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全是愛1991新蟲 (小有名氣)
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[求助]
哪位有BiOI的XRD JCPDS No. 73-2062 這個(gè)標(biāo)準(zhǔn)的數(shù)據(jù)啊,急需,謝謝! 已有2人參與
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| 如果有其他的BiOI的標(biāo)準(zhǔn)卡,也可以提供給我,萬分感謝! |
木蟲 (著名寫手)
有木有蟲
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Card Information Names: Bismuth Oxide Iodide Formula: Bi O I PDF Number: 73-2062 Quality: calculated Subfiles: inorganic FIZ Cell and Symmetry Information System: tetragonal Space Group: P4/nmm (no. 129) a: 3.98400 c: 9.12800 Density (Dx): 8.064 Z: 2 Instrument Information Radiation: CuKa1 Wavelength: 1.54060 Instrument(d): calculated Cut Off: 17.7 Instrument(I): calculated I type: peak heights I/Icor: 8.86 Comments and Additional Information ICSD Number: 024610 SD ICSD SG: P4/NMMS1 IT # is: 129 SG short form: P4/nmm TT No R value given. TT At least one TF missing. TI X-ray studies on Bi O Cl, Bi O Br and Bi O I WY c2 a (P4/NMMS1) AF AXY Literature References General: Calculated from ICSD using POWD-12++ (1997) Structure: Sillen, L.G. Sven. Kem. Tidskr. 53 39 (1941) Peak Data PeakList h k l d I 0 0 1 9.1280 370 0 0 2 4.5640 37 0 1 1 3.6517 21 0 1 2 3.0015 999 1 1 0 2.8173 419 1 1 1 2.6920 22 0 1 3 2.4182 85 1 1 2 2.3973 54 0 0 4 2.2820 65 1 1 3 2.0672 7 0 2 0 1.9922 165 0 1 4 1.9802 65 0 2 1 1.9464 21 2 0 2 1.8256 23 0 0 5 1.8256 23 1 1 4 1.7732 135 1 2 1 1.7488 6 1 2 2 1.6598 276 1 2 3 1.5376 34 1 1 5 1.5321 41 0 0 6 1.5213 10 0 2 4 1.5008 56 0 1 6 1.4213 27 2 2 0 1.4086 43 1 2 4 1.4044 46 2 2 1 1.3922 6 0 2 5 1.3459 19 1 1 6 1.3386 17 0 3 1 1.3143 1 0 0 7 1.3040 2 0 3 2 1.2752 49 1 3 0 1.2600 45 1 3 1 1.2481 4 0 1 7 1.2393 18 0 3 3 1.2172 7 1 3 2 1.2145 10 0 2 6 1.2091 14 2 2 4 1.1987 22 1 1 7 1.1834 4 1 3 3 1.1641 2 1 2 6 1.1570 22 0 3 4 1.1479 7 0 0 8 1.1410 1 2 2 5 1.1152 7 1 3 4 1.1030 37 0 1 8 1.0969 9 0 2 7 1.0911 5 |
木蟲 (著名寫手)
有木有蟲
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首選應(yīng)該是這個(gè)卡片: Card Information Names: Bismuth Oxide Iodide Formula: Bi O I PDF Number: 10-445 Quality: star Subfiles: inorganic CP NBS Cell and Symmetry Information System: tetragonal Space Group: P4/nmm (no. 129) a: 3.994 c: 9.149 Density (Dx): 8.006 Z: 2 Instrument Information Radiation: CuKa1 Wavelength: 1.5405 Filter: Ni Instrument(d): unknown Instrument(I): diffractometer I type: unknown Comments and Additional Information Preparation: Sample prepared at NBS, Gaithersburg, Maryland, USA, by reacting Bi2 O3 with concentrated HI. General: Pattern was improved by heating the material in air for two hours at 450 C. Analysis: Spectrographic analysis showed <0.1% Ni; <0.01% Al, Co, Fe, Si. Temperature: Pattern taken at 25 C. Colour: Dark red-orange Lines: Plus 19 additional reflections to 0.9414. Literature References General: Natl. Bur. Stand. (U.S.), Circ. 539 9 16 (1960) Peak Data PeakList h k l d I 0 0 1 9.1500 20 0 0 2 4.5800 8 1 0 1 3.6610 4 1 0 2 3.0110 100 1 1 0 2.8240 55 1 1 1 2.6990 4 1 0 3 2.4240 12 1 1 2 2.4030 8 0 0 4 2.2870 10 1 1 3 2.0720 4 2 0 0 1.9970 25 1 0 4 1.9850 12 2 0 1 1.9520 4 0 0 5 1.8290 4 1 1 4 1.7780 16 2 1 2 1.6640 30 2 1 3 1.5410 8 1 1 5 1.5359 4 0 0 6 1.5246 4 2 0 4 1.5045 8 1 0 6 1.4244 6 2 2 0 1.4120 8 2 1 4 1.4078 6 2 2 1 1.3957 1 2 2 2 1.3495 6 1 1 6 1.3422 6 0 0 7 1.3073 2 3 0 2 1.2786 4 3 1 0 1.2634 4 1 0 7 1.2424 4 3 0 3 1.2200 1 3 1 2 1.2176 4 2 0 6 1.2121 1 2 2 4 1.2017 4 1 1 7 1.1860 2 2 1 6 1.1597 2 3 0 4 1.1502 1 0 0 8 1.1436 1 2 2 5 1.1181 1 |
