 |
 |
 |
 |
 |
 |
||
 |
 |
 |
 |
 |
| 4 | 1/1 | 返回列表 |
| 查看: 784 | 回復(fù): 3 | |||
水木清清木蟲 (著名寫手)
|
[交流]
晶體結(jié)構(gòu)解析的審稿意見回復(fù) 已有1人參與
|
|
關(guān)于晶體結(jié)構(gòu)解析的審稿意見，需要怎么樣回答才好？沒有投稿經(jīng)驗(yàn)望大家多多指點(diǎn)！ [Cu(L)(DMF)砠H~2~O]~n~ (1) -------------------------- 1.1 Routine geometry checks show that the coordinates presented in the CIF do not form fully connected ligand sets. Thus O1 must be moved so that it is directly bonded to C7 and O3 must be moved so that it is directly bonded to C8. The refinement should then be redone, the CIF remade and the text refreshed. 1.2 We should be explicitly told in the descriptive text that the asymmetric unit has two half L ligands, each with the central N-H moiety on a twofold axis, 1.3 We are told in the text that SQUEEZE was used to remove the contributions of disordered solvent; the authors have included the CIF format output from PLATON (generated as platon.sqf) at the end of the CIF. The contribution of any disordered solvent removed by the SQUEEZE process should now be included in the overall formula, formula weight, density, F(000), etc., calculations reported in Table S1 and in the CIF. This should now be done with appropriate explanations in the _platon_squeeze_details section of the CIF. 1.4 In the CIF the O5 atom is wrongly flagged as "riding". Corrections are needed. 1.5 We see from the CIF that 30 Uiso/Uij restrained atom sites, 9 distance or angle restraints and 259 least-squares restraints were used in the refinement. We should be told - at least in the "_refine_special_details" section of the CIF or in an ESI text - exactly what these restraints were and why they were necessary. [An easy way to show what restraints were employed (but not why they were needed) is to include the relevant lines from the SHELXL.ins file in the "_refine_special_details" section of the CIF.] [Cu~2~(L)~2~(H~2~O)~2~xH~2~O]~n~ (2) ------------------------------------ 2.1 We should be told in the descriptive text about the crystallographically-imposed twofold symmetry in this structure. 2.2 As with compound 1, we are told in the text that SQUEEZE was used to remove the contributions of disordered solvent; the authors have included the CIF format output from PLATON (generated as platon.sqf) at the end of the CIF. The contribution of any disordered solvent removed by the SQUEEZE process should now be included in the overall formula, formula weight, density, F(000), etc., calculations reported in Table S1 and in the CIF. This should now be done with appropriate explanations in the _platon_squeeze_details section of the CIF. [Cu(L)(H~2~O)H~2~O]~n~ (3) -------------------------- 3.1 Routine geometry checks show that the coordinates presented in the CIF do not form fully connected ligand sets. Thus C14-O4 must be moved so that C14 is directly bonded to C11, and O1 must be moved so that it is directly bonded to repositioned C14. The refinement should then be redone, the CIF remade and the text refreshed. 3.2 We see from the CIF that 21 Uiso/Uij restrained atom sites, 4 distance or angle restraints and 162 least-squares restraints were used in the refinement. We should be told - at least in the "_refine_special_details" section of the CIF or in an ESI text - exactly what these restraints were and why they were necessary. [An easy way to show what restraints were employed (but not why they were needed) is to include the relevant lines from the SHELXL.ins file in the "_refine_special_details" section of the CIF.] Text ---- T1. In the descriptive text, it would be more informative if all dimensions were reported with their correct s.u. values. |
回復(fù)此樓» 猜你喜歡
求助
已經(jīng)有1人回復(fù)
-
0703化學(xué)26考研調(diào)劑，一志愿南昌大學(xué)
已經(jīng)有2人回復(fù)
-
無機(jī)化學(xué)論文潤(rùn)色/翻譯怎么收費(fèi)?
