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冰刃001木蟲 (小有名氣)
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[求助]
求助CIF文章退修意見。
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CHECKCIF文件時,有數(shù)據(jù)完整度低錯誤,在INS中添加了OMIT 0.00 50.10,精修就消除了,最后生成的TEX中,Completeness to theta = 25.05 99.9 % 但審稿人意見還是,數(shù)據(jù)完整度只有89%,太低。(是根據(jù)CHECKCIF中的Data completeness= 1.77/0.89 這個嗎?) 另,審稿人要求CIF進(jìn)行出版檢查,檢查結(jié)果數(shù)據(jù)有10個A級警告(如下): Alert level A CELL003_ALERT_1_A _cell_measurement_reflns_used is missing Number of reflections used to measure unit cell. CELL004_ALERT_1_A _cell_measurement_theta_min is missing Minimum theta of reflections used to measure unit cell. The following tests will not be performed. CELLT_01 CELL005_ALERT_1_A _cell_measurement_theta_max is missing Maximum theta of reflections used to measure unit cell. The following tests will not be performed. CELLT_01 EXPT005_ALERT_1_A _exptl_crystal_description is missing Crystal habit description. The following tests will not be performed. CRYSR_01 EXPT010_ALERT_1_A _exptl_crystal_colour (_pd_char_colour for powder) is missing Crystal colour. The following tests will not be performed. CRYSC_01 DIFF003_ALERT_1_A _diffrn_measurement_device_type is missing Diffractometer make and type. Replaces _diffrn_measurement_type. DIFF005_ALERT_1_A _diffrn_measurement_method is missing Mode of intensity measurement and scan. DIFF019_ALERT_1_A _diffrn_standards_number is missing Number of standards used in measurement. DIFF020_ALERT_1_A _diffrn_standards_interval_count and _diffrn_standards_interval_time are missing. Number of measurements between standards or time (min) between standards. DIFF022_ALERT_1_A _diffrn_standards_decay_% is missing Percentage decrease in standards intensity 請教,這些問題該如何處理,謝謝。 |
至尊木蟲 (職業(yè)作家)

木蟲 (小有名氣)
至尊木蟲 (職業(yè)作家)

木蟲 (小有名氣)
木蟲 (小有名氣)
木蟲 (小有名氣)
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