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sushq07金蟲 (小有名氣)
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[求助]
質(zhì)子化水的拉曼光譜求助
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請(qǐng)教大家賜教, 我一個(gè)多孔配位聚合物孔道里有質(zhì)子化的水,我想用激光拉曼光譜進(jìn)行驗(yàn)證,不知道可不可行,如果可以,需要多少樣品以及樣品是否需要處理,謝謝 |
金蟲 (小有名氣)
銀蟲 (初入文壇)
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Find something here, hope it'll be helpful. http://www.lsbu.ac.uk/water/methods.html As far as i know, water (or protonated water) is a very weak Raman scatterer. So if you want to prove its existence in porous polymer, why not try IR instead of Raman? (Sorry that I don't have chinese input on my laptop.) |

銀蟲 (初入文壇)
| Forgot one point here, Raman measurement generally doesn't require very complicated sample preparation. 'cuz one of its major advantages is its simple sample preparation process and versatility. Hope this could facilitate addressing your problem a little. |

銀蟲 (初入文壇)
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http://pubs.acs.org/doi/abs/10.1021/ja907023c Crystal Structures and Properties of Large Protonated Water Clusters Encapsulated by Metal−Organic Frameworks One similar study you might find interesting. |

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