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yuanchunma金蟲 (正式寫手)
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[求助]
求一個生物堿化合物微譜數(shù)據(jù)
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| 碳譜數(shù)據(jù)如下： 157.6, 149.3, 148.6, 130.1, 125.2, 123.6, 123.4, 122.9, 122.6, 119.7, 115, 104.5, 103.4, 103.2, 77.1, 69.8, 67.9, 63.9, 55.8 (OMe), 55.8(OMe), 55.3(OMe), 31.9, 29.6, 29.3, 27, 22.6, 19.6, 14.1 |
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木蟲 (正式寫手)
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【答案】應(yīng)助回帖
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感謝參與，應(yīng)助指數(shù) +1
yuanchunma: 金幣+20, ★★★★★最佳答案 2013-01-30 13:33:39
感謝參與，應(yīng)助指數(shù) +1
yuanchunma: 金幣+20, ★★★★★最佳答案 2013-01-30 13:33:39
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查詢結(jié)果：共查到47個化合物(查詢結(jié)果僅供參考) 1 . boehmeriasin A C24H27NO3 相似度:71.4% Planta Medica 2003 69 842-845 Cytotoxic Alkaloids from Boehmeria siamensis Yinggang Luo,Yan Liu,Dixiang Luo, Xiaoping Gao,Bogang Li,Guolin Zhang Structure 13C NMR 碳譜模擬圖 2 . tylophoridicine F C23H25NO5 相似度:64.2% Planta Medica 2004 70 441-445 Cytotoxic Alkaloids from the Roots of Tylophora atrofolliculata Xueshi Huang,Song Gao,Lihua Fan Shishan Yu,Xiaotian Liang Structure 13C NMR 碳譜模擬圖 3 . (-)-(R)-13aα-antofine 相似度:60.7% Journal of Natural Products 2002 65 1299-1302 In Vitro Cytotoxic Activity of Phenanthroindolizidine Alkaloids from Cynanchum vincetoxicum and Tylophora tanakae against Drug-Sensitive and Multidrug-Resistant Cancer Cells Dan Stærk, Anne K. Lykkeberg, Jette Christensen, Bogdan A. Budnik,Fumiko Abe, and Jerzy W. Jaroszewski Structure 13C NMR 碳譜模擬圖 4 . antofine 相似度:60.7% Planta Medica 2003 69 21-25 Cytotoxic Activity and G2/M Cell Cycle Arrest Mediated by Antofine,A Phenanthroindolizidine Alkaloid Isolated from Cynanchum paniculatum Sang Kook Lee,Kyung-Ae Nam,Yoen-Hoi Heo Structure 13C NMR 碳譜模擬圖 5 . antofine 相似度:60.7% Chinese Journal of Natural Medicines 2006 4 352-354 Antitumor Constituents from the Roots of Tylophora floribunda WANG Hong-Gang; MA Yuan-Gang; YU Bo-Yang; YUAN Sheng-Tao Structure 13C NMR 碳譜模擬圖 6 . (S)-1-[(9-bromo-2,3,6-trimethoxyphenanthren-10-yl)methyl]-N,N-diethylpyrrolidine-2-carboxamide C27H33BrN2O4 相似度:60.7% European Journal of Organic Chemistry 2010 292-299 Efficient and Chirally Specific Synthesis of Phenanthro-Indolizidine Alkaloids by Parham-Type Cycloacylation Ziwen Wang, Zheng Li, Kailiang Wang and Qingmin Wang Structure 13C NMR 碳譜模擬圖 7 . (+)-antofine C23H25NO3 相似度:60.7% European Journal of Organic Chemistry 2010 292-299 Efficient and Chirally Specific Synthesis of Phenanthro-Indolizidine Alkaloids by Parham-Type Cycloacylation Ziwen Wang, Zheng Li, Kailiang Wang and Qingmin Wang Structure 13C NMR 碳譜模擬圖 8 . antofine 相似度:57.1% Phytochemistry 1990 29 3327-3330 An antimicrobial alkaloid from Ficus septica Beat Baumgartner,Clemens A.J. Erdelmeier,Anthony D. Wright,Topul Rali,Otto Sticher Structure 13C NMR 碳譜模擬圖 9 . 