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shenyunfan鐵蟲 (初入文壇)
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[求助]
求Ag 和AgCl 的XRD標(biāo)準(zhǔn)卡
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| 哪位大神有Ag 和 AgCl 的XRD標(biāo)準(zhǔn)卡,我需要可以在origin中作圖的數(shù)據(jù)。 |
木蟲 (著名寫手)
有木有蟲
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Ag: 1. PDF#04-0783: QM=Indexed(I); d=(Unknown); I=Diffractometer Silver-3C, syn Ag Light gray metallic Radiation=CuKa1 Lambda=1.54056 Filter=Ni Calibration= 2T=38.116-134.882 I/Ic(RIR)=5.20 Ref: Swanson, Tatge. Natl. Bur. Stand. (U.S.), Circ. 539, vI p23 (1953) Cubic - Powder Diffraction, Fm-3m (225) Z=4 mp=960.6$DE CELL: 4.0862 x 4.0862 x 4.0862 <90.0 x 90.0 x 90.0> P.S=cF4 (Cu) Density(c)=10.500 Density(m)=10.500 Mwt=107.87 Vol=68.23 F(9)=64.7(.0154,9/0) Ref: Ibid. Strong Lines: 2.36/X 2.04/4 1.23/3 1.45/3 0.94/2 0.83/1 1.18/1 0.91/1 1.02/1 0.00/1 NOTE: See ICSD 64706 (PDF 01-087-0597). Sample obtained from Johnson Matthey Company, Ltd. Purity >99.999%. Spectrographic analysis indicated faint traces of Ca, Fe and Cu. Pattern taken at 27 C. Opaque mineral optical data on specimen from Great Bear Lake, Canada: RR2Re=94.1, Disp.=16, VHN100=55-63, Color values .314, .321, 94.2, Ref.: IMA Commission on Ore Microscopy QDF. 2-Theta d(?) I(f) ( h k l ) Theta 1/(2d) 2pi/d n^2 38.116 2.3590 100.0 ( 1 1 1) 19.058 0.2120 2.6635 3 44.277 2.0440 40.0 ( 2 0 0) 22.139 0.2446 3.0740 4 64.426 1.4450 25.0 ( 2 2 0) 32.213 0.3460 4.3482 8 77.472 1.2310 26.0 ( 3 1 1) 38.736 0.4062 5.1041 11 81.536 1.1796 12.0 ( 2 2 2) 40.768 0.4239 5.3265 12 97.888 1.0215 4.0 ( 4 0 0) 48.944 0.4895 6.1509 16 110.497 0.9375 15.0 ( 3 3 1) 55.248 0.5333 6.7021 19 114.924 0.9137 12.0 ( 4 2 0) 57.462 0.5472 6.8766 20 134.882 0.8341 13.0 ( 4 2 2) 67.441 0.5994 7.5329 24 2. PDF#41-1402: QM=Indexed(I); d=Debye-Scherrer(114.0mm); I=Film/Visual Silver-4H Ag Radiation=FeKa Lambda=1.9373 Filter= Calibration= 2T=35.891-100.758 I/Ic(RIR)= Ref: Novgorodova, D., Gorshkov, A., Mokhov, A. Zap. Vses. Mineral. O-va, v108 p552 (1979) Hexagonal - (Unknown), P63/mmc (194) Z=4 mp= CELL: 2.8862 x 2.8862 x 10.0 <90.0 x 90.0 x 120.0> P.S=hP4 (La) Density(c)=9.530 Density(m)=10.47A Mwt=107.87 Vol=72.14 F(15)=34.1(.0169,26/0) Ref: Ibid. Strong Lines: 1.44/X 2.00/8 2.50/6 1.24/X 1.17/9 1.39/2 1.25/2 1.00/2 2.43/1 2.24/1 NOTE: Specimen from northeastern USSR. Microprobe analysis, average of six (wt.