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yiatcheng新蟲 (初入文壇)
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[求助]
求XRD衍射峰卡片 已有1人參與
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做的是鐵酸銅納米材料 需要CuFe2O4,Cu,Fe,Fe2O3,CuO的衍射卡片 |
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fatewu
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青若: 金幣+2, 謝謝回帖，歡迎常來(lái)無(wú)機(jī)物化版交流 2015-05-21 09:24:12
青若: 金幣+2, 謝謝回帖，歡迎常來(lái)無(wú)機(jī)物化版交流 2015-05-21 09:24:12
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PDF#04-0836: QM=Star(+); d=(Unknown); I=Diffractometer Copper, syn Cu (Red) Radiation=CuKa1 Lambda=1.5405 Filter=Ni Calibration= d-Cutoff= I/Ic(RIR)= Ref= Swanson, Tatge. Natl. Bur. Stand. (U.S.), Circ. 539, I 15 (1953) Cubic - Powder Diffraction, Fm-3m (225) Z=4 mp=1083 Cell=3.615 Pearson=cF4 (Cu) Density(c)=8.936 Density(m)=8.950 Mwt=63.55 Vol=47.24 F(8)=87.0(.0115,8) Ref= Ibid. Strong Line: 2.09/X 1.81/5 1.28/2 1.09/2 0.83/1 0.81/1 1.04/1 0.90/1 0.00/1 0.00/1 NOTE: It had been heated in an H2 atmosphere at 300 C. See ICSD 64699 (PDF 01-085-1326). Sample from metallurgical laboratory of NBS, Gaithersburg, Maryland, USA. Pattern taken at 26 C. Impurities from 0.001-0.01%, Ag, Al, Bi, Fe, Si, Zn. Opaque mineral optical data on specimen from unspecified locality, R3R%=60.65, Disp.=Std. VHN100=96-104, d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d 2.088 100.0 100.0 1 1 1 3 43.297 21.648 0.2395 3.0092 1.808 46.0 53.0 2 0 0 4 50.433 25.216 0.2765 3.4752 1.278 20.0 33.0 2 2 0 8 74.130 37.065 0.3912 4.9164 1.090 17.0 33.0 3 1 1 11 89.931 44.965 0.4587 5.7644 1.043 5.0 10.0 2 2 2 12 95.139 47.570 0.4791 6.0207 0.903 3.0 7.0 4 0 0 16 116.918 58.459 0.5532 6.9520 0.829 9.0 23.0 3 3 1 19 136.507 68.253 0.6029 7.5765 0.808 8.0 21.0 4 2 0 20 144.714 72.357 0.6186 7.7733 |
2樓2015-05-20 20:51:39
fatewu
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小木蟲浪漫體驗(yàn)師~\(^o^)/~
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青若: 金幣+1, 謝謝回帖，歡迎常來(lái)無(wú)機(jī)物化版交流 2015-05-21 09:24:23
青若: 金幣+1, 謝謝回帖，歡迎常來(lái)無(wú)機(jī)物化版交流 2015-05-21 09:24:23
|
PDF#06-0696: QM=Star(+); d=(Unknown); I=Diffractometer Iron, syn Fe (Gray, light gray metallic) Radiation=CuKa1 Lambda=1.5405 Filter=Ni Calibration= d-Cutoff= I/Ic(RIR)= Ref= Swanson et al. Natl. Bur. Stand. (U.S.), Circ. 539, IV 3 (1955) Cubic - Powder Diffraction, Im-3m (229) Z=2 mp= Cell=2.8664 Pearson=cI2 (W) Density(c)=7.874 Density(m)=7.86A Mwt=55.85 Vol=23.55 F(6)=222.1(.0045,6) Ref= Ibid. Strong Line: 2.03/X 1.17/3 1.43/2 0.91/1 1.01/1 0.83/1 0.00/1 0.00/1 0.00/1 0.00/1 NOTE: Total impurities of sample <0.0013% each