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ly_tryh鐵桿木蟲 (著名寫手)
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[求助]
解譜求助（只有碳譜），謝謝了。 已有2人參與
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像是不飽和脂肪酸甘油酯，但是查文獻和常見的哪幾種（油酸、亞油酸、棕櫚酸等）數(shù)據(jù)對不上，感覺像是有雜質(zhì)（不知道雜質(zhì)是不是三萜，16.2,16.4,17.9,18.0,18.2,19.3,19.3,21.2,23.3,23.8,26.0,27.8,31.0,31.5,32.1,36.6,37.9,38.0,38.3,40.6,42.1,42.4,45.3,53.3,55.0,60.7等，有的標(biāo)圖上了），但是判斷不清那些是有用的。 特別是比較迷惑的116.5的信號。還有就是為什么羰基信號那么低？ 沒有思路啊，急求各位解譜高手幫忙啊。 Document 1_副本.jpg |
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4樓2014-08-14 17:29:14
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ly_tryh: 金幣+5, ★有幫助, 謝謝，不過想解的是主要物質(zhì)。 2014-08-11 08:41:33
ly_tryh: 金幣+5, ★有幫助, 謝謝，不過想解的是主要物質(zhì)。 2014-08-11 08:41:33
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???????????鵽12010????????(???????????ο?) -------------------------------------------------------------------------------- 1 . 3??,13??-Dihydroxy-urs-11-en-28-oic acid ?????:85.1% Journal of Shenyang Pharmaceutical University 2012 29 22-25 Isolation and identification of chemical constituents from whole plant of Polygonum hydropiper L. HUANG Jian; HOU Peng-yi; WU Li-jun; GAO Hui-yuan Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 2 . camaldulin C31H46O4 ?????:80.6% Journal of Natural Products 2000 63 1265-1268 Spasmolytic Constituents from Eucalyptus camaldulensis var. obtusa Leaves Sabira Begum,Farhat, Ishrat Sultana, Bina S. Siddiqui, Farhana Shaheen, and Anwar H. Gilani Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 3 . 11,12-dehydroursolic lactone acetate C32H48O4 ?????:80.6% Agricultural and Biological Chemistry 1984 48 373-376 Germination Inhibitor from Eucalyptus pulverulenta Matthew L. BOLTE, Jenny BOWERS, Wilfrid D. CROW, Dugald M. PATON, Akira SAKURAI, Nobutaka TAKAHASHI, Masami UJIIE, Shigeo YOSHIDA Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 4 . compound 2 ?????:80% Acta Pharmaceutica Sinica 1996 31 437-440 STRUCTURE ELUCIDATION OF LIQUIDAMBARIC LACTONE YR Sun and YF sun Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 5 . 3-hydroxy-11-urs-en-28,13-olide,11,12-dehydroursolic acid lactone ?????:76.6% China Journal of Chinese Materia Medica 2006 31 1434-1436 Studies on triterpenoid from Potentilla chinensis WANG Qinghe, LI Zhiyong, SHEN Yang, LIN Houwen, SHU Wei, ZHOU Jianbin Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 6 . 3??,13??-dihydroxy-urs-11-en-28-oic acid C30H48O4 ?????:76.6% Phytochemistry 1996 42 1665-1666 Two diterpenoids from copaiba oile Honore Monti, Nicolas Tiliacos, Robert Faur Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 7 . ursolic acid lactone ?????:76.6% Phytochemistry 1993 33 151-153 Triterpene esters from Eucalyptus tereticornis Wang Hongcheng, Yasuo Fujimotot Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 8 . 3??-hydroxy-urs-11-en-28,13-lactone ?????:76.6% Chemical & Pharmaceutical Bulletin 2011 59(9) 1180-1182 Biotransformation of Ursolic Acid by an Endophytic Fungus from Medicinal Plant Huperzia serrata Shao-bin FU, Jun-shan YANG, Jin-long CUI, Xu FENG, and Di-an SUN Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 9 . ursolic acid lactone C30H46O3 ?????:76.6% Chinese Traditional and Herbal Drugs 2009 40 1036-1039 ?????????????о? ??????;?θ???;?????? Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 10 . 11,12-dehydroursolic acid lactone C30H46O3 ?????:76.6% Natural Product Research and Development 2007 19 232-234 Pentacyclic Triterpenes from Eucalyptus globulus Labill.Fruits TAN Man-liang;WANG Ye; ZHOU Li-gang; JIANG Wei-bo Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 11 . 3??-hydroxy-urs-11-en-28,13??-olide ?????:76.6% Phytochemistry Letters 2011 4 432-435 Insecticidal activity of Tanacetum chiliophyllum (Fisch. & Mey.) var. monocephalum grierson extracts and a new sesquiterpene lactone Kaan Polatoğlu, Ömer Cem Karakoç, Ayhan Gökçe, Nezhun Gören Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 12 . 3??,13??-dihydroxy-urs-11-en-28-oic acid-13-lactone C30H46O3 ?????:76.6% Chinese Journal of Oceanology and Limnology 2009 27 288-296 Chemical constituents of marine medicinal mangrove plant Sonneratia caseolaris TIAN Minqing, DAI Haofu, LI Xiaoming, WANG Bingui Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 13 . 3??-hydroxyurs-11-en-13??,28-olide ?????:76.6% The Chinese Pharmaceutical Journal 2000 52 69-77 Constituents of the Leaves of Erythrina arborescens ?S???(Keh-Feng Huang), ?????(Ping-Chuan Tseng), ????O(Ling-Ping Wu), ??????(Shiow-Ling Liou) Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 14 . 3??-hydroxy-urs-11-en-28,13??-olide ?????:76.6% Phytochemistry Letters 2011 4 421-425 Ovarian antiproliferative activity directed isolation of triterpenoids from fruits of Eucalyptus camaldulensis Dehnh G??laçtı Topçu, Gön??l Yapar, Zeynep T??rkmen, Ahmet Ceyhan Gören, Sevil Öks??z, Jennifer K. Schilling, David G.I. Kingston Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 15 . 3??-hydroxy-urs-11-en-13??(28)-olide C30H46O3 ?????:76.6% Chinese Traditional and Herbal Drugs 2012 43 444-447 Chemical constituents from leaves of Ilex cornuta ZHOU Si-xiang; YAO Zhi-rong; LI Jun; TU Peng-fei Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 16 . 3??-hydroxyurs-28,13-olide ?????:73.3% Chemical & Pharmaceutical Bulletin 1983 31 1567-1571 Triterpenoids of the Bark of Pieris japonica D. DON (Japanese Name : Asebi). II. 13C Nuclear Magnetic Resonance of the ??-Lactones of Ursane- and Oleanane-type Triterpenes MASAAKI KATAI,TADAMASA TERAI and HARUO MEGURI Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 17 . 3??,13??-?????-????-11-?-28-???? ?????:73.3% Chinese Traditional and Herbal Drugs 2011 42(4) 661-663 Chemical constituents of Paederia scandens YU Xiao-yan Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 18 . 11,12-dehydroursolic acid lactone ?????:73.3% Journal of Shenyang Pharmaceutical University 2011 28 260-262 Isolation and identification of chemical constituents of flower of Lomatogonium rotatum (L.) Fries ex Nym(2) JIA Ling-yun, YUAN Jiu-zhi, SUN Qi-shi Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 19 . ursolic acid lactone ?????:73.3% Journal of Shenyang Pharmaceutical University 2005 22 81-109 Isolation and identification of the chemical constituents of Verbena officinalis L1 ZI Jia-chen, LI Yu-shan, LIU Xing-guo, Tohru YAMAKUNI, Yasushi OHIZUMI Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 20 . 3-??-hydroxy-urs-11-en-28,13-olide ?????:73.3% Journal of the Chinese Chemical Society 1993 40 87-91 Constituents of Clinopodium umbrosum ??????(Shu-Mei Lee);????(Jeng-Shiow Lai);??????