7-demethoxyty-lophorine C24H27O3N 相似度:57.1% Natural Product Research and Development 2002 14(2) 1-5 THE CHEMICAL CONSTITUENTS OF COLEUS FORSKOHLII YAO Chun-suo SHEN Yun-heng XU Yun-long Structure 13C NMR 碳譜模擬圖 10 . antofine C23H25NO3 相似度:57.1% Bioorganic & Medicinal Chemistry 2008 16 6233-6241 Total synthesis of phenanthroindolizidine alkaloids (±)-antofine, (±)-deoxypergularinine, and their dehydro congeners and evaluation of their cytotoxic activity Chung-Ren Su, Amooru G. Damu, Po-Cheng Chiang, Kenneth F. Bastow, Susan L. Morris-Natschke, Kuo-Hsiung Lee, Tian-Shung Wu Structure 13C NMR 碳譜模擬圖 11 . (S)-1-[(10-bromo-2,3,6-trimethoxyphenanthren-9-yl)methyl]-N,N-diethylpyrrolidine-2-carboxamide C27H33BrN2O4 相似度:57.1% European Journal of Organic Chemistry 2010 292-299 Efficient and Chirally Specific Synthesis of Phenanthro-Indolizidine Alkaloids by Parham-Type Cycloacylation Ziwen Wang, Zheng Li, Kailiang Wang and Qingmin Wang Structure 13C NMR 碳譜模擬圖 12 . (13aS,14S)-tylophorinine C23H25NO4 相似度:57.1% European Journal of Organic Chemistry 2010 292-299 Efficient and Chirally Specific Synthesis of Phenanthro-Indolizidine Alkaloids by Parham-Type Cycloacylation Ziwen Wang, Zheng Li, Kailiang Wang and Qingmin Wang Structure 13C NMR 碳譜模擬圖 13 . 6,7,10,11-Tetramethoxy-2-(2-methoxybenzyl)-1,2,3,4-tetrahydrodibenzo[f,h]isoquinoline C29H31NO5 相似度:57.1% Bioorganic & Medicinal Chemistry 2012 20 5893-5900 Synthesis and evaluation of the anti-proliferative and NF-κB activities of a library of simplified tylophorine analogs Micah J. Niphakis, Bryant C. Gay, Kwon Ho Hong, Nicholas P. Bleeker, Gunda I. Georg Structure 13C NMR 碳譜模擬圖 14 . 2-((6,7,10,11-Tetramethoxy-3,4-dihydrodibenzo [f,h]isoquinolin-2(1H)-yl)methyl)phenol C28H29NO5 相似度:57.1% Bioorganic & Medicinal Chemistry 2012 20 5893-5900 Synthesis and evaluation of the anti-proliferative and NF-κB activities of a library of simplified tylophorine analogs Micah J. Niphakis, Bryant C. Gay, Kwon Ho Hong, Nicholas P. Bleeker, Gunda I. Georg Structure 13C NMR 碳譜模擬圖 15 . 2-[(6-Bromohexyl)oxy]-3-methoxy-6,7,10,11-tetrakis(octyloxy)triphenylene C57H88BrO6 相似度:53.5% Helvetica Chimica Acta 2009 92 2024-2037 Concise Synthesis of [1,1′-Biisoquinoline]-4,4′-diol via a Protecting Group Strategy and Its Application for Potential Liquid-Crystalline Compounds Elisabeth Kapatsina, Markus Mateescu, Angelika Baro, Wolfgang Frey, Sabine Laschat Structure 13C NMR 碳譜模擬圖 16 . compound 3a 相似度:53.5% Organic letters 2002 4 157-159 Design and Synthesis of Discotic Nematic Liquid Crystals Sandeep Kumar and Sanjay K. Varshney Structure 13C NMR 碳譜模擬圖 17 . O-(3,4-dimethoxyphenylpropenoyl)-(3,4-dihydro-6-methoxy-2,2,7,8-tetramethyl-2H-1-benzopyran-5-acetamid-oxime) 相似度:53.5% Bioorganic & Medicinal Chemistry 2010 18 3898-3909 Synthesis of a second generation chroman/catechol hybrids and evaluation of their activity in protecting neuronal cells from oxidative stress-induced cell death Maria Koufaki, Elissavet Theodorou, Xanthippi Alexi, Michael N. Alexis Structure 13C NMR 碳譜模擬圖 18 . deoxypergularinine C23H25NO3 相似度:53.5% Bioorganic & Medicinal Chemistry 2008 16 6233-6241 Total synthesis of phenanthroindolizidine alkaloids (±)-antofine, (±)-deoxypergularinine, and their dehydro congeners and evaluation of their cytotoxic activity Chung-Ren Su, Amooru G. Damu, Po-Cheng Chiang, Kenneth F. Bastow, Susan