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sunny熙夏新蟲 (初入文壇)
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[求助]
求助粉末衍射數(shù)據(jù)庫(JCPDS)中的Zn(AC)2和Zn(NO3)2卡片數(shù)據(jù) 已有1人參與
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| 求助粉末衍射數(shù)據(jù)庫(JCPDS)中的乙酸鋅和硝酸鋅卡片數(shù)據(jù) |
木蟲 (著名寫手)
有木有蟲
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Name and formula Reference code: 00-021-1467 Compound name: Zinc Acetate Empirical formula: C4H6O4Zn Chemical formula: C4H6O4Zn Crystallographic parameters Crystal system: Tetragonal a (?): 11.1300 b (?): 11.1300 c (?): 10.9500 Alpha (°): 90.0000 Beta (°): 90.0000 Gamma (°): 90.0000 Volume of cell (10^6 pm^3): 1356.45 RIR: - Subfiles and quality Subfiles: Forensic Inorganic Organic Quality: Blank (B) Comments Creation Date: 1970/1/1 Modification Date: 1970/1/1 References Primary reference: Djega, Mariadasson, Kerloub., C. R. Seances Acad. Sci., Ser. C, 264, 1753, (1967) Peak list No. h k l d [A] 2Theta[deg] I [%] 1 1 1 0 7.85000 11.263 100.0 2 2 0 0 5.57000 15.898 12.0 3 2 1 1 4.54000 19.537 55.0 4 1 1 2 4.52000 19.625 90.0 5 2 2 0 3.94000 22.549 85.0 6 2 0 2 3.91000 22.724 12.0 7 3 1 0 3.52000 25.281 20.0 8 1 0 3 3.46000 25.727 4.0 9 3 2 1 2.97600 30.002 12.0 10 2 1 3 2.94100 30.368 80.0 11 4 0 0 2.77400 32.244 4.0 12 0 0 4 2.73200 32.754 8.0 13 3 0 3 2.61000 34.331 12.0 14 2 0 4 2.46800 36.373 6.0 15 3 3 2 2.36800 37.967 12.0 16 3 2 3 2.34500 38.354 14.0 17 2 2 4 2.23700 40.284 8.0 18 5 0 1 2.18100 41.365 12.0 19 3 1 4 2.15900 41.806 8.0 20 5 1 2 2.02500 44.716 40.0 21 2 1 5 2.00000 45.306 10.0 22 4 0 4 1.94400 46.687 6.0 23 5 3 0 1.90700 47.649 4.0 24 5 0 3 1.90000 47.835 40.0 25 3 0 5 1.88600 48.213 6.0 26 4 2 4 1.84600 49.326 12.0 27 5 2 3 1.79400 50.856 6.0 28 4 4 3 1.73000 52.880 6.0 29 5 3 3 1.69600 54.025 6.0 30 6 2 2 1.67100 54.901 8.0 |
木蟲 (著名寫手)
有木有蟲
新蟲 (初入文壇)
新蟲 (初入文壇)
木蟲 (著名寫手)
有木有蟲
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有3種: 1. Name and formula Reference code: 00-019-1464 Compound name: Zinc Nitrate Hydrate Empirical formula: H12N2O12Zn Chemical formula: Zn ( NO3 )2 ?6H2O Crystallographic parameters Crystal system: Unknown RIR: - Subfiles and quality Subfiles: Corrosion Inorganic Quality: Low precision (O) Comments Creation Date: 1970/1/1 Modification Date: 1970/1/1 Comment: Stable below 19 C. References Primary reference: Weigel, Imelik, Prettre., Bull. Soc. Chim. Fr., 836, (1964) Peak list No. h k l d [A] 2Theta[deg] I [%] 1 7.05000 12.546 60.0 2 5.15000 17.204 100.0 3 4.88000 18.164 30.0 4 4.65000 19.071 90.0 5 3.67000 24.232 60.0 6 3.51000 25.354 60.0 7 3.41000 26.111 70.0 8 3.10000 28.776 30.0 9 2.80000 31.937 20.0 10 2.71000 33.027 30.0 11 2.67000 33.537 30.0 12 2.57000 34.882 60.0 13 2.48000 36.191 30.0 14 2.43000 36.963 20.0 2. Name and formula Reference code: 00-025-1231 Compound name: Zinc Nitrate Hydrate Empirical formula: H12N2O12Zn Chemical formula: Zn ( NO3 )2 ?6H2O Crystallographic parameters Crystal system: Orthorhombic Space group: Pnma Space group number: 62 a (?): 12.3720 b (?): 12.9020 c (?): 6.3020 Alpha (°): 90.0000 Beta (°): 90.0000 Gamma (°): 90.0000 Calculated density (g/cm^3): 1.96 Volume of cell (10^6 pm^3): 1005.95 Z: 4.00 RIR: - Subfiles and quality Subfiles: Common Phase Corrosion Inorganic NBS pattern Quality: Star (S) Comments Color: Colorless Creation Date: 1970/1/1 Modification Date: 1970/1/1 Color: Colorless Additional