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peihong1121鐵蟲 (初入文壇)
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[求助]
求Cu3As和As的XRD中出峰的位置？
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| 求Cu3As和As的XRD中出峰的位置？ |
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xhtangxh
木蟲 (著名寫手)
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【答案】應(yīng)助回帖
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PDF#30-0100: QM=Calculated(C); d=Calculated; I=Calculated Arsenolamprite As Radiation=CuKa Lambda=1.54188 Filter= Calibration= 2T=16.119-130.940 I/Ic(RIR)=6.56 Ref: Calvert, L., National Research Council of Canada, Ottawa, Canada. ICDD Grant-in-Aid (1978) Orthorhombic - Powder Diffraction, Bmab (64) Z=8 mp= CELL: 3.65 x 4.47 x 11.0 <90.0 x 90.0 x 90.0> P.S=oC8 (P) Density(c)=5.546 Density(m)=5.79A Mwt=74.92 Vol=179.47 F(30)=119.8(.0056,45/0) Ref: Smith, P. et al. Philos. Mag., v31 p57 (1976) Strong Lines: 2.74/X 1.74/3 2.24/2 3.47/2 1.69/1 5.49/1 1.82/1 1.88/1 1.52/1 1.44/1 NOTE: Plus 8 additional reflections to 0.7857. 2-Theta d(?) I(f) ( h k l ) Theta 1/(2d) 2pi/d n^2 16.119 5.4940 11.0 ( 0 0 2) 8.060 0.0910 1.1436 25.659 3.4690 23.0 ( 0 1 2) 12.829 0.1441 1.8112 32.679 2.7380 100.0 ( 1 1 1) 16.340 0.1826 2.2948 38.399 2.3423 1.0 ( 0 1 4) 19.199 0.2135 2.6825 40.318 2.2351 24.0 ( 0 2 0) 20.159 0.2237 2.8111 43.679 2.0706 1.0 ( 0 2 2) 21.840 0.2415 3.0345 48.438 1.8777 9.0 ( 1 2 1) 24.219 0.2663 3.3462 49.698 1.8330 4.0 ( 0 0 6) 24.849 0.2728 3.4278 49.940 1.8247 11.0 ( 2 0 0) 24.970 0.2740 3.4434 52.678 1.7361 32.0 ( 1 1 5) 26.339 0.2880 3.6191 54.200 1.6909 12.0 ( 1 2 3) 27.100 0.2957 3.7159 56.977 1.6149 3.0 ( 2 1 2) 28.489 0.3096 3.8908 60.879 1.5204 9.0 ( 2 0 4) 30.440 0.3289 4.1326 64.777 1.4380 7.0 ( 0 3 2) 32.389 0.3477 4.3694 65.837 1.4174 2.0 ( 0 2 6) 32.919 0.3528 4.4329 66.037 1.4136 5.0 ( 2 2 0) 33.018 0.3537 4.4448 68.140 1.3750 2.0 ( 0 0 8) 34.070 0.3636 4.5696 68.497 1.3687 2.0 ( 1 3 1) 34.248 0.3653 4.5906 72.018 1.3102 1.0 ( 0 3 4) 36.009 0.3816 4.7956 73.097 1.2935 2.0 ( 2 0 6) 36.548 0.3865 4.8575 75.576 1.2571 4.0 ( 2 2 4) 37.788 0.3977 4.9982 76.639 1.2423 1.0 ( 2 1 6) 38.319 0.4025 5.0577 78.874 1.2126 4.0 ( 1 2 7) 39.437 0.4123 5.1816 82.256 1.1711 1.0 ( 0 2 8) 41.128 0.4269 5.3652 82.582 1.1673 4.0 ( 3 1 1) 41.291 0.4283 5.3827 83.534 1.1564 2.0 ( 0 3 6) 41.767 0.4324 5.4334 85.995 1.1295 5.0 ( 2 3 2) 42.997 0.4427 5.5628 86.721 1.1219 5.0 ( 1 1 9) 43.360 0.4457 5.6005 88.895 1.1000 1.0 ( 0 0 10) 44.447 0.4545 5.7120 89.079 1.0982 2.0 ( 2 0 8) 44.540 0.4553 5.7213 92.492 1.0664 1.0 ( 2 1 8) 46.246 0.4689 5.8920 92.842 1.0633 3.0 ( 1 4 1) 46.421 0.4702 