L. Morris-Natschke, Kuo-Hsiung Lee, Tian-Shung Wu Structure 13C NMR 碳譜模擬圖 19 . (9aR)-2,3,6-trimethoxy-9,9a,10,11,12,13-hexahydro-13a-azabenzotriphenylen-14-one C24H25NO4 相似度:53.5% European Journal of Organic Chemistry 2010 1943-1950 First Asymmetric Synthesis of Boehmeriasin A David Dumoulin, Stéphane Lebrun, Axel Couture, Eric Deniau and Pierre Grandclaudon Structure 13C NMR 碳譜模擬圖 20 . (S)-1-[(9-bromo-2,3,6,7-tetramethoxyphenanthren-10-yl)methyl]-N,N-diethylpyrrolidine-2-carboxamide C28H35BrN2O5 相似度:53.5% European Journal of Organic Chemistry 2010 292-299 Efficient and Chirally Specific Synthesis of Phenanthro-Indolizidine Alkaloids by Parham-Type Cycloacylation Ziwen Wang, Zheng Li, Kailiang Wang and Qingmin Wang Structure 13C NMR 碳譜模擬圖 21 . (13aS,14S)-14-hydroxyantofine C23H25NO4 相似度:53.5% European Journal of Organic Chemistry 2010 292-299 Efficient and Chirally Specific Synthesis of Phenanthro-Indolizidine Alkaloids by Parham-Type Cycloacylation Ziwen Wang, Zheng Li, Kailiang Wang and Qingmin Wang Structure 13C NMR 碳譜模擬圖 22 . (+)-deoxytylophorinine C23H25NO3 相似度:53.5% European Journal of Organic Chemistry 2010 292-299 Efficient and Chirally Specific Synthesis of Phenanthro-Indolizidine Alkaloids by Parham-Type Cycloacylation Ziwen Wang, Zheng Li, Kailiang Wang and Qingmin Wang Structure 13C NMR 碳譜模擬圖 23 . 6,7,10,11-Tetramethoxy-2-(4-nitrobenzyl)-1,2,3,4-tetrahydrodibenzo[f,h]isoquinoline C28H28N2O6 相似度:53.5% Bioorganic & Medicinal Chemistry 2012 20 5893-5900 Synthesis and evaluation of the anti-proliferative and NF-κB activities of a library of simplified tylophorine analogs Micah J. Niphakis, Bryant C. Gay, Kwon Ho Hong, Nicholas P. Bleeker, Gunda I. Georg Structure 13C NMR 碳譜模擬圖 24 . 6,7,10,11-tetramethoxy-2-(4-methoxybenzyl)-1,2,3,4-tetrahydrodibenzo[f,h]isoquinoline C29H31NO5 相似度:53.5% Bioorganic & Medicinal Chemistry 2012 20 5893-5900 Synthesis and evaluation of the anti-proliferative and NF-κB activities of a library of simplified tylophorine analogs Micah J. Niphakis, Bryant C. Gay, Kwon Ho Hong, Nicholas P. Bleeker, Gunda I. Georg Structure 13C NMR 碳譜模擬圖 25 . 2-(4-(tert-Butyl)benzyl)-6,7,10,11-tetramethoxy-1,2,3,4-tetrahydrodibenzo[f,h]isoquinoline C32H37NO4 相似度:53.5% Bioorganic & Medicinal Chemistry 2012 20 5893-5900 Synthesis and evaluation of the anti-proliferative and NF-κB activities of a library of simplified tylophorine analogs Micah J. Niphakis, Bryant C. Gay, Kwon Ho Hong, Nicholas P. Bleeker, Gunda I. Georg Structure 13C NMR 碳譜模擬圖 26 . tert-Butyl (2-(6,7,10,11-Tetramethoxy-3,4-dihydrodibenzo[f,h]isoquinolin-2(1H)-yl)ethyl)carbamate C28H26N2O6 相似度:53.5% Bioorganic & Medicinal Chemistry 2012 20 5893-5900 Synthesis and evaluation of the anti-proliferative and NF-κB activities of a library of simplified tylophorine analogs Micah J. Niphakis, Bryant C. Gay, Kwon Ho Hong, Nicholas P. Bleeker, Gunda I. Georg Structure 13C NMR 碳譜模擬圖 27 . 6,7,10,11-Tetramethoxy-2-(3-methoxybenzyl)-1,2,3,4-tetrahydrodibenzo[f,h]isoquinoline C32H31NO4 相似度:51.7% Bioorganic & Medicinal Chemistry 2012 20 5893-5900 Synthesis and evaluation of the anti-proliferative and NF-κB activities of a library of simplified tylophorine analogs Micah J. Niphakis, Bryant C. Gay, Kwon Ho Hong, Nicholas P. Bleeker, Gunda I. Georg Structure 13C NMR 碳譜模擬圖 28 . 