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cff5616金蟲 (正式寫手)
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[求助]
求助：Pt Sn Sb 的各個晶面的晶面間距，并標(biāo)明文獻(xiàn)出處
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求助：Pt Sn Sb 的各個晶面的晶面間距，并標(biāo)明文獻(xiàn)出處。 例如：Pt （110）的晶面間距d=？ 文獻(xiàn)出處（所給信息能夠檢索出這篇文獻(xiàn)即可） 謝謝 |
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» 本主題相關(guān)價值貼推薦，對您同樣有幫助:
- 【求助】Cu的111晶面的晶面間距是多少？
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未來的院士
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9樓2013-10-17 11:27:00
zyhou
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非文王木木: 金幣+1, 感謝交流···歡迎常來 2013-10-16 10:30:29
cff5616: 金幣+5, ★★★很有幫助 2013-10-16 19:15:48
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要求好高��！ 做過Pt, Pt-Sb合金，沒有做過單獨(dú)的Sn, Sb 純Pt的可以參考： Catalysis Communications, Volume 41, 5 November 2013, Pages 101-105 Carbon, Volume 50, Issue 2, February 2012, Pages 586-596 Pt－Sb合金可以參考！ Applied Catalysis B: Environmental, Volume 127, 30 October 2012, Pages 212-220 |
2樓2013-10-16 09:15:54
xhtangxh
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jiangyun2: 金幣+2, C-EPI+1, 謝謝分享，辛苦了~ 2013-10-17 10:32:35
感謝參與，應(yīng)助指數(shù) +1
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jiangyun2: 金幣+2, C-EPI+1, 謝謝分享，辛苦了~ 2013-10-17 10:32:35
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這個查一下PDF卡片就清楚了。d值單位為埃。 1.Pt Card Information Names: Platinum Platinum, syn Formula: Pt PDF Number: 4-802 Quality: star Subfiles: inorganic mineral alloy CP EDU FOR NBS Cell and Symmetry Information System: cubic Space Group: Fm-3m (no. 225) a: 3.9231 Density (Dm): 21.370 Density (Dx): 21.472 Z: 4 Instrument Information Radiation: CuKa1 Wavelength: 1.54056 Filter: Ni Instrument(d): unknown Instrument(I): diffractometer I type: unknown Comments and Additional Information Colour: Light gray metallic Preparation: Sample prepared at NBS, Gaithersburg, Maryland, USA, and estimated to be more than 99.99% pure. Temperature: Pattern taken at 26 C. General: Opaque mineral optical data on specimen from unspecified locality: RR#2R#e=70.3, Disp.=16, VHN#5#0=122-129, Color values=.318, .324, 70.7, Ref.: IMA Commission on Ore Microscopy QDF. Literature References General: Swanson, Tatge. Natl. Bur. Stand. (U.S.), Circ. 539 I 31 (1953) Peak Data PeakList h k l d I 1 1 1 2.2650 100 2 0 0 1.9616 53 2 2 0 1.3873 31 3 1 1 1.1826 33 2 2 2 1.1325 12 4 0 0 0.9808 6 3 3 1 0.9000 22 4 2 0 0.8773 20 4 2 2 0.8008 29 2.Sn Sn有三種晶型 (1)體心四方 Card Information Names: Tin Tin, syn Formula: Sn PDF Number: 4-673 Quality: star Subfiles: inorganic mineral alloy CP EDU FOR NBS Cell and Symmetry Information System: tetragonal Space Group: I41/amd (no. 141) a: 5.831 c: 3.182 Density (Dx): 7.286 Z: 4 Instrument Information Radiation: CuKa1 Wavelength: 1.54056 Filter: Ni Instrument(d): unknown Instrument(I): diffractometer I type: unknown I/Icor: 1.97 Comments and Additional Information General: Space group given by Mark, Polanyi, Z. Phys., 18 75-96 (1925). Pattern: See ICSD 40037 (PDF 01-086-2264). Source: Sample was furnished by Johnson Matthey Company, Ltd. and annealed 12 hours at 160 C. Analysis: Analysis (wt.%): Pb 0.0012, Sb 0.001, Fe 0.00027, Cu 0.0002, As 0.0002, Bi 0.00012, S 0.0003, Sn 99.997 (by difference), other form alpha-Sn (cubic). Temperature: Pattern taken at 26 C. Melting Point: 231.8 Colour: Light gray metallic Literature References General: Swanson, Tatge. Natl. Bur. Stand. (U.S.), Circ. 539 I 24 (1953) Colour: Dana's System of Mineralogy, 7th Ed. 485 ( ) Peak Data PeakList h k l d I 2 0 0 2.9150 100 1 0 1 2.7930 90 2 2 0 2.0620 34 2 1 1 2.0170 74 3 0 1 1.6590 17 1 1 2 1.4840 23 4 0 0 1.4580 13 3 2 1 1.4420 20 4 2 0 1.3040 15 4 1 1 1.2920 15 3 1 2 1.2050 20 5 0 1 1.0950 13 1 0 3 1.0434 3 3 3 2 1.0401 5 4 4 0 1.0309 2 5 2 1 1.0252 5 2 1 3 0.9824 5 6 0 0 0.9718 2 3 0 3 