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截止晚10點(diǎn) The test solution was deaerated with oxygen free nitrogen (OFN) before charging into the autoclave vessel. The dissolved oxygen content was measured by a Hamilton optical oxygen meter following purging and found to be less than 5ppb. All the lines to the autoclave from the deaeration vessel were purged with nitrogen and evacuated. The test solutions were transferred to the autoclaves under pressure of OFN and purged with OFN in the autoclave for a further 30 minutes. The quantity of solution transferred to each autoclave was sufficient to give a ratio of approximately 20ml/cm2 of specimen surface area. |
至尊木蟲 (知名作家)
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| 測試溶液在充入高壓釜容器之前先用無氧氮?dú)猓∣FN)進(jìn)行脫氣(排除空氣)。驅(qū)氣后用一漢密爾頓光氧計(jì)測定溶解的氧含量,結(jié)果低于5ppb。從脫氣容器到高壓釜的所有通道都用氮?dú)怛?qū)氣,并抽真空。在無氧氮?dú)鈮毫ο罗D(zhuǎn)移測試溶液到高壓釜中,并用OFN在高壓釜另外驅(qū)氣30分鐘。溶液轉(zhuǎn)移到每個(gè)高壓釜的量足夠多,以得到約為20毫升/cm2樣品表面積的比率。 |
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