新蟲 (小有名氣)
新蟲 (小有名氣)
至尊木蟲 (小有名氣)
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PDF#73-2062: QM=Calculated(C); d=Calculated; I=Calculated Bismuth Oxide Iodide Bi O I Radiation=CuKa1 Lambda=1.54060 Filter= Calibration= 2T=9.681-89.820 I/Ic(RIR)=8.86 Ref: Calculated from ICSD using POWD-12++ (1997) Tetragonal - (Unknown), P4/nmm (129) Z=2 mp= CELL: 3.984 x 3.984 x 9.128 <90.0 x 90.0 x 90.0> P.S=tP6 (?) Density(c)=8.064 Density(m)=7.17A Mwt=351.88 Vol=144.88 F(30)=326.4(.0025,37/0) Ref: Sillen, L.G. Sven. Kem. Tidskr., v53 p39 (1941) Strong Lines: 3.00/X 2.82/4 9.13/4 1.66/3 1.99/2 1.77/1 2.42/1 2.28/1 1.98/1 1.50/1 FIZ=024610: ICSD SG: P4/NMMS1 IT is: 129 SG short form: P4/nmm No R value given. At least one TF missing. X-ray studies on Bi O Cl, Bi O Br and Bi O I c2 a (P4/NMMS1) AXY 2-Theta d(?) I(f) ( h k l ) Theta 1/(2d) 2pi/d n^2 9.681 9.1280 37.0 ( 0 0 1) 4.841 0.0548 0.6883 19.433 4.5640 3.7 ( 0 0 2) 9.716 0.1096 1.3767 24.355 3.6517 2.1 ( 0 1 1) 12.177 0.1369 1.7206 29.740 3.0015 100.0 ( 0 1 2) 14.870 0.1666 2.0933 31.735 2.8173 41.9 ( 1 1 0) 15.868 0.1775 2.2303 33.254 2.6920 2.2 ( 1 1 1) 16.627 0.1857 2.3341 37.149 2.4182 8.5 ( 0 1 3) 18.574 0.2068 2.5983 37.484 2.3973 5.4 ( 1 1 2) 18.742 0.2086 2.6209 39.455 2.2820 6.5 ( 0 0 4) 19.727 0.2191 2.7534 43.755 2.0672 0.7 ( 1 1 3) 21.877 0.2419 3.0395 45.492 1.9922 16.5 ( 0 2 0) 22.746 0.2510 3.1539 45.783 1.9802 6.5 ( 0 1 4) 22.891 0.2525 3.1730 46.626 1.9464 2.1 ( 0 2 1) 23.313 0.2569 3.2281 49.913 1.8256 2.3 ( 0 0 5) 24.957 0.2739 3.4417 49.913 1.8256 2.3 ( 2 0 2) 24.957 0.2739 3.4417 51.493 1.7732 13.5 ( 1 1 4) 25.746 0.2820 3.5433 52.266 1.7488 0.6 ( 1 2 1) 26.133 0.2859 3.5928 55.300 1.6598 27.6 ( 1 2 2) 27.650 0.3012 3.7854 60.128 1.5376 3.4 ( 1 2 3) 30.064 0.3252 4.0864 60.367 1.5321 4.1 ( 1 1 5) 30.184 0.3264 4.1011 60.838 1.5213 1.0 ( 0 0 6) 30.419 0.3287 4.1301 61.762 1.5008 5.6 ( 0 2 4) 30.881 0.3332 4.1866 65.636 1.4213 2.7 ( 0 1 6) 32.818 0.3518 4.4209 66.299 1.4086 4.3 ( 2 2 0) 33.150 0.3550 4.4605 66.524 1.4044 4.6 ( 1 2 4) 33.262 0.3560 4.4739 67.188 1.3922 0.6 ( 2 2 1) 33.594 0.3592 4.5133 69.821 1.3459 1.9 ( 0 2 5) 34.911 0.3715 4.6683 70.259 1.3386 1.7 ( 1 1 6) 35.129 0.3735 4.6937 71.759 1.3143 0.1 ( 0 3 1) 35.879 0.3804 4.7807 72.414 1.3040 0.2 ( 0 0 7) 36.207 0.3834 4.8184 74.318 1.2752 4.9 ( 0 3 2) 37.159 0.3921 4.9271 75.374 1.2600 4.5 ( 1 3 0) 37.687 0.3968 4.9868 76.216 1.2481 0.4 ( 1 3 1) 38.108 0.4006 5.0341 76.857 1.2393 1.8 ( 0 1 7) 38.428 0.4034 5.0699 78.517 1.2172 0.7 ( 0 3 3) 39.258 0.4108 5.1619 78.724 1.2145 1.0 ( 1 3 2) 39.362 0.4117 5.1733 79.147 1.2091 1.4 ( 0 2 6) 39.574 0.4135 5.1966 79.975 1.1987 2.2 ( 2 2 4) 39.987 0.4171 5.2418 81.221 1.1834 0.4 ( 1 1 7) 40.611 0.4225 5.3095 82.859 1.1641 0.2 ( 1 3 3) 41.429 0.4295 5.3975 83.482 1.1570 2.2 ( 1 2 6) 41.741 0.4322 5.4306 84.296 1.1479 0.7 ( 0 3 4) 42.148 0.4356 5.4737 84.923 1.1410 0.1 ( 0 0 8) 42.461 0.4382 5.5067 87.369 1.1152 0.7 ( 2 2 5) 43.684 0.4483 5.6339 88.589 1.1030 3.7 ( 1 3 4) 44.294 0.4533 5.6964 89.212 1.0969 0.9 ( 0 1 8) 44.606 0.4558 5.7281 89.820 1.0911 0.5 ( 0 2 7) 44.910 0.4583 5.7588 |

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