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people2416鐵桿木蟲 (正式寫手)
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[求助]
請高手幫我看看吧,O(∩_∩)O謝謝
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小弟做合成的,對晶體知之甚少,我現(xiàn)在有一個(gè)單晶,有幾個(gè)G類錯(cuò)誤,想發(fā)Acta E,不知道需不需要修改了?如果需要,應(yīng)該怎么改啊,小弟實(shí)在能力有限,請各位不吝賜教,謝謝! Alert level G REFLT03_ALERT_4_G Please check that the estimate of the number of Friedel pairs is correct. If it is not, please give the correct count in the _publ_section_exptl_refinement section of the submitted CIF. From the CIF: _diffrn_reflns_theta_max 26.99 From the CIF: _reflns_number_total 2441 Count of symmetry unique reflns 1449 Completeness (_total/calc) 168.46% TEST3: Check Friedels for noncentro structure Estimate of Friedel pairs measured 992 Fraction of Friedel pairs measured 0.685 Are heavy atom types Z>Si present yes PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF .... ? PLAT007_ALERT_5_G Note: Number of Unrefined D-H Atoms ............ 2 PLAT194_ALERT_1_G Missing _cell_measurement_reflns_used datum .... ? PLAT195_ALERT_1_G Missing _cell_measurement_theta_max datum .... ? PLAT196_ALERT_1_G Missing _cell_measurement_theta_min datum .... ? 另外,還想請教一下文章中Refinement一項(xiàng)怎么寫的?投稿的話不知道有沒有什么模板的啊,請大家?guī)蛶臀野,小弟再次向大家表示感謝。! |
至尊木蟲 (職業(yè)作家)
鐵桿木蟲 (正式寫手)
至尊木蟲 (職業(yè)作家)
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鐵桿木蟲 (正式寫手)
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