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| A stainless steel milling vial was loaded in a glovebox under nitrogen atmosphere with approximately 1.0 g of non-spherical millimeter-sized flakes of bulk aluminum and 25 mL of valeraldehyde. Stainless steel milling balls were added to the vial, which was then sealed and placed in the high-energy ball mill. After HEBM,the supernatant liquid was removed from the vial and centrifuged,removing any suspended aluminum particles. |
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