%): Ag 99.07, Au 0.19, Sb 0.20, Bi 0.22. 1 Reference reports 1.27. See ICSD 64707 (PDF 01-087-0598). 2-Theta d(?) I(f) ( h k l ) Theta 1/(2d) 2pi/d n^2 35.891 2.5000 60.0 ( 1 0 0) 17.945 0.2000 2.5133 35.891 2.5000 60.0 ( 0 0 4) 17.945 0.2000 2.5133 37.041 2.4250 10.0 ( 1 0 1) 18.520 0.2062 2.5910 40.301 2.2360 10.0 ( 1-1 2) 20.151 0.2236 2.8100 45.305 2.0000 80.0 ( 1 0 3) 22.652 0.2500 3.1416 51.688 1.7670 10.0 ( 1 0 4) 25.844 0.2830 3.5558 55.078 1.6660 10.0 ( 0 0 6) 27.539 0.3001 3.7714 59.136 1.5610 10.0 ( 1 0 5) 29.568 0.3203 4.0251 64.526 1.4430 100.0 ( 1 1 0) 32.263 0.3465 4.3543 67.526 1.3860 20.0 ( 1 1 2) 33.763 0.3608 4.5333 76.082 1.2500 20.0 ( 0 0 8) 38.041 0.4000 5.0265 76.807 1.2400 100.0 ( 2 0 1) 38.403 0.4032 5.0671 78.921 1.2120 10.0 ( 2 0 2) 39.460 0.4125 5.1841 82.350 1.1700 90.0 ( 2 0 3) 41.175 0.4274 5.3702 87.099 1.1180 10.0 ( 1 0 8) 43.549 0.4472 5.6200 100.758 1.0000 20.0 ( 0 0 10) 50.379 0.5000 6.2832 |
木蟲 (著名寫手)
有木有蟲
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AgCl: 1. PDF#31-1238: QM=Star(S); d=(Unknown); I=Diffractometer Chlorargyrite, syn Ag Cl Colorless Radiation=CuKa1 Lambda=1.5405 Filter=Ni Calibration= 2T=27.831-134.065 I/Ic(RIR)= Ref: Natl. Bur. Stand. (U.S.), Circ. 539, v4 p44 (1955) Cubic - Powder Diffraction, Fm-3m (225) Z=4 mp= CELL: 5.5491 x 5.5491 x 5.5491 <90.0 x 90.0 x 90.0> P.S=cF8 (Cl Na) Density(c)=5.571 Density(m)=5.556 Mwt=143.32 Vol=170.87 F(16)=134.5(.0074,16/0) Ref: Ibid. Strong Lines: 2.77/X 3.20/5 1.96/5 1.67/2 1.60/2 1.24/1 1.13/1 1.39/1 1.27/1 1.07/1 NOTE: Sample prepared at NBS, Gaithersburg, Maryland, USA. Spectroscopic analysis: Al, Fe <0.1%; Mg, Si <0.01%; Ca, Cu, Pb <0.001%; Mn <0.0001%. Pattern taken at 26 C. To replace 00-006-0480. See ICSD 64734 (PDF 01-085-1355). 2-Theta d(?) I(f) ( h k l ) Theta 1/(2d) 2pi/d n^2 27.831 3.2030 50.0 ( 1 1 1) 13.915 0.1561 1.9617 3 32.243 2.7740 100.0 ( 2 0 0) 16.122 0.1802 2.2650 4 46.233 1.9620 50.0 ( 2 2 0) 23.116 0.2548 3.2024 8 54.828 1.6730 16.0 ( 3 1 1) 27.414 0.2989 3.7556 11 57.478 1.6020 16.0 ( 2 2 2) 28.739 0.3121 3.9221 12 67.471 1.3870 6.0 ( 4 0 0) 33.735 0.3605 4.5301 16 74.471 1.2730 4.0 ( 3 3 1) 37.235 0.3928 4.9357 19 76.734 1.2410 12.0 ( 4 2 0) 38.367 0.4029 5.0630 20 85.703 1.1326 8.0 ( 4 2 2) 42.851 0.4415 5.5476 24 92.313 1.0680 4.0 ( 5 1 1) 46.157 0.4682 5.8831 27 103.478 0.9810 2.0 ( 4 4 0) 51.739 0.5097 