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kardinalxing木蟲 (正式寫手)
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幫忙查下微譜數(shù)據(jù)，金幣好商量！
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幫忙查一下： 化合物1 13.98, 22.48，24.60, 25.07, 27.99, 28.83, 28.99, 29.29, 29.71, 31.48, 33.22, 33.45, 69.87, 73.91, 75.62, 127.87,13 6.72, 145.29, 159.80 溶劑為氘氯仿 溶劑峰分別為76.58， 77.00， 77.43， 78.04 希望高手幫忙查下 謝謝！ |
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1 . Embeliaribyl ester C44H86O3 相似度:73.6% Pharmazie 2005 60 69-71 New compounds from the seeds of Embelia ribes Burm K. Haq, M. Ali, and A. W. Siddiqui Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 2 . compound 9 相似度:73.6% Australian Journal of Chemistry 1991 44 843-854 Epoxy Lipids From the Australian Epiphytic Brown Alga Notheia anomala. II. LM Murray, RA Barrow and RJ Capon Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 3 . (±)-coriolic acid 相似度:73.6% Shoyakugaku Zasshi 1987 41 174-179 Studies on the Crude Drug Containing the Angiotensin I Converting Enzyme Inhibitors (II) : On the Active Principles of Fritillaria verticillata WILLDENOW var. thumber gii BAKER NIITSU KAZUAKI,Tsumura Laboratory, IKEYA YUKINOBU,Tsumura Laboratory, et al. Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 4 . α-palmitoyl-β-linoleoyl-α'-linoleoyl glycerol 相似度:70% Fitoterapia 2006 77 296-299 Triglycerides from Urena lobata Carlo F. Morelli, Paola Cairoli , Giovanna Speranza , Mahiuddin Alamgir ,Sultana Rajia Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 5 . compound 3 C18H30O3 相似度:68.4% Journal of Natural Products 2002 65 1712-1714 Aldehyde Dehydrogenase Inhibitors from the Mushroom Clitocybe clavipes Hirokazu Kawagishi, Toshiyuki Miyazawa,Hiroko Kume,Yasushi Arimoto, and Takahiro Inakuma Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 6 . (9R,10E,12S,13S)-9,12,13-Trihydroxyoctadec-10-enoic Acid 相似度:68.4% Helvetica Chimica Acta 2009 92 2052-2057 Synthesis of (-)-Pinellic Acid and Its (9R,12S,13S)-Diastereoisomer Gowravaram Sabitha, Martha Bhikshapathi, Erigala Venkata Reddy, Jhillu S. Yadav Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 7 . 9,10-Dihydroxystearic acid 相似度:68.4% Steroids 2008 73 1098-1109 Synthesis of highly pure oxyphytosterols and (oxy)phytosterol esters: Part II. (Oxy)-sitosterol esters derived from oleic acid and from 9,10-dihydroxystearic acid [1] Diane Julien-David, Philippe Geoffroy, Eric Marchioni, Françis Raul, Dalal Aoudé-Werner, Michel Miesch Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 8 . compound 8a 相似度:68.4% Tetrahedron Letters 2005 46 2487-2490 Allylic oxidation: easy synthesis of alkenones from activated alkenes with TEMPO Tony Breton, Denis Liaigre, El Mustapha Belgsir Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 9 . compound 8b 相似度:68.4% Tetrahedron Letters 2005 46 2487-2490 Allylic oxidation: easy synthesis of alkenones from activated alkenes with TEMPO Tony Breton, Denis Liaigre, El Mustapha Belgsir Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 10 . compound 8c 相似度:68.4% Tetrahedron Letters 2005 46 2487-2490 Allylic oxidation: easy synthesis of alkenones from activated alkenes with TEMPO Tony Breton, Denis Liaigre, El Mustapha Belgsir Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 11 . (9Z,11E)-13-oxo-9,11-ocatadecadienoic acid C18H30O3 相似度:68.4% Bioscience, Biotechnology, and Biochemistry 2000 64 882-886 (10E,12Z,15Z)-9-Hydroxy-10,12,15-octadecatrienoic Acid Methyl Ester as an Anti-inflammatory Compound from Ehretia dicksonii Mei DONG, Yukiko ODA, Mitsuru HIROTA Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 12 . 