5.9091 96.100 1.0357 4.0 ( 3 1 5) 48.050 0.4828 6.0666 97.338 1.0258 5.0 ( 1 4 3) 48.669 0.4874 6.1252 99.331 1.0105 1.0 ( 0 3 8) 49.665 0.4948 6.2179 102.614 0.9869 1.0 ( 0 2 10) 51.307 0.5066 6.3666 102.802 0.9856 1.0 ( 2 2 8) 51.401 0.5073 6.3750 104.120 0.9767 2.0 ( 2 3 6) 52.060 0.5119 6.4331 106.539 0.9611 1.0 ( 1 4 5) 53.269 0.5202 6.5375 109.695 0.9421 1.0 ( 2 0 10) 54.847 0.5307 6.6693 110.234 0.9390 1.0 ( 2 4 2) 55.117 0.5325 6.6914 114.728 0.9147 1.0 ( 1 3 9) 57.364 0.5466 6.8691 115.180 0.9124 1.0 ( 4 0 0) 57.590 0.5480 6.8864 120.890 0.8855 2.0 ( 1 2 11) 60.445 0.5647 7.0956 121.326 0.8836 6.0 ( 1 4 7) 60.663 0.5659 7.1109 121.604 0.8824 3.0 ( 0 5 2) 60.802 0.5666 7.1206 125.076 0.8681 1.0 ( 2 2 10) 62.538 0.5760 7.2379 125.587 0.8661 2.0 ( 4 0 4) 62.794 0.5773 7.2546 130.940 0.8467 2.0 ( 3 1 9) 65.470 0.5905 7.4208 |
5樓2013-10-23 10:56:55
xhtangxh
木蟲 (著名寫手)
有木有蟲
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【答案】應(yīng)助回帖
★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★
感謝參與，應(yīng)助指數(shù) +1
jiangyun2: 金幣+3, 謝謝回帖交流，歡迎常來~~ 2013-10-23 10:55:47
peihong1121(jiangyun2代發(fā)): 金幣+20 2013-11-04 10:46:12
感謝參與，應(yīng)助指數(shù) +1
jiangyun2: 金幣+3, 謝謝回帖交流，歡迎常來~~ 2013-10-23 10:55:47
peihong1121(jiangyun2代發(fā)): 金幣+20 2013-11-04 10:46:12
|
PDF#14-0454: QM=Blank(B); d=Other/Unknown(57.3mm); I=Film/Visual Domeykite-$GB Cu3 As Gray metallic Radiation=CuKa Lambda=1.5418 Filter=Ni Calibration= 2T=24.502-119.876 I/Ic(RIR)= Ref: Berry, Thompson. Mem. Geol. Soc. Am., v85 p31 (1962) Hexagonal - Powder Diffraction, P-3c1 (165) Z=6 mp= CELL: 7.16 x 7.16 x 7.33 <90.0 x 90.0 x 120.0> P.S=hP24 (As Cu3) Density(c)=8.130 Density(m)=7.200 Mwt=265.56 Vol=325.43 F(30)=2.8(0.111,97/2) Ref: Ibid. Strong Lines: 2.08/X 2.02/X 1.45/5 1.19/5 3.63/4 1.33/4 2.37/3 2.23/3 1.80/3 3.21/2 NOTE: Specimen from Houghton County, Michigan, USA. 1 Corresponds to strongest reflection of arsenian copper d(111)=2.104. To replace 00-002-1251. See ICSD 16840 (PDF 01-072-1329); See ICSD 26776 (PDF 01-074-1068). 2-Theta d(?) I(f) ( h k l ) Theta 1/(2d) 2pi/d n^2 24.502 3.6300 40.0 ( 0 0 2) 12.251 0.1377 1.7309 27.769 3.2100 20.0 ( 1 1 1) 13.884 0.1558 1.9574 35.022 2.5600 10.0 ( 1 1 2) 17.511 0.1953 2.4544 37.933 2.3700 30.0 ( 2 0 2) 18.966 0.2110 2.6511 40.415 2.2300 30.0 ( 2 1 1) 20.207 0.2242 2.8176 42.401 2.1300 5.0 21.201 0.2347 2.9499 43.472 2.0800 100.0 ( 3 0 0) 21.736 0.2404 3.0208 44.832 2.0200 100.0 ( 1 1 3) 22.416 0.2475 3.1105 45.960 1.9730 20.0 ( 2 1 2) 22.980 0.2534 3.1846 50.553 1.8040 30.0 ( 3 0 2) 25.276 0.2772 3.4829 52.164 1.7520 20.0 ( 1 0 4) 26.082 0.2854 3.5863 54.864 1.6720 10.0 ( 3 1 1) 27.432 