| 5 | 1/1 | 返回列表 |
| 查看: 1047 | 回復(fù): 10 | ||
| 當(dāng)前只顯示滿足指定條件的回帖,點擊這里查看本話題的所有回帖 | ||
hnthdht至尊木蟲 (職業(yè)作家)
知識青年
|
[求助]
審稿人問Is the compd really triclinic ?
|
|
|
數(shù)據(jù)如下,這有問題嗎? _symmetry_cell_setting Triclinic _symmetry_space_group_name_H-M P-1 _cell_length_a 9.7217(6) _cell_length_b 10.6264(6) _cell_length_c 11.6749(7) _cell_angle_alpha 63.7590(10) _cell_angle_beta 89.8230(10) _cell_angle_gamma 74.9970(10) _cell_volume 1036.25(11) _cell_formula_units_Z 2 |

至尊木蟲 (職業(yè)作家)
知識青年
|
checkcif結(jié)果如下,A,B,C,D錯誤都沒有啊 Datablock: 4 Bond precision: C-C = 0.0056 A Wavelength=0.71073 Cell: a=9.7217(6) b=10.6264(6) c=11.6749(7) alpha=63.759(1) beta=89.823(1) gamma=74.997(1) Temperature: 298 K Calculated Reported Volume 1036.25(11) 1036.25(11) Space group P -1 P-1 Hall group -P 1 ? Moiety formula Mo4 O13, C12 H20 N4 ? Sum formula C12 H20 Mo4 N4 O13 C12 H20 Mo4 N4 O13 Mr 812.08 812.08 Dx,g cm-3 2.603 2.603 Z 2 2 Mu (mm-1) 2.442 2.442 F000 784.0 784.0 F000’ 770.53 h,k,lmax 12,13,14 12,13,14 Nref 4298 4210 Tmin,Tmax 0.711,0.783 0.696,0.792 Tmin’ 0.670 Correction method= NONE Data completeness= 0.980 Theta(max)= 26.500 R(reflections)= 0.0273( 3914) wR2(reflections)= 0.0664( 4210) S = 1.072 Npar= 300 The following ALERTS were generated. Each ALERT has the format test-name_ALERT_alert-type_alert-level. Click on the hyperlinks for more details of the test. Alert level G PLAT004_ALERT_5_G Info: Polymeric Structure Found with Dimension . 1 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF .... ? PLAT154_ALERT_1_G The su’s on the Cell Angles are Equal .......... 0.00100 Deg. PLAT432_ALERT_2_G Short Inter X...Y Contact O12 .. C4 .. 2.97 Ang. PLAT764_ALERT_4_G Overcomplete CIF Bond List Detected (Rep/Expd) . 1.15 Ratio |

鐵桿木蟲 (著名寫手)
金蟲 (小有名氣)

| 最具人氣熱帖推薦 [查看全部] | 作者 | 回/看 | 最后發(fā)表 | |
|---|---|---|---|---|
|
[考研] 尋找調(diào)劑 +4 | 倔強(qiáng)芒? 2026-03-21 | 4/200 |
|
|---|---|---|---|---|
|
[考研] 298求調(diào)劑一志愿211 +3 | 上岸6666@ 2026-03-20 | 3/150 |
|
|
[考研] 260求調(diào)劑 +3 | 朱芷琳 2026-03-20 | 4/200 |
|
|
[考研] 考研調(diào)劑 +4 | 來好運來來來 2026-03-21 | 4/200 |
|
|
[考研] 280求調(diào)劑 +11 | 咕嚕曉曉 2026-03-18 | 12/600 |
|
|
[考研] 0805 316求調(diào)劑 +3 | 大雪深藏 2026-03-18 | 3/150 |
|
|
[考研] 311求調(diào)劑 +3 | 勇敢的小吳 2026-03-20 | 3/150 |
|
|
[考研] 求調(diào)劑 +3 | .m.. 2026-03-21 | 4/200 |
|
|
[基金申請]
學(xué)校已經(jīng)提交到NSFC,還能修改嗎?
40+4
|
babangida 2026-03-19 | 9/450 |
|
|
[考研] 0805材料320求調(diào)劑 +3 | 深海物語 2026-03-20 | 3/150 |
|
|
[考研] 279求調(diào)劑 +5 | 紅衣隱官 2026-03-21 | 5/250 |
|
|
[考研] 265求調(diào)劑 +9 | 梁梁校校 2026-03-17 | 9/450 |
|
|
[考研] 一志愿 南京航空航天大學(xué)大學(xué) ,080500材料科學(xué)與工程學(xué)碩 +5 | @taotao 2026-03-20 | 5/250 |
|
|
[考研] 281求調(diào)劑(0805) +14 | 煙汐憶海 2026-03-16 | 25/1250 |
|
|
[考研] 一志愿中國海洋大學(xué),生物學(xué),301分,求調(diào)劑 +5 | 1孫悟空 2026-03-17 | 6/300 |
|
|
[考研] 0703化學(xué)調(diào)劑 +4 | 18889395102 2026-03-18 | 4/200 |
|
|
[考研] 085600材料與化工調(diào)劑 324分 +10 | llllkkkhh 2026-03-18 | 12/600 |
|
|
[考研] 0703化學(xué)調(diào)劑 +5 | pupcoco 2026-03-17 | 8/400 |
|
|
[考研] 一志愿,福州大學(xué)材料專碩339分求調(diào)劑 +3 | 木子momo青爭 2026-03-15 | 3/150 |
|
|
[考研] 中科院材料273求調(diào)劑 +4 | yzydy 2026-03-15 | 4/200 |
|