已經(jīng)有140人回復(fù)
-
有沒有化學(xué)、材料專業(yè)的同學(xué)需要調(diào)劑 考慮天津高效的可以郵件或者私信
已經(jīng)有1人回復(fù)
-
26年博士招生
已經(jīng)有16人回復(fù)
-
江西理工大學(xué)功能晶態(tài)材料方向劉遂軍課題組招收2026年秋季入學(xué)博士研究生
已經(jīng)有11人回復(fù)
-
寧夏大學(xué)團(tuán)簇新材料團(tuán)隊(duì)招收材料/化學(xué)/化工專業(yè)博士生
已經(jīng)有0人回復(fù)
-
MIL-101有單晶樣品嗎
已經(jīng)有1人回復(fù)
-
已刪除
已經(jīng)有3人回復(fù)
-
收調(diào)劑研究生
已經(jīng)有2人回復(fù)
-
【2026 考研調(diào)劑】哈爾濱工程大學(xué)核科學(xué)與技術(shù)學(xué)院核化工系 招收調(diào)劑生
已經(jīng)有2人回復(fù)
» 本主題相關(guān)價(jià)值貼推薦，對(duì)您同樣有幫助:
- 請(qǐng)幫忙看看這個(gè)審稿意見
已經(jīng)有4人回復(fù)
- 改進(jìn)控制算法文章，審稿人犀利的意見怎么回復(fù)，求大神幫助
已經(jīng)有4人回復(fù)
- 審稿意見里晶體學(xué)數(shù)據(jù)問題
已經(jīng)有3人回復(fù)
- 請(qǐng)大家?guī)臀曳治鱿聦徃逡庖?/a>
已經(jīng)有18人回復(fù)
- 電子與信息學(xué)報(bào)審稿意見空白
已經(jīng)有3人回復(fù)
- Science China E, 審稿意見返回了，請(qǐng)大家給點(diǎn)意見
已經(jīng)有18人回復(fù)
- 審稿意見怎么回答��？請(qǐng)教給位牛人~
已經(jīng)有6人回復(fù)
- 如何回復(fù)審稿人意見
已經(jīng)有17人回復(fù)
- 關(guān)于晶體的審稿人意見什么意思，急求，謝了
已經(jīng)有6人回復(fù)
- 如何回復(fù)要求精修的審稿意見？
已經(jīng)有12人回復(fù)
- 如何回復(fù)審稿人意見
已經(jīng)有7人回復(fù)
- 我該怎么回復(fù)審稿人的意見
已經(jīng)有3人回復(fù)
- 關(guān)于審稿意見中看不懂的一個(gè)問題
已經(jīng)有14人回復(fù)
- 有關(guān)晶體常數(shù)的審稿意見。
已經(jīng)有5人回復(fù)
- 審稿人意見，實(shí)在不知道怎么回答怎么辦
已經(jīng)有14人回復(fù)
- 專家審稿意見，請(qǐng)大家?guī)兔Ψ治觯?/a>
已經(jīng)有5人回復(fù)
- 論文審稿意見回來了，大家看看如何回復(fù)啊
已經(jīng)有16人回復(fù)
- Revision Needs Approval 要等多久啊是不是和第一次審稿一樣還有外審一樣久啊
已經(jīng)有9人回復(fù)
- 審稿意見怎么回復(fù)
已經(jīng)有3人回復(fù)
- 很有趣：當(dāng)Reviewer變成文章的合作者時(shí)，如何回復(fù)他的審稿意見？請(qǐng)高人指點(diǎn)，謝謝！
已經(jīng)有35人回復(fù)
- 誰見過這樣的審稿意見？
已經(jīng)有34人回復(fù)
- 審稿意見回復(fù)請(qǐng)教
已經(jīng)有4人回復(fù)
- SCI文章審稿人意見回來，卻不知如何答復(fù)，請(qǐng)各位前輩指點(diǎn)
已經(jīng)有7人回復(fù)
- CryEngComm小修，大家都是多久回復(fù)的。（附有審稿意見）
已經(jīng)有16人回復(fù)
xi2004
至尊木蟲 (職業(yè)作家)
- CMEI: 10
- 應(yīng)助: 125 (高中生)
- 金幣: 16769.9
- 散金: 12393
- 紅花: 221
- 帖子: 4161
- 在線: 436.9小時(shí)
- 蟲號(hào): 354550
- 注冊(cè): 2007-04-24
- 專業(yè): 結(jié)構(gòu)化學(xué)
2樓2012-08-13 09:59:54
水木清清
木蟲 (著名寫手)
- 應(yīng)助: 0 (幼兒園)
- 金幣: 5304.9
- 帖子: 1709
- 在線: 180.1小時(shí)
- 蟲號(hào): 371373
- 注冊(cè): 2007-05-14
- 性別: MM
- 專業(yè): 無機(jī)材料化學(xué)
|