9,12-octadecadienoic acid (Z,Z)-2,3-dihydroxypropyl ester C21H38O4 相似度:68.4% Natural Product Research and Development 2010 22 998-1000 Chemical Constituents and Identification of the Caules of Clematis armandii Franch. and Clematis montana Buch.-Ham. LIU Jing-jing;CHEN Xing; WEI Zhi-qi; LI Bin Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 13 . (-)-(13S,9Z,11E)-13-hydroxy-9,11-ocatadecadienoic acid methyl ester 相似度:68.4% Tetrahedron 1997 53 617-624 The chemoenzymatic synthesis of(S)-13-hydroxyoctadeca-(9Z, 11E)-dienoic acid using the hydroxynitrile lyase from Hevea brasiliensis Dean V. Johnson, Herfried Griengl Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 14 . (6S,7R,9R,10R)-6,9-epoxynonadec-18-ene-7,10-diol C19H36O3 相似度:68.4% Tetrahedron 1998 54 2227-2242 Marine nematocides: Tetrahydrofurans from a southern Australian brown alga, Notheia anomala Robert J. Capon, Russell A Barrow, Simone Rochfort, Michael Jobling, Colin Skene, Ernest Lacey, Jennifer H Gill, Thomas Friedel, David Wadsworth Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 15 . methyl (9S,10S,12S,13S)-10,13-epoxy-9,12-dihydroxyoctadecanonate 相似度:68.4% Tetrahedron 1998 54 2227-2242 Marine nematocides: Tetrahydrofurans from a southern Australian brown alga, Notheia anomala Robert J. Capon, Russell A Barrow, Simone Rochfort, Michael Jobling, Colin Skene, Ernest Lacey, Jennifer H Gill, Thomas Friedel, David Wadsworth Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 16 . (6S,7S,9R,10R)-6,9-epoxynonadec-18-ene-7,10-diol 相似度:68.4% Australian Journal of Chemistry 1990 43 895-911 Epoxy Lipids From the Australian Epiphytic Brown Alga Notheia anomala RA Barrow and RJ Capon Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 17 . (9E,11Z) 14-Hydroxyoctadecan-9,11-dienoic acid C18H32O3 相似度:68.4% Natural Product Communications 2006 1 101-107 Constituents of Erythrina lysistemon: Their Brine ShrimpLethality, Antimicrobial and Radical Scavenging Activities Benard F. Juma and Runner R. T. Majinda Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 18 . (9S,10E,12Z)-9-Hydroxy-10,12-octadecadienoic Acid C18H32O3 相似度:68.4% Journal of Agricultural and Food Chemistry 2008 56 5062-5068 Isolation and Identification of Antifungal Fatty Acids from the Basidiomycete Gomphus floccosus Charles L. Cantrell, Bethany P. Case, E. Edward Mena, Toby M. Kniffin, Stephen O. Duke and David E. Wedge Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 19 . (9E,11Z)-13-Oxo-9,11-octadecadienoic Acid C18H30O3 相似度:68.4% Journal of Agricultural and Food Chemistry 2008 56 5062-5068 Isolation and Identification of Antifungal Fatty Acids from the Basidiomycete Gomphus floccosus Charles L. Cantrell, Bethany P. Case, E. Edward Mena, Toby M. Kniffin, Stephen O. Duke and David E. Wedge Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 20 . Nonanoate C19H34O3 相似度:68.4% Journal of Agricultural and Food Chemistry 2002 50 3522-3526 Antimicrobial and Bactericidal Activities of Esters of 2-endo-Hydroxy-1,8-cineole as New Aroma Chemicals Mitsuo Miyazawa and Yuya Hashimoto |
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kardinalxing2樓2013-01-16 17:50:51
新新手
木蟲 (小有名氣)
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★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★
kardinalxing: 金幣+30, ★★★很有幫助, 謝謝 2013-01-16 18:17:45
kardinalxing: 金幣+30, ★★★很有幫助, 謝謝 2013-01-16 18:17:45
