/platon/index.html --------------------------------------------------------------- 10. Experimental, reference: .... to the literature (Abbady, 1979). Please send me an email indicating how you have responded to each of the comments. You should upload a new CIF at the web address: http://submission.iucr.org/submi ... Xaz7dXI43jLy/si2371 Please acknowledge receipt of this message as soon as you see it, so that I know it has arrived safely. Best wishes |
回復(fù)此樓» 猜你喜歡
284求調(diào)劑
已經(jīng)有10人回復(fù)
-
一志愿山東大學(xué)藥學(xué)學(xué)碩求調(diào)劑
已經(jīng)有4人回復(fù)
-
07化學(xué)280分求調(diào)劑
已經(jīng)有4人回復(fù)
-
298-一志愿中國農(nóng)業(yè)大學(xué)-求調(diào)劑
已經(jīng)有12人回復(fù)
-
求材料，環(huán)境專業(yè)調(diào)劑
已經(jīng)有3人回復(fù)
-
335求調(diào)劑
已經(jīng)有5人回復(fù)
-
求調(diào)劑
已經(jīng)有7人回復(fù)
-
一志愿吉大化學(xué)322求調(diào)劑
已經(jīng)有4人回復(fù)
-
環(huán)境學(xué)碩288求調(diào)劑
已經(jīng)有8人回復(fù)
-
341求調(diào)劑(一志愿湖南大學(xué)070300)
已經(jīng)有6人回復(fù)
» 本主題相關(guān)價(jià)值貼推薦，對(duì)您同樣有幫助:
- 急求ACTA E 審稿意見回復(fù)
已經(jīng)有3人回復(fù)
- 請(qǐng)教Appliced optics 修改意見中為什么只看到一個(gè)審稿人的意見？
已經(jīng)有9人回復(fù)
- 投了ACTA，返回大修，審稿人問到數(shù)據(jù)重現(xiàn)性的問題，如何回答？
已經(jīng)有7人回復(fù)
- acta E 審稿意見回復(fù)（語法方面的)，萬急！~~~~~ 請(qǐng)高手看下！
已經(jīng)有7人回復(fù)
- 【請(qǐng)教】請(qǐng)教acta e審稿意見
已經(jīng)有4人回復(fù)
- 審稿意見回來了，有些地方看不明白，請(qǐng)教大家
已經(jīng)有3人回復(fù)
- 審稿意見回復(fù)請(qǐng)教
已經(jīng)有4人回復(fù)
- 【請(qǐng)教】投稿acta e 后被拒，修改后再投稿...
已經(jīng)有11人回復(fù)
- 審稿意見回來。請(qǐng)教投過國際氫能源的蟲友啊
已經(jīng)有17人回復(fù)
yguang
木蟲 (職業(yè)作家)
- 應(yīng)助: 24 (小學(xué)生)
- 金幣: 12850.8
- 紅花: 14
- 帖子: 4683
- 在線: 618.4小時(shí)
- 蟲號(hào): 696608
- 注冊(cè): 2009-02-05
- 專業(yè): 微生物遺傳育種學(xué)
3樓2011-08-18 12:16:43
2樓2011-08-18 12:09:07
4樓2011-08-18 12:22:01
5樓2011-08-18 13:37:26
| 最具人氣熱帖推薦 [查看全部] | 作者 | 回/看 | 最后發(fā)表 | |
|---|---|---|---|---|
|
[考研] 07化學(xué)280分求調(diào)劑 +4 | 722865 2026-03-23 | 4/200 |
|
|---|---|---|---|---|
|
[考研] 298-一志愿中國農(nóng)業(yè)大學(xué)-求調(diào)劑 +11 | 手機(jī)用戶 2026-03-17 | 12/600 |
|
|
|
[考研] 求調(diào)劑 +7 | 十三加油 2026-03-21 | 7/350 |
|
|
|
[考研] 085600材料與化工調(diào)劑 +7 | A-哆啦Z夢(mèng) 2026-03-23 | 12/600 |
|
|
|
[考研] 335分 | 材料與化工專碩 | GPA 4.07 | 有科研經(jīng)歷 +4 | cccchenso 2026-03-23 | 4/200 |
|
|
|
[考研] 265求調(diào)劑 +10 | 梁梁校校 2026-03-17 | 10/500 |
|
|
|
[考研] 一志愿武理材料工程348求調(diào)劑 +6 | ￣^￣゜汗 2026-03-19 | 9/450 |
|
|
|
[論文投稿] 急發(fā)核心期刊論文 +3 | 賢達(dá)問津 2026-03-23 | 5/250 |
|
|
|
[考研] 接收2026碩士調(diào)劑(學(xué)碩+專碩) +4 | allen-yin 2026-03-23 | 6/300 |
|
|
|
[考研] 北科281學(xué)碩材料求調(diào)劑 +8 | tcxiaoxx 2026-03-20 | 9/450 |
|
|
|
[考研] 276求調(diào)劑 +3 | YNRYG 2026-03-21 | 4/200 |
|
|
|
[考研] 307求調(diào)劑 +11 | 冷笙123 2026-03-17 | 11/550 |
|
|
|
[考研] 315分，誠求調(diào)劑，材料與化工085600 +3 | 13756423260 2026-03-22 | 3/150 |
|
|
|
[考研] 求調(diào)劑一志愿海大，0703化學(xué)學(xué)碩304分，有大創(chuàng)項(xiàng)目，四級(jí)已過 +6 | 幸運(yùn)哩哩 2026-03-22 | 10/500 |
|
|
|
[考研] 286分人工智能專業(yè)請(qǐng)求調(diào)劑愿意跨考！ +4 | lemonzzn 2026-03-17 | 8/400 |
|
|
|
[考研] 一志愿深大，0703化學(xué)，總分302，求調(diào)劑 +4 | 七月-七七 2026-03-21 | 4/200 |
|
|
|
[考研] 336求調(diào)劑 +5 | rmc8866 2026-03-21 | 5/250 |
|
|
|
[考研] 265求調(diào)劑 +12 | 梁梁校校 2026-03-19 | 14/700 |
|
|
|
[考研] 中南大學(xué)化學(xué)學(xué)碩337求調(diào)劑 +3 | niko- 2026-03-19 | 6/300 |
|
|
|
[考研] 廣西大學(xué)家禽遺傳育種課題組2026年碩士招生（接收計(jì)算機(jī)專業(yè)調(diào)劑） +3 | 123阿標(biāo) 2026-03-17 | 3/150 |
|