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我們已經(jīng)針對(duì)審稿人的意見在實(shí)驗(yàn)部分添加了各個(gè)樣品的加入量，在這篇文章中Ni/Ti（原子比）的理論值是1:20，在實(shí)驗(yàn)中樣品的各個(gè)元素并沒有損失。 確實(shí)XPS技術(shù)不是一個(gè)合適的測(cè)定元素含量的方法，他只是一個(gè)表面的定性工具，用來定量誤差很大。正如審稿人所說ICP是一個(gè)比較合適的方法。我們測(cè)試XPS的目的是為了驗(yàn)證鎳的前軀體硝酸鎳是否在400度下完全分解為氧化鎳，并不是為了對(duì)其晶型定量分析。XPS結(jié)構(gòu)顯示硝酸鎳在400度下完全分解為氧化鎳，Ni/Ti（原子比）為1:25，確實(shí)存在一定的誤差。 |
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wolfmanhd(金幣+5, 翻譯EPI+1): 這是翻譯軟件翻譯的 2012-01-15 10:34:12
愛與雨下(翻譯EPI-1): 2012-01-15 12:37:14
愛與雨下(金幣-5): 2012-01-15 12:37:29
愛與雨下: epi收回 2012-01-15 12:37:47
愛與雨下(金幣-5): 2012-01-15 12:38:17
愛與雨下: google翻譯！ 2012-01-15 12:38:22
wolfmanhd(金幣+5, 翻譯EPI+1): 這是翻譯軟件翻譯的 2012-01-15 10:34:12
愛與雨下(翻譯EPI-1): 2012-01-15 12:37:14
愛與雨下(金幣-5): 2012-01-15 12:37:29
愛與雨下: epi收回 2012-01-15 12:37:47
愛與雨下(金幣-5): 2012-01-15 12:38:17
愛與雨下: google翻譯！ 2012-01-15 12:38:22
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僅供參考 We have sent to the opinions of the part in the experiment added each sample addition amount, in this article Ni/Ti (atomic ratio) is the theoretical 1:20, in the experiment of sample each element and no damage. Really XPS technology is not an appropriate determination method for the determination of the elements, he is just a surface qualitative tools, used to quantitative error is very large. As referees said ICP is a more appropriate method. We test the purpose of the XPS was to examine the body nitric acid nickel nickel before in 400 degrees is the complete decomposition for oxidation nickel, and not for the crystal quantitative analysis. XPS structure shows in 400 degrees nickel nitric acid oxidation nickel for all under decomposition, Ni/Ti (atomic ratio) for pitted, does exist certain error. |
2樓2012-01-14 23:15:01
weichin
鐵桿木蟲 (職業(yè)作家)
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【答案】應(yīng)助回帖
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wolfmanhd(金幣+45, 翻譯EPI+1): ★★★很有幫助 2012-01-16 10:48:29
愛與雨下(金幣+1): 2012-01-16 11:55:25
wolfmanhd(金幣+45, 翻譯EPI+1): ★★★很有幫助 2012-01-16 10:48:29
愛與雨下(金幣+1): 2012-01-16 11:55:25
| According the reviewers’ comments, we have increased the inputs of each sample in the experiment. The theoretical value of Ni/Ti atomic ratio is 1:25, and no element of the samples in the experiment was lost. The XPS technique is certainly not suitable for measuring the content of each element; but rather, it is only a superficial qualitative tool which causes big errors in quantitative determination. Just as the reviewer pointed out, the ICP is a more appropriated tool. We chose the XPS technique with a view to testing whether the nickel precursor nickel nitrate is completely decomposed into nickel oxide under the temperature of 400 degrees Celsius, rather than to giving a quantitative analysis of its crystal form. The XPS structure showed that nickel nitrate is completely decomposed into nickel oxide under the temperature of 400 degrees Celsius with Ni/Ti atomic ratio being 1:25, and there were certainly some errors. |
3樓2012-01-15 15:31:02
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