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1054356769鐵蟲 (正式寫手)
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[求助]
急求LiSr4(BO3)3的XRD標準卡片!急求!
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| 急求LiSr4(BO3)3的XRD標準卡片!急求! |
版主 (文壇精英)
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*data for ICSD #170861 Coll Code 170861 Rec Date 2006/04/01 Mod Date 2010/08/01 Chem Name Lithium Tetrastrontium Trisborate Structured Li Sr4 (B O3)3 Sum B3 Li1 O9 Sr4 ANX AB3C4X9 D(calc) 4.24 Title Structure determination and relative properties of novel cubic borates M M'4 (B O3)3 (M= Li, M'= Sr and M= Na, M'= Sr, Ba) Author(s) Wu, L.;Chen, X.-L.;Li, H.;He, M.;Xu, Y.-P.;Li, X.-Z. Reference Inorganic Chemistry (2005), 44(18), 6409-6414 Unit Cell 14.95066(5) 14.95066(5) 14.95066(5) 90. 90. 90. Vol 3341.83 Z 16 Space Group I a -3 d SG Number 230 Cryst Sys cubic Pearson cI272 Wyckoff h g2 f b a R Value .0609 Red Cell I 12.947 12.947 12.947 109.471 109.471 109.471 1670.915 Trans Red 0.500 0.500 -0.500 / -0.500 0.500 0.500 / 0.500 -0.500 0.500 Comments AE: Li: 6o O6; Sr1: 6o O6; Sr2: 6p2c O8; B: 3l O3; O1: 60 Li Sr4 B; O2: 3l Sr2 B The structure has been assigned a PDF number (calculated powder diffraction data): 01-073-3772 Rietveld profile refinement applied Structure type prototype : LiSr4B3O9 Temperature factors available Structure type : LiSr4B3O9 X-ray diffraction (powder) Atom # OX SITE x y z SOF H ITF(U) Sr 1 +2 16 a .0000 .0000 .0000 1 0 .0188(10) Sr 2 +2 48 f .0000 .2500 .00242(8) 1 0 .0106(3) O 1 -2 96 h .1335(5) .2714(3) .1286(6) 1 0 .007(1) O 2 -2 48 g .1769(4) .4269(4) .1250 1 0 .024(3) B 1 +3 48 g .1086(7) .3586(7) .1250 1 0 .003(5) Li 1 +1 16 b .1250 .1250 .1250 1 0 .033(13) Std. Notes Transformation Method: Tidy Std. Cell 14.9507 14.9507 14.9507 90 90 90 Std. Vol. 3341.83 Std. Z 16 Std. SG IA3-D Std. Atom Atom # OX SITE x y z SOF Sr 1 +2 16 a 0 0 0 1. Sr 2 +2 48 f .00242 0 .25 1. O 1 -2 96 h .12860 .13350 .27140 1. O 2 -2 48 g .125 .67690 .57310 1. B 1 +3 48 g .125 .60860 .64140 1. Li 1 +1 16 b .125 .125 .125 1. *end for ICSD #170861 |

版主 (文壇精英)
| Li Sr4 (B O3)3的cif文件 |

鐵桿木蟲 (職業(yè)作家)
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############################################################################## ### Entry exported from Match! User Database ### ############################################################################## ### Entry No.: ### ############################################################################## ### Data published by: ### ### ### ### COD (Crystallography Open Database) ### ### ### ############################################################################## **************************** Phase Classification **************************** Formula sum : B3 Li O9 Sr4 Sample name : 4309484 I/Ic : 7.06 Quality : C (calculated) Reference : ******************************* Origin of Data ******************************* Entry source : COD (Crystallography Open Database); http://www.crystallography.net Orig. entry no: 4309484 ***************************** Crystal Structure ****************************** Published crystallographic data: Space group : I a -3 d (230) Crystal system : cubic Cell parameters : a= A Cell meas. cond. : T= K Formula units (Z): 16 Atomic coordinates: Element x y z Bi