0.2990 3.7579 56.139 1.6370 5.0 ( 1 1 4) 28.070 0.3054 3.8382 64.426 1.4450 50.0 ( 2 2 3) 32.213 0.3460 4.3482 66.815 1.3990 10.0 ( 3 2 1) 33.408 0.3574 4.4912 70.844 1.3290 40.0 ( 4 1 1) 35.422 0.3762 4.7278 75.725 1.2550 10.0 ( 3 1 4) 37.863 0.3984 5.0065 77.999 1.2240 10.0 ( 0 0 6) 39.000 0.4085 5.1333 80.350 1.1940 5.0 ( 3 3 0) 40.175 0.4188 5.2623 81.004 1.1860 50.0 ( 4 1 3) 40.502 0.4216 5.2978 83.304 1.1590 20.0 ( 4 2 1) 41.652 0.4314 5.4212 85.292 1.1370 10.0 ( 2 0 6) 42.646 0.4398 5.5261 87.002 1.1190 5.0 ( 4 2 2) 43.501 0.4468 5.6150 88.590 1.1030 5.0 ( 5 1 1) 44.295 0.4533 5.6965 91.321 1.0770 5.0 45.660 0.4643 5.8340 94.143 1.0520 20.0 ( 3 0 6) 47.072 0.4753 5.9726 96.310 1.0340 10.0 ( 6 0 0) 48.155 0.4836 6.0766 99.264 1.0110 10.0 ( 4 3 1) 49.632 0.4946 6.2148 101.316 0.9960 5.0 ( 3 1 6) 50.658 0.5020 6.3084 102.890 0.9850 5.0 ( 5 2 1) 51.445 0.5076 6.3789 113.704 0.9200 10.0 ( 5 2 3) 56.852 0.5435 6.8295 116.263 0.9070 10.0 ( 4 1 6) 58.131 0.5513 6.9274 119.876 0.8900 10.0 ( 4 3 4) 59.938 0.5618 7.0598 |
2樓2013-10-23 10:49:15
xhtangxh
木蟲 (著名寫手)
有木有蟲
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【答案】應(yīng)助回帖
|
PDF#44-1475: QM=Star(S); d=Diffractometer; I=Diffractometer Domeykite Cu3 As Light gray metallic Radiation=CuKa1 Lambda=1.54056 Filter=Graph Calibration=Internal(Si) 2T=22.618-107.925 I/Ic(RIR)= Ref: Worman, W., Nodland, D., McCarthy, G., Bayliss, P., North Dakota State Univ., Fargo, ND, USA. ICDD Grant-in-Aid (1992) Cubic - Powder Diffraction, I-43d (220) Z=16 mp= CELL: 9.6202 x 9.6202 x 9.6202 <90.0 x 90.0 x 90.0> P.S=cI64 (As Cu3) Density(c)=7.925 Density(m)=8.09A Mwt=265.56 Vol=890.33 F(30)=136.8(.0063,35/0) Ref: Iglesias, J., Nowacki, W. Z. Kristallogr., Kristallgeom., Kristallphys., Kristallchem., v145 p334 (1977) Strong Lines: 2.05/X 1.89/8 1.96/5 2.15/5 3.04/3 3.93/3 2.57/2 3.40/2 1.31/2 1.22/1 NOTE: Specimen from Mohawk mine, Keweenaw County, Michigan, USA. X-ray fluorescence analysis: major Cu and As. Average relative standard deviation in intensity of the ten strongest reflections for three specimen mounts is 9%. Validated by calculated pattern. To replace 00-009-0333. See ICSD 100149 (PDF 01-083-1297). 2-Theta d(?) I(f) ( h k l ) Theta 1/(2d) 2pi/d n^2 22.618 3.9280 29.0 ( 2 1 1) 11.309 0.1273 1.5996 6 26.165 3.4030 15.0 ( 2 2 0) 13.082 0.1469 1.8464 8 29.336 3.0420 32.0 ( 3 1 0) 14.668 0.1644 2.0655 10 34.868 2.5710 20.0 ( 3 2 1) 17.434 0.1945 2.4439 14 37.355 2.4053 7.0 ( 4 0 0) 18.678 0.2079 2.6122 16 41.968 2.1510 45.0 ( 4 2 0) 20.984 0.2325 2.9211 20 44.109 2.0514 100.0 ( 3 3 2) 22.055 0.2437 3.0629 22 46.183 1.9640 54.0 ( 4 2 2) 23.091 0.2546 