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[求助]
急求�。�！在線等！��！求聚丙烯的PDF卡
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| 聚丙烯的PDF卡，做XRD 時用于對比的PDF卡。 |
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yanhj0
鐵桿木蟲 (知名作家)
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【答案】應(yīng)助回帖
★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★
dj880317: 金幣+45, ★★★★★最佳答案, 謝謝你，完全吻合，就是這個了。 2012-06-07 20:42:47
dj880317: 回帖置頂 2012-06-07 20:45:15
dj880317: 金幣+45, ★★★★★最佳答案, 謝謝你，完全吻合，就是這個了。 2012-06-07 20:42:47
dj880317: 回帖置頂 2012-06-07 20:45:15
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PDF#50-2397: QM=Calculated(C); d=Calculated; I=Calculated $GA-Polypropylene ( C3 H6 )n Radiation=CuKa1 Lambda=1.54060 Filter= Calibration= 2T=8.503-75.999 I/Ic(RIR)=1.06 Ref: Kaduk, J., Amoco Corporation, Naperville, IL, USA. Private Communication (1998) Monoclinic - Single Crystal, P21/c (14) Z=12 mp= CELL: 6.63 x 20.78 x 6.5 <90.0 x 99.5 x 90.0> P.S=mP108 (?) Density(c)=0.949 Density(m)=0.94A Mwt=42.08 Vol=883.23 F(30)=58.8(.0093,55/0) Ref: Immirzi, A., Iannelli, P. Macromolecules, v21 p768 (1988) Strong Lines: 6.24/X 4.76/7 4.06/7 5.20/5 4.16/4 3.46/1 3.12/1 3.06/1 2.09/1 2.13/1 NOTE: Hydrogen atoms included in calculated positions. Isotropic B = 2.5 for C and 5.0 for H. Symmetric Cauchy profile function with resolution FWHM=0.08$DE at 2$GU=30$DE. 2-Theta d(?) I(f) ( h k l) Theta 1/(2d) 2pi/d n^2 8.503 10.3900 2.6 ( 0 2 0) 4.252 0.0481 0.6047 13.530 6.5391 1.2 ( 1 0 0) 6.765 0.0765 0.9609 14.187 6.2375 100.0 ( 1 1 0) 7.094 0.0802 1.0073 17.054 5.1950 54.0 ( 0 4 0) 8.527 0.0962 1.2095 18.646 4.7549 71.4 ( 1 3 0) 9.323 0.1052 1.3214 19.657 4.5126 2.3 (-1 2 1) 9.828 0.1108 1.3924 21.364 4.1556 36.9 ( 1 1 1) 10.682 0.1203 1.5120 21.877 4.0593 70.4 (-1 3 1) 10.939 0.1232 1.5478 22.626 3.9267 1.8 ( 1 2 1) 11.313 0.1273 1.6001 24.592 3.6170 3.7 (-1 4 1) 12.296 0.1382 1.7371 24.592 3.6170 3.7 ( 1 3 1) 12.296 0.1382 1.7371 25.372 3.5075 2.6 ( 1 5 0) 12.686 0.1426 1.7913 25.701 3.4633 10.8 ( 0 6 0) 12.851 0.1444 1.8142 27.253 3.2695 2.8 ( 2 0 0) 13.627 0.1529 1.9217 27.253 3.2695 2.8 ( 1 4 1) 13.627 0.1529 1.9217 27.869 3.1986 1.9 (-1 5 1) 13.935 0.1563 1.9643 28.145 3.1680 1.5 ( 0 1 2) 14.072 0.1578 