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帶溶劑峰，查得 1 . (3S,8R,9R,10R)-3-(tert-Butyldimethylsilyloxy)heptadeca-1-en-4,6-diyne-8,9,10-triol C23H40O4Si 相似度:65.2% Tetrahedron 2012 68 262-271 A flexible organocatalytic enantioselective synthesis of heptadeca-1-ene-4,6-diyne-3S,8R,9S,10S-tetrol and its congeners Gullapalli Kumaraswamy, Kadivendi Sadaiah Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 2 . 4,6-Tricosadiynoic acid 相似度:65.2% Journal of the Brazilian Chemical Society 2001 12 64-72 Synthesis of the Diacetylenic Phospholipids 1,2-(10',12'-Heptadecadiynoyl)-sn-Glycero-3-Phophatidylcholine and 1,2-(4',6'-Tricosadiynoyl)-sn-Glycero-3-Phophatidylcholine Paulo T. Hennies, Maria H. C. Santana and Carlos R. D. Correia Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 3 . Di-O-alkadienyl ethers C86H162O4 相似度:62.9% Phytochemistry 1995 40 543-554 n-alkenylpyrogallol dimethyl ethers, aliphatic diol monoesters and some minor ether lipids from Botryococcus braunii a race P. Metzger, Y. Pouet Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 4 . 1,2-(10',12'-Tricosadiynoyl)-sn-glycero-3-phophatidylcholine C54H92NO8P 相似度:62.9% Journal of the Brazilian Chemical Society 2001 12 64-72 Synthesis of the Diacetylenic Phospholipids 1,2-(10',12'-Heptadecadiynoyl)-sn-Glycero-3-Phophatidylcholine and 1,2-(4',6'-Tricosadiynoyl)-sn-Glycero-3-Phophatidylcholine Paulo T. Hennies, Maria H. C. Santana and Carlos R. D. Correia Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 5 . digonazole C34H58N2O7 相似度:62.5% Journal of Natural Products 1994 Vol 57 829 Amino Acid Derivatives from the Marine Sponge Jaspis digonoxea Amira Rudi, Yoel Kashman, Yehuda Benayahu, Michael Schleyer Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 6 . (9E)-(11S,12R,15R,16R)-19-benzyloxy-11-(methoxymethoxy)-12,15-oxido-9-nonadecen-16-ol C28H46O5 相似度:62.5% The Journal of Organic Chemistry 1998 63 7066-7071 Total Synthesis of the Nonadjacent Bis-Tetrahydrofuran Annonaceous Acetogenin Squamostatin-D James A. Marshall and Hongjian Jiang Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 7 . compound 4 C21H36O5 相似度:60.8% Journal of Natural Products 2002 65 1712-1714 Aldehyde Dehydrogenase Inhibitors from the Mushroom Clitocybe clavipes Hirokazu Kawagishi, Toshiyuki Miyazawa,Hiroko Kume,Yasushi Arimoto, and Takahiro Inakuma Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 8 . compound 15 相似度:60.8% Journal of Natural Products 1997 60 1251-1260 New Acylated Sulfoglycolipids and Digalactolipids and Related Known Glycolipids from Cyanobacteria with a Potential To Inhibit the Reverse Transcriptase of HIV-1 Vered Reshef, Erez Mizrachi, Tal Maretzki, Colin Silberstein, Shoshana Loya, Amnon Hizi, and Shmuel Carmeli Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 9 . 9,10-Di-tert-butyldimethylsilyloxystearic acid C30H64O4Si2 相似度:60.8% Steroids 2008 73 1098-1109 Synthesis of highly pure oxyphytosterols and (oxy)phytosterol esters: Part II. (Oxy)-sitosterol esters derived from oleic acid and from 9,10-dihydroxystearic acid [1] Diane Julien-David, Philippe Geoffroy, Eric Marchioni, Françis Raul, Dalal Aoudé-Werner, Michel Miesch Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 10 . α-palmitoyl-β-linoleoyl-α'-linoleoyl glycerol 相似度:60.8% Fitoterapia 2006 77 296-299 Triglycerides from Urena lobata Carlo F. Morelli, Paola Cairoli , Giovanna Speranza , Mahiuddin Alamgir ,Sultana Rajia Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 11 . (12Z)-4-phenyl-1-(9-hydroxy-octadec-12-enoyl)-thiosemicarbazide C25H41N3O2S 相似度:60.8% Indian Journal of Chemistry 2009 48B 97-102 Substituted 1,2,4-triazoles and thiazolidinones from fatty acids: Spectral characterization and antimicrobial activity Banday,Mudasir Rashid; Rauf,Abdul Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 12 . Compound 4 C35H67NO5 相似度:60.8% Bioorganic & Medicinal Chemistry Letters 2007 17 3426-3430 Annonaceous acetogenin mimics bearing a terminal lactam and their cytotoxicity against cancer cells Hai-Xia Liu, Guo-Rui Huang, Huan-Ming Zhang, Jia-Rui Wu, Zhu-Jun Yao Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 13 . phenylacetylricinoleic acid 相似度:60.8% Bioorganic & Medicinal Chemistry Letters 2010 20 3231-3234 Chemoenzymatic synthesis and cannabinoid activity of a new diazabicyclic amide of phenylacetylricinoleic acid Manuel López-Ortíz, Andrea Herrera-Solís, Axel Luviano-Jardón, Nidia Reyes-Prieto, Ivan Castillo, Ivan Monsalvo, Patricia Demare, Mónica Méndez-Díaz, Ignacio Regla, Oscar Prospéro-García Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 14 . Embeliaribyl ester C44H86O3 相似度:60.8% Pharmazie 2005 60 69-71 New compounds from the seeds of Embelia ribes Burm K. Haq, M. Ali, and A. W. Siddiqui Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 15 . compound 7a C25H44O4 相似度:60.8% Tetrahedron Letters 2003 44 1035-1037 Enantioselective synthesis of d-ribo-(2S,3S,4R)-C18-phytosphingosine using double stereodifferentiation S.Vasudeva Naidu, Pradeep Kumar Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 16 . AA005-d 4 C33H58D4O6 相似度:60.8% Tetrahedron Letters 2005 46 3525-3528 Synthesis of a tetra-deuterium-labeled derivative of potent and selective anticancer agent AA005 Hai-Xia Liu, Zhu-Jun Yao Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 17 . (1R,6R)-6-(tert-Butyldimethylsilyloxy)-1-((4R,5S)-5-heptyl-2,2-dimethyl-1,3-dioxolan-4-yl)octa-7-en-2,4-diyn-1-ol C26H44O4Si 相似度:60.8% Tetrahedron 2012 68 262-271 A flexible organocatalytic enantioselective synthesis of heptadeca-1-ene-4,6-diyne-3S,8R,9S,10S-tetrol and its congeners Gullapalli Kumaraswamy, Kadivendi Sadaiah Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 18 . methyl (9S,10S,12S,13S)-10,13-epoxy-9,12-dihydroxyoctadecanonate 相似度:60.8% Tetrahedron 1998 54 2227-2242 Marine nematocides: Tetrahydrofurans from a southern Australian brown alga, Notheia anomala Robert J. Capon, Russell A Barrow, Simone Rochfort, Michael Jobling, Colin Skene, Ernest Lacey, Jennifer H Gill, Thomas Friedel, David Wadsworth Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 19 . (2S,3S,4R,2'S,3'S)-2-(2',3'-O-isopropylideneicosanoylamino)-1,3,4-docosanetriol C49H89NO6 相似度:60.8% Journal of Medicinal Chemistry 2006 49 5830-5839 Isolation, Structure Elucidation, Total Synthesis, and Evaluation of New Natural and Synthetic Ceramides on Human SK-MEL-1 Melanoma Cells Francisco León, Ignacio Brouard, Augusto Rivera, Fernando Torres, Sara Rubio, José Quintana, Francisco Estévez, and Jaime Bermejo Structure 13C NMR 碳譜模擬圖 -------------------------------------------------------------------------------- 20 . (6S,7S,9R,10R)-6,9-epoxynonadec-18-ene-7,10-diol 10-acetate C21H38O4 相似度:60.8% Australian Journal of Chemistry 1990 43 895-911 Epoxy Lipids From the Australian Epiphytic Brown Alga Notheia anomala RA Barrow and RJ Capon |
3樓2013-01-16 17:53:50
kardinalxing
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4樓2013-01-16 18:18:09
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