3.1992 24 48.187 1.8869 76.0 ( 5 1 0) 24.093 0.2650 3.3299 26 52.033 1.7561 1.0 ( 5 2 1) 26.017 0.2847 3.5779 30 55.662 1.6499 1.0 ( 5 3 0) 27.831 0.3030 3.8082 34 59.148 1.5607 5.0 ( 6 1 1) 29.574 0.3204 4.0259 38 60.848 1.5211 4.0 ( 6 2 0) 30.424 0.3287 4.1307 40 62.519 1.4844 5.0 ( 5 4 1) 31.260 0.3368 4.2328 42 65.785 1.4184 1.0 ( 6 3 1) 32.892 0.3525 4.4298 46 67.382 1.3886 1.0 ( 4 4 4) 33.691 0.3601 4.5248 48 68.979 1.3603 4.0 ( 7 1 0) 34.490 0.3676 4.6190 50 72.081 1.3092 15.0 ( 7 2 1) 36.041 0.3819 4.7993 54 75.162 1.2630 3.0 ( 7 3 0) 37.581 0.3959 4.9748 58 78.174 1.2217 10.0 ( 7 3 2) 39.087 0.4093 5.1430 62 81.145 1.1843 8.0 ( 7 4 1) 40.572 0.4222 5.3054 66 82.642 1.1666 2.0 ( 8 2 0) 41.321 0.4286 5.3859 68 84.114 1.1499 2.0 ( 6 5 3) 42.057 0.4348 5.4641 70 85.590 1.1338 2.0 ( 8 2 2) 42.795 0.4410 5.5417 72 87.060 1.1184 6.0 ( 8 3 1) 43.530 0.4471 5.6180 74 90.004 1.0893 4.0 ( 7 5 2) 45.002 0.4590 5.7681 78 92.944 1.0624 1.0 ( 9 1 0) 46.472 0.4706 5.9141 82 94.425 1.0496 1.0 ( 8 4 2) 47.213 0.4764 5.9863 84 95.879 1.0375 2.0 ( 9 2 1) 47.940 0.4819 6.0561 86 97.351 1.0257 2.0 ( 6 6 4) 48.675 0.4875 6.1258 88 98.853 1.0141 5.0 ( 9 3 0) 49.426 0.4930 6.1958 90 101.834 0.9923 3.0 ( 9 3 2) 50.917 0.5039 6.3318 94 103.347 0.9819 1.0 ( 8 4 4) 51.673 0.5092 6.3991 96 104.860 0.9718 1.0 ( 9 4 1) 52.430 0.5145 6.4653 98 107.925 0.9526 1.0 ( 10 1 1) 53.963 0.5249 6.5960 102 |
3樓2013-10-23 10:49:54
xhtangxh
木蟲 (著名寫手)
有木有蟲
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【答案】應(yīng)助回帖
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PDF#05-0632: QM=Indexed(I); d=(Unknown); I=Diffractometer Arsenic, syn As Light gray metallic Radiation=CuKa1 Lambda=1.5405 Filter=Ni Calibration= 2T=25.281-119.809 I/Ic(RIR)= Ref: Swanson, Fuyat. Natl. Bur. Stand. (U.S.), Circ. 539, vIII p6 (1954) Rhombohedral - Powder Diffraction, R-3m (166) Z=6 mp= CELL: 3.76 x 3.76 x 10.548 <90.0 x 90.0 x 120.0> P.S=hR2 (As) Density(c)=5.778 Density(m)=5.705 Mwt=74.92 Vol=129.14 F(27)=32.6(0.024,34/0) Ref: Ibid. Strong Lines: 2.77/X 3.52/3 1.88/3 2.05/2 1.56/1 1.77/1 1.76/1 1.20/1 3.11/1 1.66/1 NOTE: See ICSD 16516 (PDF 01-072-1046), 16517 (PDF 01-072-1047); 16518 (PDF 01-072-1048). Sample from Baker Chemical Company. Spectroscopic analysis: <0.1% Bi, Sb; <0.01% Fe, Si; <0.001% Ag, Al, Ca, Mg, Pb. Pattern taken at 26 C. Sample was purified by sublimation in a nitrogen atmosphere. Rhombohedral parameters: a=4.132, $GA=54.13, Z=2. Opaque mineral optical data on specimen from Borneo, R3R%=51.3-56.4, Disp.=Std. VHN100=83-149. 