1.9834 28.598 3.1188 8.8 ( 2 2 0) 14.299 0.1603 2.0146 28.829 3.0942 1.6 (-2 1 1) 14.415 0.1616 2.0306 28.902 3.0866 1.6 (-1 0 2) 14.451 0.1620 2.0356 29.130 3.0630 6.5 (-1 1 2) 14.565 0.1632 2.0513 29.130 3.0630 6.5 ( 0 2 2) 14.565 0.1632 2.0513 29.794 2.9962 0.2 (-2 2 1) 14.897 0.1669 2.0971 30.080 2.9684 1.0 ( 1 5 1) 15.040 0.1684 2.1167 30.709 2.9090 0.2 ( 0 3 2) 15.354 0.1719 2.1599 31.374 2.8489 3.3 (-1 6 1) 15.687 0.1755 2.2055 32.326 2.7671 0.2 ( 2 4 0) 16.163 0.1807 2.2707 32.803 2.7279 1.5 ( 0 4 2) 16.402 0.1833 2.3033 32.999 2.7122 3.4 ( 2 1 1) 16.499 0.1844 2.3166 33.231 2.6938 1.4 ( 0 7 1) 16.615 0.1856 2.3325 33.856 2.6455 1.2 ( 2 2 1) 16.928 0.1890 2.3751 34.201 2.6196 0.1 ( 1 2 2) 17.100 0.1909 2.3985 34.501 2.5975 0.1 ( 0 8 0) 17.250 0.1925 2.4189 34.886 2.5697 0.3 ( 2 5 0) 17.443 0.1946 2.4451 35.245 2.5444 3.6 ( 2 3 1) 17.622 0.1965 2.4695 35.577 2.5213 0.4 ( 1 3 2) 17.788 0.1983 2.4920 35.894 2.4998 2.2 (-2 5 1) 17.947 0.2000 2.5135 37.112 2.4205 2.3 ( 2 4 1) 18.556 0.2066 2.5958 37.321 2.4074 0.9 ( 0 8 1) 18.661 0.2077 2.6099 37.809 2.3775 0.6 ( 2 6 0) 18.904 0.2103 2.6428 38.226 2.3525 0.2 (-2 3 2) 19.113 0.2125 2.6709 38.226 2.3525 0.2 ( 0 6 2) 19.113 0.2125 2.6709 38.751 2.3218 3.5 (-2 6 1) 19.375 0.2153 2.7061 39.028 2.3060 3.9 (-1 6 2) 19.514 0.2168 2.7247 39.028 2.3060 3.9 (-1 8 1) 19.514 0.2168 2.7247 39.923 2.2563 0.1 (-2 4 2) 19.962 0.2216 2.7847 40.699 2.2151 0.1 ( 1 8 1) 20.349 0.2257 2.8365 41.033 2.1978 0.2 ( 2 7 0) 20.516 0.2275 2.8588 41.440 2.1772 1.2 ( 0 9 1) 20.720 0.2297 2.8860 41.440 2.1772 1.2 ( 1 9 0) 20.720 0.2297 2.8860 41.627 2.1678 0.9 ( 3 1 0) 20.814 0.2306 2.8984 41.914 2.1536 4.1 (-2 7 1) 20.957 0.2322 2.9175 42.202 2.1396 1.3 (-1 7 2) 21.101 0.2337 2.9366 42.466 2.1269 5.1 (-1 1 3) 21.233 0.2351 2.9542 42.466 2.1269 5.1 ( 0 1 3) 21.233 0.2351 2.9542 42.830 2.1097 1.1 ( 2 1 2) 21.415 0.2370 2.9783 43.185 2.0931 6.3 ( 0 2 3) 21.592 0.2389 3.0018 43.185 2.0931 6.3 (-1 2 3) 21.592 0.2389 3.0018 43.560 2.0760 0.6 (-3 3 1) 21.780 0.2408 3.0266 44.300 2.0430 1.6 (-1 3 3) 22.150 0.2447 3.0755 44.300 2.0430 1.6 ( 0 3 3) 22.150 0.2447 3.0755 44.511 2.0338 0.8 ( 2 8 0) 22.256 0.2458 3.0894 44.607 2.0297 0.8 (-2 6 2) 22.303 0.2463 3.0957 44.877 2.0181 0.8 ( 0 8 2) 22.438 0.2478 3.1134 45.136 2.0071 0.9 (-3 4 1) 22.568 0.2491 3.1305 45.338 1.9986 0.3 ( 1 7 2) 22.669 0.2502 3.1437 45.338 1.9986 0.3 (-2 8 1) 22.669 0.2502 3.1437 45.868 1.9768 0.5 ( 0 10 1) 22.934 0.2529 3.1785 45.868 1.9768 0.5 ( 1 10 0) 22.934 0.2529 3.1785 46.324 1.9583 1.0 ( 3 1 1) 23.162 0.2553 3.2084 46.524 1.9504 0.7 (-3 1 2) 23.262 0.2564 3.2215 46.974 1.9328 3.4 ( 3 2 1) 23.487 0.2587 3.2509 47.320 1.9194 1.8 (-1 10 1) 23.660 0.2605 3.2735 47.607 1.9085 0.3 (-2 2 3) 23.804 0.2620 3.2922 48.211 1.8860 0.8 ( 2 9 0) 24.105 0.2651 3.3315 48.554 1.8735 0.4 ( 0 9 2) 24.277 0.2669 3.3538 48.665 1.8695 0.3 (-2 3 3) 24.332 0.2675 3.3609 48.665 1.8695 0.3 ( 1 3 3) 24.332 0.2675 3.3609 48.989 1.8579 0.3 (-2 9 1) 24.494 0.2691 3.3819 49.507 1.8396 0.5 ( 3 4 1) 24.753 0.2718 3.4155 49.697 1.8331 0.3 (-3 4 2) 24.848 0.2728 3.4277 50.117 1.8187 0.6 ( 1 4 3) 25.058 0.2749 3.4548 50.117 1.8187 0.6 (-2 4 3) 25.058 0.2749 3.4548 50.312 1.8121 0.6 ( 0 11 1) 25.156 0.2759 3.4674 50.417 1.8085 0.5 ( 2 6 2) 25.209 0.2765 3.4742 51.346 1.7780 0.4 ( 3 5 1) 25.673 0.2812 3.5339 51.530 1.7721 0.2 (-3 5 2) 25.765 0.2822 3.5457 51.670 1.7676 0.1 (-1 11 1) 25.835 0.2829 3.5546 52.006 1.7569 0.7 ( 3 7 0) 26.003 0.2846 3.5762 52.006 1.7569 0.7 (-3 7 1) 26.003 0.2846 3.5762 52.824 1.7317 0.8 (-2 10 1) 26.412 0.2887 3.6284 52.824 1.7317 0.8 ( 0 12 0) 26.412 0.2887 3.6284 53.022 1.7256 0.7 ( 1 11 1) 26.511 0.2897 3.6411 53.531 1.7105 0.2 ( 3 6 1) 26.765 0.2923 3.6734 54.107 1.6936 0.1 (-2 6 3) 27.054 0.2952 3.7100 54.794 1.6740 0.7 ( 1 12 0) 27.397 0.2987 3.7535 54.794 1.6740 0.7 ( 0 12 1) 27.397 0.2987 3.7535 55.005 1.6681 0.9 (-3 8 1) 27.502 0.2998 3.7668 55.485 1.6547 0.3 ( 2 10 1) 27.743 0.3022 3.7971 55.649 1.6502 0.1 ( 1 10 2) 27.825 0.3030 3.8074 55.649 1.6502 0.1 ( 0 8 3) 27.825 0.3030 3.8074 55.801 1.6461 0.1 ( 2 2 3) 27.900 0.3037 3.8169 55.801 1.6461 0.1 (-4 1 1) 27.900 0.3037 3.8169 56.152 1.6366 0.6 ( 2 11 0) 28.076 0.3055 3.8391 56.152 1.6366 0.6 (-1 12 1) 28.076 0.3055 3.8391 56.412 1.6297 0.5 ( 4 1 0) 28.206 0.3068 3.8554 56.412 1.6297 0.5 (-4 2 1) 28.206 0.3068 3.8554 56.596 1.6249 0.2 (-2 7 3) 28.298 0.3077 3.8669 56.596 1.6249 0.2 ( 1 7 3) 28.298 0.3077 3.8669 56.982 1.6148 0.5 (-1 1 4) 