(Yueh-Hsiung Kuo) Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 21 . ilelatifol D C30H46O4 ?????:73.3% Phytotherapy Research 2007 21 558-561 Ursolic acid: a potent Inhibitor of superoxides produced in the cellular system Muhammad S. Ali, Syed A. Ibrahim, Saima Jalil and Muhammad I. Choudhary Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 22 . 3??-hydroxy-urs-11-en-28,13??-olide ?????:73.3% Chemistry of Natural Compounds 2013 49 381-382 Phytochemical constituents of Comastoma pedunculatum Li Tang, Xiao-Ming Xu, Ying Liu, Yi-Run Wang, Chun-Lin Long, Jin-Chao Feng Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 23 . 3??-hydroxyurs-11??,12??-epoxy-13??,28-olide ?????:73.3% The Chinese Pharmaceutical Journal 2000 52 69-77 Constituents of the Leaves of Erythrina arborescens ?S???(Keh-Feng Huang), ?????(Ping-Chuan Tseng), ????O(Ling-Ping Wu), ??????(Shiow-Ling Liou) Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 24 . 3??,13??-dihydroxyurs-11-en-28-oic acid ?????:73.3% Molecules 2014 19 9515-9534 Studies on Cytotoxic Constituents from the Leaves of Elaeagnus oldhamii Maxim. in Non-Small Cell Lung Cancer A549 Cells Chi-Ren Liao, Yueh-Hsiung Kuo, Yu-Ling Ho, Ching-Ying Wang, Chang -Syun Yang, Cheng-Wen Lin and Yuan-Shiun Chang Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 25 . 3??-Hydroxyurs-11-en-13??(28)-olide ?????:73.0% Phytochemical Analysis 2005 16 364-369 Chemical composition of the epicuticular wax from the fruits of Eucalyptus globulus Susana I. Pereira, Carmen S. R. Freire, Carlos Pascoal Neto, Armando J. D. Silvestre and Artur M. S. Silva Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 26 . ursolic acid ?????:73.0% Journal of Shenyang Pharmaceutical University 2010 27 113-115 Isolation and identification of chemical constituents from stems and leaves of Quercus variabilis Blume XIN Yan, LI Qian, JIA Ling-yun, YUAN Jiu-zhi, SUN Qi-shi Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 27 . 28-nor-urs-12-ene-3??, 17??-diol C29H48O2 ?????:72.4% Phytochemistry 2005 66 627-632 Cladocalol, a pentacyclic 28-nor-triterpene from Eucalyptus cladocalyx with cytotoxic activity Samira Benyahia, Samir Benayache, Fadila Benayache, Francisco Le??n,Jos?? Quintana, Mat??as L??pez, Juan C. Hern??ndez,Francisco Est??vez, Jaime Bermejo Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 28 . 28-no??-urs-12-ene-3??,17??-diol C29H48O2 ?????:72.4% Journal of Natural Products 2006 69 1164-1167 Taraxasterane- and Ursane-Type Triterpenes from Nerium oleander and Their Biological Activities Ming Zhao, Shujun Zhang, Liwei Fu, Na Li, Jiao Bai, Junichi Sakai, Liyan Wang, Wanxia Tang, Toshiaki Hasegawa, Hirotsugu Ogura, Takao Kataoka, Seiko Oka, Miwa Kiuch, Katutoshi Hirose, and Masayoshi Ando Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 29 . (3??,18??,20??)-3-acetoxy-N-hydroxy-11-oxo-olean-12-en-29-amide ?????:70.9% Bioorganic & Medicinal Chemistry 2010 18 7522-7541 Synthesis of novel 3-amino and 29-hydroxamic acid derivatives of glycyrrhetinic acid as selective 11??-hydroxysteroid dehydrogenase 2 inhibitors Christian Stanetty, Laszlo Czollner, Iris Koller, Priti Shah, Rawindra Gaware, Thierry Da Cunha, Alex Odermatt, Ulrich Jordis, Paul Kosma, Dirk Claßen-Houben Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 30 . uvaol ?????:70.3% Modern Chinese Medicine 2011 13(1) 23-25 Isolation and Identification of Chemical Constituents from RosmarinusOfficinalis L1 WANG Hui, , GAO Hui-yuan, ZHANG Zhen-qiu, WULi-jun Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 31 . 