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[求助]
合成的一個(gè)化合物,希望大家?guī)椭馕鲆幌? 已有4人參與
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非常感謝大家的幫助,元素CHONSi![]() |

鐵桿木蟲 (正式寫手)

鐵桿木蟲 (正式寫手)
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新手練習(xí), 僅供參考. The report of checkCIF, Alert level A EXPT009_ALERT_1_A No crystal dimensions have been given. The following tests will not be performed. CRYSS_01,CRYSS_02 EXPT108_ALERT_1_A The magnitudes of the crystal dimensions do not match the min, mid and max definitions Alert level B Crystal system given = monoclinic PLAT019_ALERT_1_B _diffrn_measured_fraction_theta_full/_max < 1.0 0.884 Report PLAT242_ALERT_2_B Low Ueq as Compared to Neighbors for ..... Si1 Check Alert level C RFACG01_ALERT_3_C The value of the R factor is > 0.10 R factor given 0.101 RFACR01_ALERT_3_C The value of the weighted R factor is > 0.25 Weighted R factor given 0.334 THETM01_ALERT_3_C The value of sine(theta_max)/wavelength is less than 0.590 Calculated sin(theta_max)/wavelength = 0.5762 PLAT053_ALERT_1_C Minimum Crystal Dimension Missing (or Error) ... Please Check PLAT054_ALERT_1_C Medium Crystal Dimension Missing (or Error) ... Please Check PLAT055_ALERT_1_C Maximum Crystal Dimension Missing (or Error) ... Please Check PLAT084_ALERT_3_C High wR2 Value (i.e. > 0.25) ................... 0.33 Report PLAT094_ALERT_2_C Ratio of Maximum / Minimum Residual Density .... 2.51 Report PLAT220_ALERT_2_C Large Non-Solvent C Ueq(max)/Ueq(min) Range 3.6 Ratio PLAT230_ALERT_2_C Hirshfeld Test Diff for O1 -- C5 .. 6.0 su PLAT241_ALERT_2_C High Ueq as Compared to Neighbors for ..... C14 Check PLAT242_ALERT_2_C Low Ueq as Compared to Neighbors for ..... C13 Check PLAT340_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0051 Ang. A 類錯(cuò)誤, 是因?yàn)槟愕男畔⑷笔? 一般解析者, 隨意填個(gè)Size數(shù)據(jù)也可. B類錯(cuò)誤, 參見此帖 http://www.gaoyang168.com/bbs/viewthread.php?tid=5870913&fpage=1&target=blank 盲解相當(dāng)費(fèi)時(shí)的, 需要一點(diǎn)點(diǎn)嘗試. 希望樓主以后求助的話, 上結(jié)構(gòu)吧. |






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