28.491 0.3096 3.8910 56.982 1.6148 0.5 (-2 11 1) 28.491 0.3096 3.8910 57.451 1.6027 0.4 ( 0 0 4) 28.725 0.3120 3.9204 57.911 1.5911 0.2 ( 4 3 0) 28.955 0.3143 3.9491 58.154 1.5850 0.6 ( 3 9 0) 29.077 0.3155 3.9642 58.472 1.5771 0.2 (-1 3 4) 29.236 0.3170 3.9839 58.634 1.5732 0.3 (-4 4 1) 29.317 0.3178 3.9940 58.839 1.5682 0.4 ( 3 8 1) 29.419 0.3188 4.0067 59.008 1.5641 0.2 (-3 8 2) 29.504 0.3197 4.0172 59.203 1.5594 0.4 ( 4 4 0) 29.602 0.3206 4.0293 59.556 1.5510 0.2 ( 0 13 1) 29.778 0.3224 4.0511 59.883 1.5433 0.1 (-2 0 4) 29.941 0.3240 4.0713 60.280 1.5341 0.4 (-4 5 1) 30.140 0.3259 4.0957 60.445 1.5303 0.3 ( 2 12 0) 30.222 0.3267 4.1059 60.608 1.5266 0.2 (-2 2 4) 30.304 0.3275 4.1159 60.839 1.5213 0.3 ( 4 1 1) 30.419 0.3287 4.1301 60.839 1.5213 0.3 ( 4 5 0) 30.419 0.3287 4.1301 61.114 1.5151 0.5 (-2 12 1) 30.557 0.3300 4.1470 61.383 1.5091 1.1 ( 4 2 1) 30.692 0.3313 4.1635 61.383 1.5091 1.1 (-1 5 4) 30.692 0.3313 4.1635 61.668 1.5028 0.2 (-3 10 1) 30.834 0.3327 4.1809 61.956 1.4965 0.4 (-3 9 2) 30.978 0.3341 4.1985 61.956 1.4965 0.4 ( 1 1 4) 30.978 0.3341 4.1985 62.445 1.4860 0.3 (-2 9 3) 31.223 0.3365 4.2283 62.445 1.4860 0.3 ( 1 9 3) 31.223 0.3365 4.2283 62.754 1.4794 0.4 ( 4 6 0) 31.377 0.3380 4.2471 62.754 1.4794 0.4 (-2 4 4) 31.377 0.3380 4.2471 63.374 1.4664 0.3 ( 1 3 4) 31.687 0.3410 4.2847 63.908 1.4555 0.1 ( 0 6 4) 31.954 0.3435 4.3170 63.908 1.4555 0.1 (-3 7 3) 31.954 0.3435 4.3170 64.337 1.4468 0.1 (-2 5 4) 32.169 0.3456 4.3429 64.337 1.4468 0.1 ( 0 14 1) 32.169 0.3456 4.3429 64.544 1.4426 0.1 (-4 7 1) 32.272 0.3466 4.3554 64.877 1.4360 0.1 ( 2 13 0) 32.439 0.3482 4.3754 65.101 1.4316 0.1 ( 4 5 1) 32.551 0.3493 4.3888 65.363 1.4265 0.2 (-3 11 1) 32.681 0.3505 4.4045 65.363 1.4265 0.2 (-2 12 2) 32.681 0.3505 4.4045 65.607 1.4218 0.2 (-1 13 2) 32.804 0.3517 4.4191 65.607 1.4218 0.2 (-1 7 4) 32.804 0.3517 4.4191 65.945 1.4153 0.1 ( 0 11 3) 32.972 0.3533 4.4393 65.945 1.4153 0.1 (-1 11 3) 32.972 0.3533 4.4393 66.244 1.4097 0.4 (-2 6 4) 33.122 0.3547 4.4572 66.716 1.4008 0.2 ( 1 14 1) 33.358 0.3569 4.4853 66.716 1.4008 0.2 ( 3 2 3) 33.358 0.3569 4.4853 66.996 1.3957 0.1 (-3 2 4) 33.498 0.3583 4.5019 66.996 1.3957 0.1 ( 4 6 1) 33.498 0.3583 4.5019 67.661 1.3836 0.2 ( 4 8 0) 33.830 0.3614 