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巴拉熊_新蟲 (初入文壇)
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[求助]
投稿ACTAE,檢測沒有AB錯(cuò)誤,上傳FCF出現(xiàn)了錯(cuò)誤!急急急求指導(dǎo)修改! 已有2人參與
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投稿之前檢測過,沒有AB類錯(cuò)誤。上傳FCF文件之后,出現(xiàn)以下錯(cuò)誤,求指導(dǎo)修改! Alert level B Crystal system given = triclinic PLAT921_ALERT_1_B R1 in the CIF and FCF Differ by ............... -0.0136 Check PLAT922_ALERT_1_B wR2 in the CIF and FCF Differ by ............... -0.0346 Check PLAT934_ALERT_3_B Number of (Iobs-Icalc)/SigmaW > 10 Outliers .... 3 Check Alert level C PLAT761_ALERT_1_C CIF Contains no X-H Bonds ...................... Please Check PLAT762_ALERT_1_C CIF Contains no X-Y-H or H-Y-H Angles .......... Please Check PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 6 Why ? PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 2 Why ? PLAT923_ALERT_1_C S values in the CIF and FCF Differ by ....... -0.375 Check PLAT926_ALERT_1_C Reported and Calculated R1 Differ by ......... -0.0022 Check PLAT927_ALERT_1_C Reported and Calculated wR2 Differ by ......... -0.0033 Check Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! PLAT164_ALERT_4_G Nr. of Refined C-H H-Atoms in Heavy-Atom Struct. 14 Note PLAT199_ALERT_1_G Reported _cell_measurement_temperature ..... (K) 293 Check PLAT200_ALERT_1_G Reported _diffrn_ambient_temperature ..... (K) 293 Check PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 985 Note PLAT982_ALERT_1_G The Zn-f'= 0.312 Deviates from the IT-value 0.284 PLAT983_ALERT_1_G The Zn-f"= 1.467 Deviates from the IT-Value 1.430 |
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