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紫彤3251木蟲(chóng) (小有名氣)
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[求助]
有關(guān)審稿人對(duì)XRD的問(wèn)題 及回復(fù) 已有6人參與
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我的論文大修后小修,然后審稿人提出了一個(gè)問(wèn)題 ,回復(fù)如下 - In page 12, line 18 - “Smaller unit-cell volume is favorable to improve electrochemical capability of the electrode” How can authors explain this? Only if when unit-cell volume is smaller, the crystallites are also smaller and lead to an increase of catalytic surface; have authors verified that, in the SEM images of the different films? If authors have an explanation for the fact of the film 4% has lower unit cell volume than the 2% and 8% films, perhaps, that could explain why 4% film is the best. 我在文章中是計(jì)算了晶胞體積,然后說(shuō)體積小催化性能好,我覺(jué)得審稿人的意思是 體積小,并且晶粒尺寸也小才能證明催化活性好,但是他說(shuō)用SEM看出,我不太懂,SEM能直接看出晶粒尺寸么?? 而且我們做的方法的sem圖是類似平面皸裂狀,并不是一般的納米球等等,這怎么看晶粒尺寸呢?? 所以我想用謝樂(lè)公式算,但是我的XRD峰較寬,結(jié)晶度一般,所以用jade軟件給出一堆值有的>1000等等 這個(gè)我不太明白, 請(qǐng)大家?guī)兔匆幌拢魑慌H酥更c(diǎn)一下!~~~謝啦!!第一篇文章,無(wú)比緊張! |

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木蟲(chóng) (小有名氣)
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