4.5413 67.661 1.3836 0.2 ( 3 3 3) 33.830 0.3614 4.5413 68.175 1.3744 0.3 (-1 8 4) 34.088 0.3638 4.5717 68.462 1.3693 0.1 (-2 7 4) 34.231 0.3651 4.5886 68.717 1.3649 0.1 ( 3 4 3) 34.359 0.3663 4.6036 68.717 1.3649 0.1 ( 4 1 2) 34.359 0.3663 4.6036 69.273 1.3553 1.0 ( 2 0 4) 34.636 0.3689 4.6362 69.273 1.3553 1.0 ( 1 15 0) 34.636 0.3689 4.6362 69.542 1.3507 0.5 ( 2 14 0) 34.771 0.3702 4.6519 69.542 1.3507 0.5 ( 2 1 4) 34.771 0.3702 4.6519 69.765 1.3469 0.1 (-1 12 3) 34.882 0.3712 4.6650 69.765 1.3469 0.1 ( 0 14 2) 34.882 0.3712 4.6650 70.046 1.3422 0.1 ( 2 2 4) 35.023 0.3725 4.6813 70.152 1.3404 0.1 (-4 5 3) 35.076 0.3730 4.6875 70.152 1.3404 0.1 ( 1 7 4) 35.076 0.3730 4.6875 70.271 1.3384 0.1 ( 3 5 3) 35.135 0.3736 4.6944 70.629 1.3325 0.2 (-3 5 4) 35.314 0.3752 4.7153 71.031 1.3260 0.2 (-1 9 4) 35.515 0.3771 4.7386 71.031 1.3260 0.2 (-2 8 4) 35.515 0.3771 4.7386 71.757 1.3143 0.1 ( 4 8 1) 35.878 0.3804 4.7806 71.757 1.3143 0.1 (-5 2 1) 35.878 0.3804 4.7806 72.043 1.3098 0.2 ( 2 4 4) 36.022 0.3817 4.7971 72.335 1.3052 0.4 ( 5 1 0) 36.168 0.3831 4.8139 72.455 1.3034 0.4 (-3 6 4) 36.227 0.3836 4.8207 72.985 1.2952 0.1 (-4 9 2) 36.492 0.3860 4.8511 73.162 1.2925 0.1 (-4 10 1) 36.581 0.3868 4.8613 73.162 1.2925 0.1 (-2 12 3) 36.581 0.3868 4.8613 73.393 1.2890 0.4 ( 3 13 0) 36.697 0.3879 4.8745 73.527 1.2870 0.4 ( 2 5 4) 36.763 0.3885 4.8821 73.671 1.2848 0.4 ( 4 10 0) 36.835 0.3892 4.8903 73.789 1.2831 0.3 (-2 9 4) 36.895 0.3897 4.8970 73.979 1.2802 0.2 (-1 13 3) 36.989 0.3906 4.9078 74.411 1.2739 0.2 ( 1 16 0) 37.206 0.3925 4.9324 74.798 1.2682 0.2 ( 5 4 0) 37.399 0.3942 4.9543 75.750 1.2546 0.1 ( 3 11 2) 37.875 0.3985 5.0079 75.999 1.2512 0.2 ( 2 11 3) 37.999 0.3996 5.0219 75.999 1.2512 0.2 (-3 11 3) 37.999 0.3996 5.0219 |
3樓2012-06-07 18:05:49
yanhj0
鐵桿木蟲 (知名作家)
- 應(yīng)助: 23 (小學(xué)生)
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dj8803172樓2012-06-07 18:01:49
yanhj0
鐵桿木蟲 (知名作家)
- 應(yīng)助: 23 (小學(xué)生)
- 金幣: 10746.3
- 散金: 7231
- 紅花: 35
- 帖子: 6420
- 在線: 1185.9小時
- 蟲號: 229
- 注冊: 2003-03-01
- 專業(yè): 無機納米化學(xué)
【答案】應(yīng)助回帖
★ ★ ★ ★ ★
dj880317: 金幣+5, ★有幫助, 感謝你的應(yīng)助。 2012-06-07 20:43:32
dj880317: 金幣+5, ★有幫助, 感謝你的應(yīng)助。 2012-06-07 20:43:32
