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fengqianxv銀蟲 (正式寫手)
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actE 編輯回信請教 已有1人參與
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1. The O atoms of both nitro groups exhibit high thermal motion. Might a disorder model be more appropriate? Please discuss this. O原子沒有無序現(xiàn)象,這個怎么回應(yīng)? 3. Your software references list all Bruker software, but your Figures at least look like they were produced with PLATON. Correct this. 圖確實(shí)是PLATON畫的,但是以前發(fā)的文章都是用Bruker software參考的? 6. In Related Literature, describe how the 'related structures' cited in Vicente et al (2005) actually relate to the structure in this manuscript. 是讓描述兩者結(jié)構(gòu)如何相關(guān)嗎? |
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1. The O atoms of both nitro groups exhibit high thermal motion. Might a disorder model be more appropriate? Please discuss this. 硝基的O原子溫度因子高,是不是有可能存在無序現(xiàn)象,請解釋? 你可以嘗試無序處理,即讓氧原子部分占據(jù)自由精修,看占有率的大小,如果接近100%,說明沒有無序現(xiàn)象的存在,溫度因子高只能從其他方面解釋,比如配位環(huán)境等做解釋,如果占有率不是接近100%,則告訴占據(jù)率,并重新精修數(shù)據(jù)。 3. Your software references list all Bruker software, but your Figures at least look like they were produced with PLATON. Correct this. 你文中的圖看起來PLATON畫的,但是引用的文獻(xiàn)確實(shí)用Bruker software,請確認(rèn)或更正? 6. In Related Literature, describe how the 'related structures' cited in Vicente et al (2005) actually relate to the structure in this manuscript. 是讓描述兩者結(jié)構(gòu)如何相關(guān)嗎? 是的 |

銀蟲 (正式寫手)
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