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[交流]
Nb2O5xrd的表征問題
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一個審稿意見:In the XRD section, could the authors comment on the board peak at ~30 degrees? It appears to the reviewer that the crystallnity of the hierarchical structure is somehow low without proper post-annealing process. A significant part of the structure might be still amorphous or hydrated. In addition, the dominant crystal structure appears to be more like pseudo-hexagonal rather than orthorhombic although both structures have very similar XRD diffraction patterns. The authors should do more detail analysis and clarify the difference from pseudo-hexagonal structure. 我想問一下,對于較寬的峰,除了歸結(jié)于晶體粒徑小以外,是否有別的解釋;另外,這個pseudo-hexagonal(偽六角)該怎么解釋,我在jade中只能找到hexagonal,pseudo-hexagonal和hexagonal是一回事嗎,差別是什么?謝謝 |
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