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鈦酸鋰的標(biāo)準(zhǔn)卡片
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| 求助鈦酸鋰Li4Ti5O12的XRD標(biāo)準(zhǔn)圖譜,發(fā)現(xiàn)文章中的標(biāo)準(zhǔn)圖譜的峰位有兩個(gè)版本 |
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PDF#49-0207: QM=Star(+); d=Diffractometer; I=Diffractometer Lithium Titanium Oxide Li4 Ti5 O12 Radiation=CuKa1 Lambda=1.54050 Filter= Calibration=External(Si) d-Cutoff=5.9 I/Ic(RIR)= Ref= Tsubone, D., Hashimoto, T., Igarashi, K., Shimizu, T. d:\program files\mdi jade 5.0\pdf\codens.dat missing! Cubic - Powder Diffraction, Fd-3m (227) Z= mp= Cell=8.3588 Pearson=cF0 (?) Density(c)=1.306 Density(m)=3.79A Mwt=459.26 Vol=584.03 F(19)=56.2(.0130,26) Ref= Ibid. Strong Line: 4.84/X 2.09/6 2.52/5 1.48/3 1.61/2 1.41/1 1.21/1 1.92/1 1.17/1 0.93/1 NOTE: Prepared from Li3 C O3 and Li2 Ti3 O7 at 930 C for 30 hours, followed by cooling in air. Pattern taken at 25 C. d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d 4.8358 100.0 70.0 1 1 1 3 18.331 9.165 0.1034 1.2993 2.9587 1.0 1.0 2 2 0 8 30.181 15.091 0.1690 2.1237 2.5217 45.0 60.0 3 1 1 11 35.571 17.786 0.1983 2.4916 2.4142 2.0 3.0 2 2 2 12 37.212 18.606 0.2071 2.6026 2.0905 62.0 100.0 4 0 0 16 43.242 21.621 0.2392 3.0056 1.9182 6.0 11.0 3 3 1 19 47.352 23.676 0.2607 3.2755 1.6088 20.0 42.0 3 3 3 27 57.213 28.607 0.3108 3.9055 1.4777 33.0 75.0 4 4 0 32 62.833 31.416 0.3384 4.2519 1.4129 11.0 26.0 5 3 1 35 66.073 33.036 0.3539 4.4470 1.2749 4.0 11.0 5 3 3 43 74.344 37.172 0.3922 4.9285 1.2601 2.0 5.0 6 2 2 44 75.363 37.681 0.3968 4.9861 1.2066 7.0 20.0 4 4 4 48 79.344 39.672 0.4144 5.2074 1.1704 5.0 14.0 5 5 1 51 82.315 41.157 0.4272 5.3684 1.0883 4.0 12.0 7 3 1 59 90.114 45.057 0.4594 5.7736 1.0447 3.0 10.0 8 0 0 64 95.005 47.503 0.4786 6.0142 0.9651 3.0 10.0 7 5 1 75 105.906 52.953 0.5181 6.5105 0.9588 1.0 4.0 6 6 2 76 106.906 53.453 0.5215 6.5531 0.9345 5.0 18.0 8 4 0 80 111.036 55.518 0.5351 6.7239 0.9174 2.0 7.0 7 5 3 83 114.197 57.099 0.5450 6.8487 |
木蟲(chóng) (著名寫(xiě)手)
有木有蟲(chóng)
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Card Information Names: Lithium Titanium Oxide Formula: Li4 Ti5 O12 PDF Number: 49-207 Quality: star Subfiles: inorganic CER COR Cell and Symmetry Information System: cubic Space Group: Fd-3m (no. 227) a: 8.3588 Instrument Information Radiation: CuKa1 Wavelength: 1.54050 Instrument(d): diffractometer Cut Off: 5.9 Standard: Si Instrument(I): diffractometer I type: unknown Comments and Additional Information Preparation: Prepared from Li3 C O3 and Li2 Ti3 O7 at 930 C for 30 hours, followed by cooling in air. Temperature: Pattern taken at 25 C. Literature References General: Tsubone, D., Hashimoto, T., Igarashi, K.,Shimizu, T. J. Ceram. Soc. Jpn. Inter. Ed. 102 179 (1994) Strong Lines: 4.84/X 2.09/6 2.52/5 1.48/3 1.61/2 1.41/1 1.21/1 1.92/1 1.17/1 0.93/1 NOTE: Prepared from Li3 C O3 and Li2 Ti3 O7 at 930 C for 30 hours, followed by cooling in air. Pattern taken at 25 C. Peak Data 2-Theta d(?) I(f) ( h k l ) Theta 1/(2d) 2pi/d n^2 18.331 4.8358 100.0 ( 1 1 1) 9.165 0.1034 1.2993 3 30.181 2.9587 1.0 ( 2 2 0) 15.091 0.1690 2.1237 8 35.571 2.5217 45.0 ( 3 1 1) 17.786 0.1983 2.4916 11 37.212 2.4142 2.0 ( 2 2 2) 18.606 0.2071 2.6026 12 43.242 2.0905 62.0 ( 4 0 0) 21.621 0.2392 3.0056 16 47.352 1.9182 6.0 ( 3 3 1) 23.676 0.2607 3.2755 19 57.213 1.6088 20.0 ( 3 3 3) 28.607 0.3108 3.9055 27 62.833 1.4777 33.0 ( 4 4 0) 31.416 0.3384 4.2519 32 66.073 1.4129 11.0 ( 5 3 1) 33.036 0.3539 4.4470 35 74.344 1.2749 4.0 ( 5 3 3) 37.172 0.3922 4.9285 43 75.363 1.2601 2.0 ( 6 2 2) 37.681 0.3968 4.9861 44 79.344 1.2066 7.0 ( 4 4 4) 39.672 0.4144 5.2074 48 82.315 1.1704 5.0 ( 5 5 1) 41.157 0.4272 5.3684 51 90.114 1.0883 4.0 ( 7 3 1) 45.057 0.4594 5.7736 59 95.005 1.0447 3.0 ( 8 0 0) 47.503 0.4786 6.0142 64 105.906 0.9651 3.0 ( 7 5 1) 52.953 0.5181 6.5105 75 106.906 0.9588 1.0 ( 6 6 2) 53.453 0.5215 6.5531 76 111.036 0.9345 5.0 ( 8 4 0) 55.518 0.5351 6.7239 80 114.197 0.9174 2.0 ( 7 5 3) 57.099 0.5450 6.8487 83 |
木蟲(chóng) (著名寫(xiě)手)
有木有蟲(chóng)
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