| 1 | 1/1 | 返回列表 |
| 查看: 266 | 回復(fù): 0 | |||
lincoln227銀蟲 (小有名氣)
|
[求助]
文章段落修改求助!
|
|
原文:“Subsequently, 4 and corresponding amine (7 equiv.) in a mixture of water/1,4-dioxane (1:1, v/v) at 95 °C for 24 h according to the previously reported procedure [20]. However, this procedure needed long reaction time and the deacetylation was incomplete due to poor solubility. Therefore, the method was modified and the problem was overcome by the use of ethanol as solvent, triethylamine as deacid reagent in the ammonolysis of 4, and sodium ethoxide as catalyst in the deacetylation. Using this efficient modified procedure, 32 of N6-alkyl(aryl)-2-alkyl(aryl)thioadenosines (Table 2, 5a1-a8 and 5b1-b24) were obtained in good yields. ” 審稿人的意見:1.the phrases are not written with the correct structure, they must be revised because nouns and verbs are not clear. 2.the paragraph of Chemistry discussion previously mentioned should be clarified being a possible option: "Subsequently, the target compounds 5 were obtained in good yields by reaction of the adequate compound 4 with the corresponding amine in ethanol using first triethylamine and after sodium, as an efficient modification of previous reported method (20)". 由于本人英語水平有限,實(shí)在看不出原文有何毛病,請(qǐng)大家不吝賜教,謝謝! |

找到一些相關(guān)的精華帖子,希望有用哦~
| 1 | 1/1 | 返回列表 |
| 最具人氣熱帖推薦 [查看全部] | 作者 | 回/看 | 最后發(fā)表 | |
|---|---|---|---|---|
|
[考研] 材料科學(xué)與工程求調(diào)劑 +6 | 深V宿舍吧 2026-03-29 | 6/300 |
|
|---|---|---|---|---|
|
[考研] 327求調(diào)劑 +6 | 汲亦昊 2026-03-29 | 6/300 |
|
|
[考研] 297求調(diào)劑 +11 | 田洪有 2026-03-26 | 11/550 |
|
|
[考研] 0703 化學(xué) 求調(diào)劑,一志愿山東大學(xué) 342 分 +4 | Shern—- 2026-03-28 | 4/200 |
|
|
[考研] 071000生物學(xué)求調(diào)劑,初試成績343 +7 | 小小甜面團(tuán) 2026-03-25 | 7/350 |
|
|
[考研] 食品工程專碩一志愿中海洋309求調(diào)劑 +4 | 小張zxy張 2026-03-26 | 8/400 |
|
|
[考研] 復(fù)試調(diào)劑 +3 | raojunqi0129 2026-03-28 | 3/150 |
|
|
[考研] 085600,材料與化工321分求調(diào)劑 +9 | 大饞小子 2026-03-28 | 9/450 |
|
|
[考研] 070300求調(diào)劑306分 +4 | 26要上岸 2026-03-27 | 4/200 |
|
|
[考研] 266分,求材料冶金能源化工等調(diào)劑 +7 | 哇呼哼呼哼 2026-03-27 | 9/450 |
|
|
[考研] 調(diào)劑 +3 | 好好讀書。 2026-03-28 | 3/150 |
|
|
[考研] 材料277求調(diào)劑 +7 | min3 2026-03-24 | 7/350 |
|
|
[考研] 328求調(diào)劑 +7 | 嗯滴的基本都 2026-03-27 | 7/350 |
|
|
[考研] 一志愿哈工大,085400,320,求調(diào)劑 +4 | gdlf9999 2026-03-24 | 4/200 |
|
|
[考研] 302求調(diào)劑 +4 | 錦衣衛(wèi)藤椒 2026-03-25 | 4/200 |
|
|
[考研] 一志愿南航材料專317分求調(diào)劑 +5 | 炸呀炸呀炸薯?xiàng)l 2026-03-23 | 5/250 |
|
|
[考研] 080500求調(diào)劑 +3 | zzzzfan 2026-03-24 | 3/150 |
|
|
[考研]
|
13659058978 2026-03-24 | 4/200 |
|
|
[考研] 335求調(diào)劑 +4 | yuyu宇 2026-03-23 | 5/250 |
|
|
[考研] 333求調(diào)劑 +3 | ALULU4408 2026-03-23 | 3/150 |
|