2-Theta d(?) I(f) ( h k l ) Theta 1/(2d) 2pi/d n^2 25.281 3.5200 26.0 ( 0 0 3) 12.640 0.1420 1.7850 28.662 3.1120 6.0 ( 1 0 1) 14.331 0.1607 2.0190 32.279 2.7710 100.0 ( 0 1 2) 16.140 0.1804 2.2675 44.141 2.0500 24.0 ( 1 0 4) 22.070 0.2439 3.0650 48.402 1.8790 26.0 ( 1 1 0) 24.201 0.2661 3.3439 51.657 1.7680 10.0 ( 0 1 5) 25.828 0.2828 3.5538 52.004 1.7570 7.0 ( 0 0 6) 26.002 0.2846 3.5761 55.367 1.6580 6.0 ( 1 1 3) 27.683 0.3016 3.7896 59.345 1.5560 11.0 ( 2 0 2) 29.672 0.3213 4.0380 67.526 1.3860 6.0 ( 0 2 4) 33.763 0.3608 4.5333 68.594 1.3670 4.0 ( 1 0 7) 34.297 0.3658 4.5963 73.393 1.2890 5.0 ( 2 0 5) 36.697 0.3879 4.8745 73.726 1.2840 5.0 ( 1 1 6) 36.863 0.3894 4.8934 78.151 1.2220 1.0 ( 0 1 8) 39.075 0.4092 5.1417 79.971 1.1987 7.0 ( 1 2 2) 39.986 0.4171 5.2417 82.162 1.1722 1.0 ( 0 0 9) 41.081 0.4265 5.3602 87.314 1.1158 4.0 ( 2 1 4) 43.657 0.4481 5.6311 88.267 1.1062 2.0 ( 0 2 7) 44.133 0.4520 5.6800 90.385 1.0857 3.0 ( 3 0 0) 45.192 0.4605 5.7872 92.865 1.0631 3.0 ( 1 2 5) 46.432 0.4703 5.9102 95.891 1.0374 2.0 ( 3 0 3) 47.946 0.4820 6.0567 101.484 0.9948 2.0 ( 1 1 9) 50.742 0.5026 6.3160 107.838 0.9531 2.0 ( 2 1 7) 53.919 0.5246 6.5924 110.111 0.9397 1.0 ( 2 2 0) 55.056 0.5321 6.6864 113.742 0.9198 3.0 ( 0 1 11) 56.871 0.5436 6.8310 117.817 0.8995 1.0 ( 1 2 8) 58.908 0.5559 6.9852 119.809 0.8903 2.0 ( 3 1 2) 59.905 0.5616 7.0574 |
4樓2013-10-23 10:55:42
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[考研] 286求調(diào)劑 +10 | Faune 2026-03-21 | 10/500 |
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[考研] 求調(diào)劑 +4 | 要好好無聊 2026-03-21 | 4/200 |
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[考研] 求調(diào)劑 +3 | .m.. 2026-03-21 | 4/200 |
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[考研] 材料與化工（0856）304求 B區(qū) 調(diào)劑 +3 | 邱gl 2026-03-21 | 3/150 |
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[考研] 22 350 本科985求調(diào)劑，求老登收留 +3 | 李軼男003 2026-03-20 | 3/150 |
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[考研] 304求調(diào)劑 +6 | 曼殊2266 2026-03-18 | 6/300 |
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[考研] 一志愿 西北大學(xué) ，070300化學(xué)學(xué)碩，總分287，雙非一本，求調(diào)劑。 +4 | 晨昏線與星海 2026-03-19 | 4/200 |
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[考研]
 材料與化工 322求調(diào)劑
+4
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然11 2026-03-19 | 4/200 |
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[考研] 329求調(diào)劑 +9 | 想上學(xué)吖吖 2026-03-19 | 9/450 |
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[考研] 一志愿吉林大學(xué)材料學(xué)碩321求調(diào)劑 +11 | Ymlll 2026-03-18 | 15/750 |
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[考研] 0856調(diào)劑，是學(xué)校就去 +8 | sllhht 2026-03-19 | 9/450 |
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