6.4049 32 110.409 0.9380 2.0 ( 5 3 1) 55.204 0.5330 6.6985 35 112.799 0.9248 4.0 ( 6 0 0) 56.399 0.5407 6.7941 36 122.783 0.8774 4.0 ( 6 2 0) 61.392 0.5699 7.1611 40 131.089 0.8462 2.0 ( 5 3 3) 65.544 0.5909 7.4252 43 134.065 0.8366 4.0 ( 6 2 2) 67.033 0.5977 7.5104 44 2. PDF#22-1326: QM=Blank(B); d=Debye-Scherrer(114.6mm); I=Film/Visual Silver Chloride Ag Cl Radiation=MoKa Lambda=0.7107 Filter=Zr Calibration= 2T=28.309-82.435 I/Ic(RIR)= Ref: Schock, Jamieson. J. Phys. Chem. Solids, v30 p1527 (1969) Hexagonal - Powder Diffraction, P3121 (152) Z=3 mp= CELL: 4.06 x 4.06 x 7.02 <90.0 x 90.0 x 120.0> P.S=hP6 (Cinnabar, Hg S) Density(c)=7.120 Density(m)=4.91A Mwt=143.32 Vol=100.21 F(10)=5.6(0.081,22/1) Ref: Ibid. Strong Lines: 2.48/X 2.03/6 3.15/5 1.41/5 1.30/5 2.29/4 1.70/4 2.83/2 1.57/2 1.17/2 NOTE: 1 High-pressure Ag line coincides. *Boron impurity. High pressure. Stable from 70-90 kbar to highest loads achieved (somewhat less than 150 kbar). 2-Theta d(?) I(f) ( h k l ) Theta 1/(2d) 2pi/d n^2 28.309 3.1500 50.0 ( 1 0 1) 14.154 0.1587 1.9947 31.566 2.8320 20.0 15.783 0.1766 2.2186 36.160 2.4820 100.0 ( 1 0 2) 18.080 0.2015 2.5315 39.347 2.2880 40.0 ( 0 0 3) 19.674 0.2185 2.7461 44.599 2.0300 60.0 ( 1 1 0) 22.300 0.2463 3.0952 53.818 1.7020 40.0 ( 2 0 1) 26.909 0.2938 3.6916 58.846 1.5680 20.0 ( 1 0 4) 29.423 0.3189 4.0071 66.227 1.4100 50.0 ( 2 0 3) 33.113 0.3546 4.4562 72.673 1.3000 50.0 ( 1 0 5) 36.336 0.3846 4.8332 76.807 1.2400 10.0 ( 2 0 4) 38.403 0.4032 5.0671 82.435 1.1690 20.0 ( 0 0 6) 41.218 0.4277 5.3748 |
鐵蟲 (初入文壇)
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鐵蟲 (初入文壇)
鐵蟲 (初入文壇)
木蟲 (著名寫手)
有木有蟲
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本帖內(nèi)容被屏蔽 |
木蟲 (著名寫手)
有木有蟲
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指導(dǎo)一下你自己做吧: 1. 啟動(dòng)Origin(不需要告訴你有幾個(gè)版本或用哪個(gè)版本吧?); 2. 選擇或新建一個(gè)工作簿(你懂的?); 3. 選擇一數(shù)據(jù)欄(比如A)輸入2theta值(或d值),選擇另一數(shù)據(jù)欄(比如B)輸入I值; 4. 雙擊欄名A,在彈出框Options項(xiàng)中Plot Designation選擇X、Format選擇Numeric或Text&Numeric; 5. 雙擊欄名B,在彈出框Options項(xiàng)中Plot Designation選擇Y、Format選擇Numeric或Text&Numeric; 6. 選定數(shù)據(jù)欄A和B,在Plot菜單下Symbol項(xiàng)選擇Scatter,作出散點(diǎn)圖; 7. 雙擊散點(diǎn)圖中任一散點(diǎn),在彈出框右側(cè)Drop Lines界面上鉤選ertical,如果你不喜歡線頂?shù)姆?hào),可以在Symbol界面選擇更換或隱去,OK。 如果你嫌強(qiáng)度太低或太高,可以在I值數(shù)據(jù)欄乘一比例系數(shù);如果你不喜歡線譜,可以函數(shù)擬峰(希望你都會(huì))。 |
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