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[求助]
求助:兩個晶體均有相同的A類錯誤
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做了兩個有機化合物的單晶,均有相同的A類錯誤: PLAT018_ALERT_1_A _diffrn_measured_fraction_theta_max .NE. _full ! 嚴重嗎?要如何解決? 謝謝! |
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_diffrn_measured_fraction_theta_max 0.848 _diffrn_reflns_theta_full 28.22 _diffrn_measured_fraction_theta_full 0.948 當將_diffrn_measured_fraction_theta_full 0.948 該位0.848, 經(jīng)檢查出現(xiàn)了新的A類錯誤, REFLT03_ALERT_3_A Reflection count < 85% complete (theta max?) From the CIF: _diffrn_reflns_theta_max 28.22 From the CIF: _diffrn_reflns_theta_full 28.22 From the CIF: _reflns_number_total 4358 TEST2: Reflns within _diffrn_reflns_theta_max Count of symmetry unique reflns 5136 Completeness (_total/calc) 84.85% PLAT029_ALERT_3_A _diffrn_measured_fraction_theta_full Low ....... 0.848 是儀器問題嗎? 需要重新培養(yǎng)單晶重測嗎? |
至尊木蟲 (文壇精英)
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