| 5 | 1/1 | 返回列表 |
| 查看: 1354 | 回復(fù): 13 | ||
| 當(dāng)前只顯示滿足指定條件的回帖,點擊這里查看本話題的所有回帖 | ||
山石巖金蟲 (著名寫手)
|
[求助]
晶體E編輯意見,急求怎么解決
|
|
|
本人新手,對晶體一竅不通。最近投了一篇晶體E編輯提出錯誤如下,請大俠們指教怎么改正。錯誤: 1.In the abstract and comments section, could you please provide standard uncertainties for all dihedral angles quoted 2.In '_publ_section_exptl_refinement' you have indicated that the Friedel pairs were merged, This is, in fact, not the case. Friedel pairs were refined in the structure and the absolute configuration determined from this data. Could you please check and correct. 3. In '_publ_section_exptl_refinement' could you provide details of the disorder present in the structure. 4. In '_publ_section_exptl_refinement' could you provide details of the location and refinement of the N-H proton in this compound. 本人是藥物化學(xué)專業(yè)的,對這個實在是搞不明白,希望專業(yè)人士幫幫忙啊。要是需要數(shù)據(jù)我發(fā)到你們郵箱里。謝謝啊! |
金蟲 (著名寫手)
至尊木蟲 (文壇精英)
|
1. 給出二面角的標(biāo)準(zhǔn)偏差 一般用xp的mpla吧 2.檢查一下解析時Friedel pairs應(yīng)該精修了,沒有merged 3.簡要描述下無序的處理 4.N-H的處理,一般是從傅里葉圖中找到然后適當(dāng)限制的吧,具體看自己的結(jié)構(gòu) 不懂的話請教解析的老師吧 |
至尊木蟲 (著名寫手)
|
1.摘要與評論部分所有二面角增加偏差值(用括號括起來); 2.在實驗精修部分,你指出了Friedal對合并了,但事實上不是如此,請再檢查并改正. 3.請在實驗精修部分提供有關(guān)結(jié)構(gòu)中無序的詳細(xì)信息.即你這個結(jié)構(gòu)中有無序,應(yīng)該加以描述. 4.在實驗精修部分請?zhí)峁┯嘘P(guān)N-H質(zhì)子確定與精修的細(xì)節(jié),即你是如何加這個氫的,如何精修的,例如有否鍵長限制等. |
金蟲 (著名寫手)
| 最具人氣熱帖推薦 [查看全部] | 作者 | 回/看 | 最后發(fā)表 | |
|---|---|---|---|---|
|
[考研] 328求調(diào)劑,英語六級551,有科研經(jīng)歷 +6 | 生物工程調(diào)劑 2026-03-17 | 10/500 |
|
|---|---|---|---|---|
|
[考研] 293求調(diào)劑 +12 | zjl的號 2026-03-16 | 17/850 |
|
|
[考研] 一志愿中南大學(xué)化學(xué)學(xué)碩0703總分337求調(diào)劑 +3 | niko- 2026-03-22 | 3/150 |
|
|
[考研]
|
酥酥魚.. 2026-03-21 | 3/150 |
|
|
[考研] 求調(diào)劑 +3 | 13341 2026-03-20 | 3/150 |
|
|
[考研] 0703化學(xué)297求調(diào)劑 +3 | Daisy☆ 2026-03-20 | 3/150 |
|
|
[考研] 材料 271求調(diào)劑 +5 | 展信悅_ 2026-03-21 | 5/250 |
|
|
[考研] 301求調(diào)劑 +10 | yy要上岸呀 2026-03-17 | 10/500 |
|
|
[考研] 初始318分求調(diào)劑(有工作經(jīng)驗) +3 | 1911236844 2026-03-17 | 3/150 |
|
|
[考研] 二本跨考鄭大材料306英一數(shù)二 +3 | z1z2z3879 2026-03-17 | 3/150 |
|
|
[考研] 一志愿西南交大,求調(diào)劑 +5 | 材化逐夢人 2026-03-18 | 5/250 |
|
|
[考研] 一志愿武漢理工材料工程專碩調(diào)劑 +9 | Doleres 2026-03-19 | 9/450 |
|
|
[考研]
|
然11 2026-03-19 | 4/200 |
|
|
[考研] 261求B區(qū)調(diào)劑,科研經(jīng)歷豐富 +3 | 牛奶很忙 2026-03-20 | 4/200 |
|
|
[考研] 求調(diào)劑 +3 | eation27 2026-03-20 | 3/150 |
|
|
[考研] 材料學(xué)碩318求調(diào)劑 +5 | February_Feb 2026-03-19 | 5/250 |
|
|
[考研] 081700化工學(xué)碩調(diào)劑 +3 | 【1】 2026-03-16 | 3/150 |
|
|
[考研] 288求調(diào)劑,一志愿華南理工大學(xué)071005 +5 | ioodiiij 2026-03-17 | 5/250 |
|
|
[考研] 085601材料工程專碩求調(diào)劑 +10 | 慕寒mio 2026-03-16 | 10/500 |
|
|
[考研] 277調(diào)劑 +5 | 自由煎餅果子 2026-03-16 | 6/300 |
|