謝謝！ 其他的問題還好處理一些，下面這個(gè)要怎么回答呢？需要自己計(jì)算formula weight, density, F(000), etc " 嗎~~~~~ “The contribution of any disordered solvent removed by the SQUEEZE process should now be included in the overall formula, formula weight, density, F(000), etc., calculations reported in Table S1 and in the CIF. This should now be done with appropriate explanations in the _platon_squeeze_details section of the CIF. " |
3樓2012-08-14 12:05:45
xi2004
至尊木蟲 (職業(yè)作家)
- CMEI: 10
- 應(yīng)助: 125 (高中生)
- 金幣: 16769.9
- 散金: 12393
- 紅花: 221
- 帖子: 4161
- 在線: 436.9小時(shí)
- 蟲號(hào): 354550
- 注冊(cè): 2007-04-24
- 專業(yè): 結(jié)構(gòu)化學(xué)
4樓2012-08-14 13:23:25
相關(guān)版塊跳轉(zhuǎn)
我要訂閱樓主 水木清清 的主題更新
| 4 | 1/1 | 返回列表 |
| 最具人氣熱帖推薦 [查看全部] | 作者 | 回/看 | 最后發(fā)表 | |
|---|---|---|---|---|
|
[考研] 【考研調(diào)劑】化學(xué)專業(yè) 281分，一志愿四川大學(xué)，誠心求調(diào)劑 +14 | 吃吃吃才有意義 2026-03-19 | 15/750 |
|
|---|---|---|---|---|
|
|
[考研] 一志愿華東理工大學(xué)081700，初試分?jǐn)?shù)271 +5 | kotoko_ik 2026-03-23 | 6/300 |
|
|
[考研] 材料專業(yè)求調(diào)劑 +11 | hanamiko 2026-03-18 | 11/550 |
|
|
|
[考研] 335分 | 材料與化工專碩 | GPA 4.07 | 有科研經(jīng)歷 +4 | cccchenso 2026-03-23 | 4/200 |
|
|
|
[考研] 327求調(diào)劑 +5 | prayer13 2026-03-23 | 5/250 |
|
|
|
[考研] 工科0856求調(diào)劑 +5 | 沐析汀汀 2026-03-21 | 5/250 |
|
|
|
[考研] 接收2026碩士調(diào)劑(學(xué)碩+專碩) +4 | allen-yin 2026-03-23 | 6/300 |
|
|
|
[考研]
 一志愿070300浙大化學(xué)358分，求調(diào)劑！
+4
|
酥酥魚.. 2026-03-21 | 4/200 |
|
|
|
[考研] 319求調(diào)劑 +4 | 小力氣珂珂 2026-03-20 | 4/200 |
|
|
|
[考研] 一志愿北京化工大學(xué)070300 學(xué)碩336求調(diào)劑 +5 | vv迷 2026-03-21 | 8/400 |
|
|
|
[考研] 354求調(diào)劑 +7 | Tyoumou 2026-03-18 | 10/500 |
|
|
|
[考研] 302求調(diào)劑 +12 | 呼呼呼。。。。 2026-03-17 | 12/600 |
|
|
|
[考研] 274求調(diào)劑 +10 | S.H1 2026-03-18 | 10/500 |
|
|
|
[考研] 南京大學(xué)化學(xué)376求調(diào)劑 +3 | hisfailed 2026-03-19 | 6/300 |
|
|
|
[考研] 317求調(diào)劑 +5 | 申子申申 2026-03-19 | 9/450 |
|
|
|
[考研] 一志愿西南交通 專碩 材料355 本科雙非 求調(diào)劑 +5 | 西南交通專材355 2026-03-19 | 5/250 |
|
|
|
[考研] 0817 化學(xué)工程 299分求調(diào)劑 有科研經(jīng)歷 有二區(qū)文章 +22 | rare12345 2026-03-18 | 22/1100 |
|
|
|
[考研] 求調(diào)劑 +3 | @taotao 2026-03-20 | 3/150 |
|
|
|
[考研] 086500 325 求調(diào)劑 +3 | 領(lǐng)帶小熊 2026-03-19 | 3/150 |
|
|
|
[考研] 材料考研調(diào)劑 +3 | xwt。 2026-03-19 | 3/150 |
|