Patterns: To replace 00-019-1465 Unit Cell: Space group erroneously given as Pn21a (33). Pattern at 25 C. Merck Index, 8th Ed., p. 1129 Sample Preparation: Sample made from aqueous solution at room temperature. This composition inverts at 19 C to the b form. Instability and cleavage make I's subject to error Structures: Compound is isostructural with beta-Co ( NO3 )2 ?6H2O Analysis: Spec anal: 0.01-0.1% Ca, 0.003-0.03% Fe, 0.001-0.01% each Ag, Ba, Cr, Si, Sr. References Primary reference: Natl. Bur. Stand. (U.S.) Monogr. 25, 12, 36, (1975) Unit cell: Ibid., Natl. Bur. Stand. (U.S.) Monogr. 25 Optical data: Ibid., Natl. Bur. Stand. (U.S.) Monogr. 25 Peak list No. h k l d [A] 2Theta[deg] I [%] 1 0 2 0 6.44900 13.720 6.0 2 2 1 0 5.58000 15.870 100.0 3 1 1 1 5.14500 17.221 75.0 4 1 2 1 4.23500 20.960 85.0 5 2 2 1 3.64600 24.394 15.0 6 2 3 0 3.53200 25.194 20.0 7 1 3 1 3.41500 26.072 4.0 8 3 1 1 3.33600 26.701 30.0 9 0 4 0 3.22800 27.611 30.0 10 0 0 2 3.15400 28.273 2.0 11 4 0 0 3.09500 28.823 40.0 12 3 2 1 3.04200 29.336 30.0 13 1 1 2 2.97100 30.054 8.0 14 0 2 2 2.83200 31.566 5.0 15 4 2 0 2.78800 32.078 35.0 16 2 1 2 2.74400 32.607 30.0 17 4 1 1 2.71500 32.965 4.0 18 4 2 1 2.55100 35.151 3.0 19 3 0 2 2.50400 35.833 9.0 20 3 1 2 2.45700 36.542 10.0 21 2 5 0 2.38000 37.768 3.0 22 1 5 1 2.34400 38.371 12.0 23 5 0 1 2.30200 39.099 3.0 24 5 1 1 2.26700 39.728 4.0 25 4 0 2 2.20800 40.836 20.0 26 5 2 1 2.16900 41.604 16.0 27 0 6 0 2.14900 42.010 25.0 28 4 2 2 2.08800 43.298 9.0 29 1 0 3 2.07100 43.671 8.0 30 3 5 1 2.06700 43.760 10.0 31 6 1 0 2.03600 44.462 4.0 32 1 6 1 2.00800 45.116 6.0 33 2 0 3 1.99000 45.547 4.0 34 5 0 2 1.94600 46.636 4.0 3. Name and formula Reference code: 00-046-0596 Compound name: Zinc Nitrate Hydrate Empirical formula: H12N2O12Zn Chemical formula: Zn ( NO3 )2 ?6H2O Crystallographic parameters Crystal system: Tetragonal Space group: P a (?): 12.4400 b (?): 12.4400 c (?): 12.6910 Alpha (°): 90.0000 Beta (°): 90.0000 Gamma (°): 90.0000 Volume of cell (10^6 pm^3): 1963.98 RIR: - Subfiles and quality Subfiles: Corrosion Inorganic Quality: Star (S) Comments Creation Date: 1970/1/1 Modification Date: 1970/1/1 Sample Preparation: Commercial zinc hexaaquonitrate was recrystallized from water, dissolved in acetone, dried and stored in a dessicator. Room temperature phase. References Primary reference: Borzecka-Prokop, B., Kapturkiewicz, E., Weselucha-Birczynska, A., Hodorowicz, S., Cryst. Res. Technol., 25, 1311, (1990) Peak list No. h k l d [A] 2Theta[deg] I [%] 1 1 0 2 5.65500 15.658 1.0 2 2 2 0 4.39800 20.175 1.0 3 3 2 1 3.32700 26.774 70.0 4 4 0 0 3.10900 28.691 20.0 5 1 0 4 3.07400 29.024 100.0 6 3 0 4 2.52200 35.568 1.0 7 4 3 1 2.44400 36.743 18.0 8 5 2 3 2.02900 44.623 20.0 9 4 3 4 1.96000 46.284 1.0 10 4 4 3 1.95100 46.510 1.0 11 6 3 0 1.85400 49.099 3.0 12 6 3 3 1.69700 53.991 4.0 13 4 2 6 1.68300 54.477 1.0 14 2 2 7 1.67800 54.653 1.0 15 6 4 2 1.66600 55.080 1.0 16 2 0 8 1.53800 60.112 14.0 17 6 3 5 1.49700 61.936 43.0 18 4 0 8 1.41340 66.049 1.0 19 7 5 3 1.36840 68.516 1.0 20 4 3 8 1.33770 70.317 1.0 21 6 2 7 1.33280 70.614 1.0 22 7 3 6 1.29260 73.158 1.0 23 10 1 5 1.11280 87.612 25.0 24 8 8 0 1.10000 88.898 3.0 25 6 5 11 0.93430 111.069 2.0 26 10 8 4 0.92890 112.046 5.0 27 13 5 1 0.89090 119.681 1.0 28 9 8 8 0.86570 125.696 1.0 29 6 3 13 0.86390 126.164 3.0 |
新蟲 (初入文壇)
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