3-acetoxy oleanolic acid ?????:70.3% Journal of Shenyang Pharmaceutical University 2011 28 417-419 Isolation and identification of chemical constituents from stems of Stauntonia brachyanthera Hand. - Mazz. CHEN Chao, LI Zhen-xing, MENG Da-li, LI Ning, LI Xian Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 32 . phyllolactone E C27H42O4 ?????:70.3% Tetrahedron 2001 57 5731-5738 Phyllolactones A-E: new bishomoscalarane sesterterpenes from the marine sponge Phyllospongia lamellosa Leng Chee Chang, Sarah Otero-Quintero, Gillian M Nicholas, Carole A Bewley Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 33 . 3-epi-corosolic acid lactone C30H46O4 ?????:70% Journal of Natural Products 2003 66 1051-1054 Ursane- and Oleanane-Type Triterpenes from Ternstroemia gymnanthera Callus Tissues Akira Ikuta,Hiroaki Tomiyasu,Yasumasa Morita,and Kouichi Yoshimura Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 34 . ardipusilloside I C53H36O22 ?????:70% Acta Pharmaceutica Sinica 1993 28 673-678 STUDIES ON THE SAPONIN CONSTITUENTS OF JIU JIELONG (ARDISIA PUSILLA) QH Zhang; XJ Wang; ZC Miao and R Feng Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 35 . 3??-hydroxy-11??,12??-epoxy-urs-13??,28-olide C30H46O4 ?????:70% Journal of Natural Products 1993 Vol 56 613 Constituents of the Leaves of Thevetia neriifolia Sabira Begum, Qayyum Adil, Bina S. Siddiqui, Salimuzzaman Siddiqui Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 36 . 3-keto-13(28)-epoxy-ursan-11-ene C30H46O2 ?????:70% Phytochemistry 1990 29 1691-1693 Terpenoids from Salvia mellifera Antonio G. Gonz??lez,Lucia S. Andres,Angel G. Ravelo,Javier G. Luis,Isabel L. Bazzocchi,Jan West Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 37 . 2??,3??-dihydroxy-11??,12??-epoxy-urs-28,13??-olide C30H46O5 ?????:70% Journal of Asian Natural Products Research 2013 15 962-968 Three new ursane-type triterpenoids from the aerial parts of Isodon excisoides Ke Jiao, Huo-Yun Li, Peng Zhang, Hui-Fang Pi, Han-Li Ruan & Ji-Zhou Wu Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 38 . ferna-9(11)-en-19a-ol ?????:70% Natural Medicines 1998 52 409-413 Pharmacognostical Studies on "Ku-tui-po" III. : Constituents of the Rhizomes of Davallia solida Tanaka Yasuko,Kitajima Jun-ichi,Ageta Hiroyuki Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 39 . ilelatifol D ?????:70% Natural Medicines 2000 54 297-305 Acyl-CoA : Cholesterol Acyltransferase(ACAT) Inhibitors from Ilex spp. Nishimura Keiichi,Miyase Toshio,Noguchi Hiroshi,Chen Xin-Min Structure 13C NMR Structure & 13C NMR ??????? -------------------------------------------------------------------------------- 40 . 13??-???-11-?-????? ?????:70% Natural Product Research and Development 2013 25 345-348 Studies on the Chemical Constituents from Sambucus adnata Wall WU Hai-bo, ZHAO Yi-ning, LI Dong-mei, LV Xiang-wen, WANG Wen-shu Structure 13C NMR Structure & 13C NMR ??????? |
2樓2014-08-08 21:29:48
ly_tryh
鐵桿木蟲 (著名寫手)
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3樓2014-08-13 12:24:51
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