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PDF#49-2204: QM=Indexed(I); d=Diffractometer; I=Film/Visual Polypropylene, syndiotatic ( C3 H6 )n Radiation=CuKa Lambda=1.5418 Filter=Ni Calibration= 2T=12.190-49.458 I/Ic(RIR)= Ref: DeRosa, C., Corradini, P. Macromolecules, v26 p5711 (1993) Orthorhombic - Powder Diffraction, Pcaa (54) Z= mp= CELL: 14.5 x 11.2 x 7.4 <90.0 x 90.0 x 90.0> P.S=oP0 (?) Density(c)=0.058 Density(m)=0.94A Mwt=42.08 Vol=1201.76 F(17)=1.9(0.089,101/0) Ref: Ibid. Strong Lines: 7.25/X 4.31/X 5.57/8 4.70/5 3.63/4 3.28/4 3.79/1 2.60/1 2.12/1 2.03/1 NOTE: Slow crystallization from the melt by heating to ~200 C under a press and cooled to room temperature at a rate of 1.5 C per minute produced the specimen (MW = 260,000). 2-Theta d(?) I(f) ( h k l) Theta 1/(2d) 2pi/d n^2 12.190 7.2546 100.0 ( 2 0 0) 6.095 0.0689 0.8661 15.887 5.5738 80.0 ( 0 2 0) 7.944 0.0897 1.1273 18.885 4.6953 50.0 ( 2 1 1) 9.442 0.1065 1.3382 20.583 4.3115 100.0 ( 1 2 1) 10.292 0.1160 1.4573 23.481 3.7856 10.0 ( 2 2 1) 11.740 0.1321 1.6598 24.480 3.6333 35.0 ( 0 0 2) 12.240 0.1376 1.7293 24.480 3.6333 35.0 ( 4 0 0) 12.240 0.1376 1.7293 27.178 3.2784 35.0 ( 3 2 1) 13.589 0.1525 1.9165 27.178 3.2784 35.0 ( 2 0 2) 13.589 0.1525 1.9165 28.876 3.0893 5.0 ( 0 2 2) 14.438 0.1618 2.0338 28.876 3.0893 5.0 ( 4 1 1) 14.438 0.1618 2.0338 29.476 3.0279 5.0 ( 1 2 2) 14.738 0.1651 2.0751 29.476 3.0279 5.0 ( 2 3 1) 14.738 0.1651 2.0751 31.474 2.8400 5.0 ( 3 1 2) 15.737 0.1761 2.2124 31.474 2.8400 5.0 ( 2 2 2) 15.737 0.1761 2.2124 34.471 2.5996 10.0 ( 4 3 0) 17.236 0.1923 2.4169 36.969 2.4295 5.0 ( 6 0 0) 18.485 0.2058 2.5862 36.969 2.4295 5.0 ( 5 2 1) 18.485 0.2058 2.5862 38.967 2.3094 5.0 ( 3 4 1) 19.484 0.2165 2.7207 38.967 2.3094 5.0 ( 3 3 2) 19.484 0.2165 2.7207 42.564 2.1222 10.0 ( 4 4 1) 21.282 0.2356 2.9607 42.564 2.1222 10.0 ( 1 5 1) 21.282 0.2356 2.9607 44.562 2.0316 10.0 ( 3 4 2) 22.281 0.2461 3.0927 44.562 2.0316 10.0 ( 6 3 0) 22.281 0.2461 3.0927 47.759 1.9028 10.0 ( 4 4 2) 23.880 0.2628 3.3021 47.759 1.9028 10.0 ( 6 2 2) 23.880 0.2628 3.3021 49.458 1.8413 10.0 ( 4 5 1) 24.729 0.2715 3.4123 49.458 1.8413 10.0 ( 1 4 3) 24.729 0.2715 3.4123 |
4樓2012-06-07 18:06:28
5樓2012-06-07 20:45:46
dididada8823
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