Focc Sr 0.000000 0.000000 0.000000 1.4830 1.0000 Sr 0.000000 0.250000 0.002420 0.8340 1.0000 O 0.133500 0.271400 0.128600 0.5520 1.0000 O 0.176900 0.426900 0.125000 1.8940 1.0000 B 0.108600 0.358600 0.125000 0.2360 1.0000 Li 0.125000 0.125000 0.125000 2.6040 1.0000 ****************************** Diffraction Data ****************************** Published diffraction lines: Wavelength used for calculation of 2theta values: lambda = 1.541874 A d 2theta Int. h k l Mult. 6.1036 14.5127 1.72 2 1 1 24 5.2859 16.7729 0.20 2 0 2 12 3.9957 22.2488 18.58 3 2 1 48 3.7377 23.8067 614.31 4 0 0 6 3.3431 26.6657 2.44 4 0 2 24 3.1875 27.9931 14.15 3 2 3 24 3.0518 29.2650 0.00 4 2 2 24 2.9321 30.4883 7.10 4 3 1 48 2.7296 32.8112 11.40 5 2 1 48 2.6429 33.9193 1000.00 4 0 4 12 2.4253 37.0684 42.10 5 3 2 48 2.3639 38.0679 0.02 6 0 2 24 2.3069 39.0456 0.77 5 4 1 48 2.2044 40.9421 10.30 6 3 1 48 2.1579 41.8635 442.42 4 4 4 8 2.1143 42.7687 0.37 5 4 3 48 2.0733 43.6587 1.66 4 6 0 24 2.0345 44.5345 9.90 5 2 5 24 1.9979 45.3968 0.73 6 4 2 48 1.8987 47.9109 9.34 6 5 1 48 1.8688 48.7269 236.30 8 0 0 6 1.8403 49.5328 3.32 7 4 1 48 1.8130 50.3291 1.00 8 0 2 24 1.7869 51.1163 3.18 6 5 3 48 1.7620 51.8950 1.50 6 0 6 12 1.7380 52.6654 1.24 7 4 3 48 1.6928 54.1831 0.00 7 5 2 48 1.6715 54.9311 350.89 8 0 4 24 1.6313 56.4070 0.21 8 4 2 48 1.6122 57.1356 4.68 6 5 5 24 1.5937 57.8581 0.85 6 4 6 24 1.5759 58.5750 0.81 7 5 4 48 1.5420 59.9928 2.76 7 6 3 48 1.5259 60.6940 263.91 8 4 4 24 1.5102 61.3905 0.60 8 5 3 48 1.4951 62.0824 0.92 6 8 0 24 1.4803 62.7699 5.02 7 2 7 24 1.4660 63.4531 0.06 8 6 2 48 1.4521 64.1324 0.01 9 4 3 48 1.4255 65.4793 2.58 7 6 5 48 1.4003 66.8120 1.07 8 7 1 48 1.3881 67.4733 0.28 8 6 4 48 1.3763 68.1315 0.43 9 6 1 48 1.3648 68.7866 0.78 10 4 2 48 1.3536 69.4389 0.20 8 7 3 48 1.3319 70.7352 1.38 9 6 3 48 1.3215 71.3795 110.68 8 0 8 12 1.2915 73.2982 4.67 7 6 7 24 1.2820 73.9334 0.85 8 6 6 24 1.2727 74.5666 0.48 8 7 5 48 1.2636 75.1978 0.00 10 6 2 48 1.2546 75.8273 1.98 9 6 5 48 1.2459 76.4549 140.01 8 4 8 24 1.2373 77.0809 0.11 9 7 4 48 1.2289 77.7054 0.05 12 0 2 24 1.2207 78.3284 2.14 10 5 5 24 1.2127 78.9500 0.72 10 6 4 48 1.2048 79.5702 0.20 9 8 3 48 1.1894 80.8071 2.31 10 7 3 48 1.1820 81.4239 118.02 12 0 4 24 1.1746 82.0397 0.00 11 5 4 48 1.1675 82.6546 0.03 8 10 0 24 1.1604 83.2686 2.96 9 2 9 24 1.1535 83.8819 0.00 10 8 2 48 1.1467 84.4944 0.12 9 8 5 48 1.1334 85.7177 1.07 10 7 5 48 1.1269 86.3286 106.05 12 4 4 24 1.1206 86.9390 0.15 12 5 3 48 1.1144 87.5491 0.30 10 8 4 48 1.1082 88.1590 0.67 10 9 1 48 1.1022 88.7686 0.21 12 6 2 48 1.0962 89.3780 0.43 11 7 4 48 1.0846 90.5969 2.63 10 9 3 48 1.0790 91.2063 38.08 8 8 8 8 1.0734 91.8159 0.51 9 8 7 48 1.0679 92.4258 0.01 12 6 4 48 1.0625 93.0359 0.96 9 6 9 24 1.0572 93.6463 0.58 10 0 10 12 1.0519 94.2571 0.02 12 7 3 48 1.0417 95.4804 3.42 10 9 5 48 1.0366 96.0929 59.48 8 12 0 24 1.0317 96.7061 0.14 11 8 5 48 1.0268 97.3201 0.01 12 8 2 48 1.0220 97.9349 0.31 13 6 3 48 1.0173 98.5507 0.06 10 4 10 24 1.0126 99.1675 0.11 11 9 4 48 ******************************** Experimental ******************************** Physical properties: Calc. density : 4.24300 g/cm^3 ********************************** Remarks *********************************** Comments : |
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