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[求助]
求助解析中cif文件出現(xiàn)的A錯(cuò)誤和B錯(cuò)誤,謝謝
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047_ALERT_1_A SumFormula Not Given ........................... ? #============================================================================== 027_ALERT_3_B _diffrn_reflns_theta_full (too) Low ............ 24.99 Deg. 415_ALERT_2_B Short Inter D-H..H-X H1WB .. H5 .. 1.97 Ang. #============================================================================== 042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ .... ? 125_ALERT_4_C No _symmetry_space_group_name_Hall Given ....... ? 302_ALERT_4_C Anion/Solvent Disorder ......................... 25.00 Perc. 720_ALERT_4_C Number of Unusual/Non-Standard Label(s) ........ 2 797_ALERT_4_C N-Atom in CIF Coordinate List out of Sequence .. N3 我想知道怎么再修,,重新收集是不可能的了,或者發(fā)文章的時(shí)候B錯(cuò)誤可以允許嗎,,求高人回答,,謝謝 [ Last edited by bxyl45 on 2013-10-15 at 12:13 ] |


鐵桿木蟲(chóng) (著名寫(xiě)手)
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047_ALERT_1_A SumFormula Not Given ........................... ?(填寫(xiě)cif文件可以解決) #============================================================================== 027_ALERT_3_B _diffrn_reflns_theta_full (too) Low ............ 24.99 Deg.(在ins文件中修改omit的數(shù)值) 415_ALERT_2_B Short Inter D-H..H-X H1WB .. H5 .. 1.97 Ang.(這是客體無(wú)序?qū)е碌?如果是那就分PART處理一下,或者就DFIX限定這兩個(gè)氫原子的距離大一點(diǎn)) #============================================================================== 042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ .... ? (填寫(xiě)cif文件可以解決) 125_ALERT_4_C No _symmetry_space_group_name_Hall Given ....... ? (填寫(xiě)cif文件可以解決) 302_ALERT_4_C Anion/Solvent Disorder ......................... 25.00 Perc. 720_ALERT_4_C Number of Unusual/Non-Standard Label(s) ........ 2 797_ALERT_4_C N-Atom in CIF Coordinate List out of Sequence .. N3 |

新蟲(chóng) (小有名氣)


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