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senling銀蟲 (正式寫手)
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求XRD標(biāo)準(zhǔn)卡數(shù)據(jù)，萬(wàn)分感謝！ 已有1人參與
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| 如題，卡號(hào)為：JCPDS card no. 10-0445；JCPDS card no. 09-0393 |
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Name and formula Reference code: 00-010-0445 Compound name: Bismuth Oxide Iodide Empirical formula: BiIO Chemical formula: BiOI Crystallographic parameters Crystal system: Tetragonal Space group: P4/nmm Space group number: 129 a (?): 3.9940 b (?): 3.9940 c (?): 9.1490 Alpha (°): 90.0000 Beta (°): 90.0000 Gamma (°): 90.0000 Calculated density (g/cm^3): 8.01 Volume of cell (10^6 pm^3): 145.95 Z: 2.00 RIR: - Subfiles and quality Subfiles: Common Phase Inorganic NBS pattern Quality: Star (S) Comments Color: Dark red-orange Creation Date: 1970/1/1 Modification Date: 1970/1/1 Sample Preparation: Sample prepared at NBS, Gaithersburg, Maryland, USA, by reacting Bi2O3 with concentrated HI. Pattern was improved by heating the material in air for two hours at 450 C Analysis: Spectrographic analysis showed <0.1% Ni; <0.01% Al, Co, Fe, Si Temperature of Data Collection: Pattern taken at 25 C Color: Dark red-orange Additional Diffraction Lines: Plus 19 additional reflections to 0.9414. References Primary reference: Natl. Bur. Stand. (U.S.), Circ. 539, 9, 16, (1960) Peak list No. h k l d [A] 2Theta[deg] I [%] 1 0 0 1 9.15000 9.658 20.0 2 0 0 2 4.58000 19.365 8.0 3 1 0 1 3.66100 24.292 4.0 4 1 0 2 3.01100 29.645 100.0 5 1 1 0 2.82400 31.658 55.0 6 1 1 1 2.69900 33.166 4.0 7 1 0 3 2.42400 37.058 12.0 8 1 1 2 2.40300 37.393 8.0 9 0 0 4 2.28700 39.366 10.0 10 1 1 3 2.07200 43.649 4.0 11 2 0 0 1.99700 45.378 25.0 12 1 0 4 1.98500 45.668 12.0 13 2 0 1 1.95200 46.485 4.0 14 0 0 5 1.82900 49.816 4.0 15 1 1 4 1.77800 51.347 16.0 16 2 1 2 1.66400 55.151 30.0 17 2 1 3 1.54100 59.983 8.0 18 1 1 5 1.53590 60.203 4.0 19 0 0 6 1.52460 60.696 4.0 20 2 0 4 1.50450 61.594 8.0 21 1 0 6 1.42440 65.475 6.0 22 2 2 0 1.41200 66.123 8.0 23 2 1 4 1.40780 66.346 6.0 24 2 2 1 1.39570 66.996 1.0 25 2 2 2 1.34950 69.613 6.0 26 1 1 6 1.34220 70.046 6.0 27 0 0 7 1.30730 72.205 2.0 28 3 0 2 1.27860 74.092 4.0 29 3 1 0 1.26340 75.136 4.0 30 1 0 7 1.24240 76.634 4.0 31 3 0 3 1.22000 78.306 1.0 32 3 1 2 1.21760 78.490 4.0 33 2 0 6 1.21210 78.915 1.0 34 2 2 4 1.20170 79.734 4.0 35 1 1 7 1.18600 81.007 2.0 36 2 1 6 1.15970 83.246 2.0 37 3 0 4 1.15020 84.089 1.0 38 0 0 8 1.14360 84.687 1.0 39 2 2 5 1.11810 87.092 1.0 Name and formula Reference code: 00-009-0393 Compound name: Bismuth Oxide Bromide Empirical formula: BiBrO Chemical formula: BiOBr Crystallographic parameters Crystal system: Tetragonal Space group: P4/nmm Space group number: 129 a (?): 3.9260 b (?): 3.9260 c (?): 8.1030 Alpha (°): 90.0000 Beta (°): 90.0000 Gamma (°): 90.0000 Calculated density (g/cm^3): 8.11 Volume of cell (10^6 pm^3): 124.90 Z: 2.00 RIR: - Subfiles and quality Subfiles: Common Phase Inorganic NBS pattern Quality: Indexed (I) Comments Color: Colorless Creation Date: 1970/1/1 Modification Date: 1970/1/1 Color: Colorless Sample Preparation: Sample prepared at NBS, Gaithersburg, Maryland, USA by heating bismuth iodide with bromine water Analysis: Spectrographic analysis: 0.01-0.1% Si; 0.001-0.01% Al; and 0.0001-0.001% Ag, B, Ca, Fe, Mg, Pb. Temperature of Data Collection: Pattern taken at 25 C. References Primary reference: Natl. Bur. Stand. (U.S.), Circ. 539, 8, 14, (1959) Peak list No. h k l d [A] 2Theta[deg] I [%] 1 0 0 1 8.11000 10.901 40.0 2 0 0 2 4.05000 21.929 10.0 3 1 0 1 3.53700 25.158 30.0 4 1 0 2 2.82100 31.693 100.0 5 1 1 0 2.77600 32.220 65.0 6 0 0 3 2.70200 33.128 6.0 7 1 1 1 2.62900 34.075 6.0 8 1 1 2 2.28600 39.384 16.0 9 1 0 3 2.22900 40.435 4.0 10 0 0 4 2.02600 44.693 8.0 11 2 0 0 1.96300 46.209 25.0 12 1 1 3 1.93700 46.866 12.0 13 2 0 1 1.90700 47.649 6.0 14 1 0 4 1.80000 50.674 14.0 15 2 1 1 1.71500 53.379 10.0 16 1 1 4 1.63690 56.145 14.0 17 2 1 2 1.61130 57.118 35.0 18 2 0 3 1.58820 58.027 6.0 19 1 0 5 1.49770 61.904 6.0 20 2 0 4 1.41010 66.223 8.0 21 2 2 0 1.38820 67.406 10.0 22 0 0 6 1.35050 69.554 4.0 23 2 1 4 1.32640 71.006 12.0 24 1 0 6 1.27700 74.200 4.0 25 3 0 2 1.24560 76.401 12.0 26 3 1 0 1.24150 76.699 14.0 27 3 1 1 1.22720 77.760 8.0 28 1 1 6 1.21450 78.729 8.0 29 2 1 5 1.19070 80.621 6.0 30 0 0 7 1.15800 83.395 6.0 31 2 2 4 1.14500 84.560 8.0 32 3 1 3 1.12820 86.121 6.0 33 2 0 6 1.11230 87.661 6.0 |
2樓2015-02-01 12:41:15
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