0.9310 3 5 1 2 0.9286 13 6 2 0 0.9219 5 6 1 1 0.9178 5 3 2 3 0.8868 4 5 4 1 0.8755 2 4 1 3 0.8485 4 5 3 2 0.8466 10 6 3 1 0.8386 4 6 4 0 0.8086 6 7 0 1 0.8058 3 (2)面心立方 Card Information Names: alpha-Tin gray tin Formula: Sn PDF Number: 5-390 Quality: star Subfiles: inorganic alloy CP EDU FOR NBS Cell and Symmetry Information System: cubic Space Group: Fd-3m (no. 227) a: 6.489 Z: 8 Instrument Information Radiation: CuKa1 Wavelength: 1.5405 Filter: Ni Instrument(d): unknown Instrument(I): diffractometer I type: unknown Comments and Additional Information Colour: Gray Preparation: Sample was made from NBS Melting Point Standard 42D by seeding it with small quantity of alpha-Sn. Analysis: Spectroscopic analysis: <0.01% Cu, Fe, Pb. General: Sample was refrigerated at 10 C until just before use. Temperature: Pattern taken at 25 C. General: Merck Index , 8th Ed., p. 1053. Pattern: See ICSD 70128 (PDF 01-087-0794). Literature References General: Swanson, Fuyat. Natl. Bur. Stand. (U.S.), Circ. 539 II 12 (1953) Peak Data PeakList h k l d I 1 1 1 3.7510 100 2 2 0 2.2940 83 3 1 1 1.9560 53 4 0 0 1.6220 12 3 3 1 1.4890 20 4 2 2 1.3250 21 5 1 1 1.2490 11 4 4 0 1.1470 6 5 3 1 1.0968 10 6 2 0 1.0260 9 5 3 3 0.9895 4 4 4 4 0.9365 3 7 1 1 0.9087 7 6 4 2 0.8671 13 7 3 1 0.8450 12 (3)另一種體心四方 Card Information Names: Tin Formula: Sn PDF Number: 18-1380 Quality: star Subfiles: inorganic alloy Cell and Symmetry Information System: tetragonal Space Group: I4/mmm (no. 139) a: 3.811 c: 3.483 Density (Dx): 7.790 Z: 2 Instrument Information Radiation: CuKa Wavelength: 1.5418 Instrument(d): unknown Instrument(I): unknown I type: unknown Comments and Additional Information Temperature: Pattern at 39 kbar, 308-320 C. Literature References General: Barnett et al. Science 141 1041 (1963) Peak Data PeakList h k l d I 1 1 0 2.6950 50 1 0 1 2.5710 100 2 0 0 1.9060 40 0 0 2 1.7410 10 2 1 1 1.5310 30 1 1 2 1.4630 5 2 2 0 1.3470 5 3.Sb Sb有四種晶型，除下面的三方晶型外還有三種高壓晶相：簡單六方(PDF 17-124)、簡單立方(PDF 17-125)、簡單單斜(PDF 26-101). Card Information Names: Antimony Antimony, syn iron black Formula: Sb PDF Number: 35-732 Quality: star Subfiles: inorganic mineral alloy CP EDU FOR PIG Cell and Symmetry Information System: rhombohedral Space Group: R-3m (no. 166) a: 4.307 c: 11.273 Density (Dx): 6.697 Z: 6 Instrument Information Radiation: CuKa1 Wavelength: 1.5405 Instrument(d): diffractometer Instrument(I): diffractometer I type: unknown Comments and Additional Information Source: Sample from C.A.F. Kahlbaum. Analysis: Spectrographic analysis (wt.%): Cu <0.01; Bi, Fe, Ni, Pb, Si, Sn <0.001; Ag, Al, Ca <0.0001. General: Unit cell given for hexagonal axes. Temperature: Pattern taken at 26 C. Pattern: To replace 00-005-0562. RL Opaque mineral optical data on specimen from Tulare County, California, USA: R#3R%=71.1-73.0, Disp.=Std. VH VHN#1#0#0=84-98. Literature References General: Swanson, H., Fuyat. Natl. Bur. Stand. (U.S.), Circ. 539 3 14 (1954) RL IMA Commission on Ore Microscopy QDF ( ) Peak Data PeakList h k l d I 0 0 3 3.7530 25 1 0 1 3.5380 4 0 1 2 3.1090 100 1 0 4 2.2480 70 1 1 0 2.1520 56 0 1 5 1.9290 12 0 0 6 1.8780 35 2 0 2 1.7700 26 0 2 4 1.5550 15 1 0 7 1.4790 13 2 0 5 1.4370 12 1 1 6 1.4160 63 1 2 2 1.3680 67 0 1 8 1.3180 30 2 1 4 1.2610 40 0 0 9 1.2520 25 3 0 0 1.2430 30 0 2 7 1.2190 11 1 2 5 1.1955 12 3 0 3 1.1802 5 2 0 8 1.1243 12 1 1 9 1.0829 32 1 0 10 1.0792 16 2 2 0 1.0768 12 2 1 7 1.0609 16 3 0 6 1.0369 17 3 1 2 1.0177 27 1 2 8 0.9966 25 0 1 11 0.9882 24 1 3 4 0.9713 15 0 2 10 0.9650 8 3 1 5 0.9402 7 2 2 6 0.9343 13 0 4 2 0.9201 8 2 0 11 0.8981 10 4 0 4 0.8853 7 3 0 9 0.8825 15 2 1 10 0.8804 15 1 3 7 0.8704 1 |
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cff56163樓2013-10-16 09:47:06
cff5616
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4樓2013-10-16 19:18:49
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