6-genzoyl-1'-methyl-3,5-diphenyldispiro[cyclohexa-2,4-diene-1,2'-indoline-3',1''-cyclohexane] C38H35NO 相似度:51.6% Journal of Heterocyclic Chemistry 2002 39 255-262 Ring transformations of heterocyclic compounds. XXI. Diastereoselective built-up of an aroylcyclohexadiene moiety as second spiro-connected ring at spiroindolines by pyrylium ring transformation Thomas Zimmermann Structure 13C NMR 碳譜模擬圖 29 . boehmeriasin B C23H25NO3 相似度:50% Planta Medica 2003 69 842-845 Cytotoxic Alkaloids from Boehmeria siamensis Yinggang Luo,Yan Liu,Dixiang Luo, Xiaoping Gao,Bogang Li,Guolin Zhang Structure 13C NMR 碳譜模擬圖 30 . 4,4'-Bis{{6-{[3,6,7,10,11-pentakis(octyloxy)triphenylen-2-yl]oxy}hexyl}oxy}-1,1'-biisoquinoline C146H216N2O14 相似度:50% Helvetica Chimica Acta 2009 92 2024-2037 Concise Synthesis of [1,1′-Biisoquinoline]-4,4′-diol via a Protecting Group Strategy and Its Application for Potential Liquid-Crystalline Compounds Elisabeth Kapatsina, Markus Mateescu, Angelika Baro, Wolfgang Frey, Sabine Laschat Structure 13C NMR 碳譜模擬圖 31 . 3-[2-(2-cyano-3-ethyl-l,2,5,6-tetrahydro-l-pyridyl)ethyl]-l-(4-methoxybenzenesulfon-yl)indole-2-acetal-dehyde Ethylene Acetal C29H33N3O5S 相似度:50% Natural Product Research 1996 8 75-82 Studies on the Synthesis of Strychnos Alkaloids Daniele Passarella; Swargam Sathyanarayana; Mercedes Amat; Joan Bosch Structure 13C NMR 碳譜模擬圖 32 . 14α-hydroxyisotylocrebrine N-oxide C24H27NO6 相似度:50% Phytochemistry 1995 39 695-699 Phenanthroindolizidine alkaloids from Tylophora tanakae Fumiko Abe, Yukiko Iwase, Tatsuo Yamauchi, Keiichi Honda, Nanao Hayashi Structure 13C NMR 碳譜模擬圖 33 . tylophorine C24H27O4 相似度:50% Phytochemistry 1995 39 695-699 Phenanthroindolizidine alkaloids from Tylophora tanakae Fumiko Abe, Yukiko Iwase, Tatsuo Yamauchi, Keiichi Honda, Nanao Hayashi Structure 13C NMR 碳譜模擬圖 34 . tert-Butyl (5S)-3-(1-Hydroxydecylidene)-2,4-dioxo-5-[4-(prop-2-en-1-yloxy)benzyl]pyrrolidine-1-carboxylate 相似度:50% Chemistry & Biodiversity 2010 7 2830-2845 Structure–Activity Relationships of Precursors and Analogs of Natural 3-Enoyl-tetramic Acids Bertram Barnickel, Frances Bayliffe, Randi Diestel, Karl Kempf, Sabine Laschat, Steffen Pachali, Florenz Sasse, Andrea Schlenk and Rainer Schobert Structure 13C NMR 碳譜模擬圖 35 . 4-Pentyl-2-(4-{[5-(2,4,6-trimethoxyphenyl)pentyl]oxy}phenyl)-pyrimido[1,2-a]benzimidazole C35H41N3O4 相似度:50% European Journal of Organic Chemistry 2012 85-92 Trimethoxyarene as a Highly Ionizable Tag for Reaction Analysis by Atmospheric Pressure Photoionization Mass Spectrometry (APPI/MS): Exploration of Heterocyclic Synthesis Mathieu Bui The Thuong, Cédric Catala, Cyril Colas, Christine Schaeffer, Alain Van Dorsselaer, André Mann and Alain Wagner Structure 13C NMR 碳譜模擬圖 |
4樓2013-01-30 00:36:25
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木蟲 (小有名氣)
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2樓2013-01-29 15:14:35
yuanchunma
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3樓2013-01-29 23:50:24
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