metals and non-metals. See ICSD 64795 (PDF 01-085-1410). Pattern taken at 25 C. The iron used was an exceptionally pure rolled sheet prepared at the NBS, Gaithersburg, Maryland, USA., [Moore, G., J. Met., 5 1443 (1953)]. It was annealed in an H2 atmosphere for 3 days at 1100 C and slowly cooled in a He atmosphere. $GG-Fe (fcc)=(1390 C) $GD-Fe (bcc). Opaque mineral optical data on specimen from Meteorite: RR2Re= 57.7, Disp.=16, VHN=158 (mean at 100, 200, 300), Color values=.311, .316, 57.9, Ref.: IMA Commisssion on Ore Microscopy QDF. d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d 2.026 100.0 100.0 1 1 0 2 44.673 22.337 0.2467 3.1001 1.433 20.0 28.0 2 0 0 4 65.021 32.511 0.3489 4.3840 1.170 30.0 52.0 2 1 1 6 82.333 41.166 0.4273 5.3693 1.013 10.0 20.0 2 2 0 8 98.945 49.473 0.4934 6.2001 0.906 12.0 27.0 3 1 0 10 116.385 58.192 0.5516 6.9320 0.827 6.0 15.0 2 2 2 12 137.136 68.568 0.6042 7.5930 |
3樓2015-05-20 20:51:57
fatewu
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★
青若: 金幣+1, 謝謝回帖，歡迎常來(lái)無(wú)機(jī)物化版交流 2015-05-21 09:24:31
青若: 金幣+1, 謝謝回帖，歡迎常來(lái)無(wú)機(jī)物化版交流 2015-05-21 09:24:31
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PDF#45-0937: QM=Star(+); d=Diffractometer; I=Diffractometer Tenorite, syn Cu O (Black) Radiation=CuKa1 Lambda=1.540598 Filter=Graph Calibration=Internal(Si) d-Cutoff=15.0 I/Ic(RIR)=2.5 Ref= Martin, K., McCarthy, G., North Dakota State Univ., Fargo, ND, USA. ICDD Grant-in-Aid (1991) Monoclinic - Powder Diffraction, C2/c (15) Z=4 mp= Cell=4.6853x3.4257x5.1303<99.549> Pearson=mC8 (Cu O) Density(c)=6.506 Density(m)=6.450 Mwt=79.55 Vol=81.20 F(30)=89.7(.0070,48) Ref= J. Solid State Chem., 89 184 (1990) Strong Line: 2.53/X 2.32/9 2.31/3 1.87/2 1.51/2 1.41/1 1.38/1 1.58/1 2.75/1 1.42/1 NOTE: Sample obtained from Fisher Scientific. Sample annealed for 72 hours at 900 C. Average relative standard deviation in intensity of the ten strongest reflections for three specimen mounts = 4.8% Validated by calculated pattern. To replace 00-041-0254. Deleted by 002 and -111 reflections are not split; WFM 10/95. See ICSD 67850 (PDF 01-080-0076). d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d 2.753 8.0 7.0 -1 1 0 32.496 16.248 0.1816 2.2823 2.527 100.0 100.0 -1 1 1 35.495 17.747 0.1979 2.4864 2.527 100.0 100.0 0 0 2 35.495 17.747 0.1979 2.4864 2.323 91.0 99.0 1 1 1 38.730 19.365 0.2152 2.7048 2.310 28.0 31.0 2 0 0 38.957 19.479 0.2165 2.7200 1.961 2.0 3.0 -1 1 2 46.248 23.124 0.2549 3.2034 1.867 20.0 27.0 -2 0 2 48.725 24.363 0.2678 3.3649 1.776 1.0 1.0 1 1 2 51.379 25.690 0.2814 3.5360 1.712 6.0 9.0 0 2 0 53.451 26.726 0.2919 3.6684 1.580 9.0 14.0 2 0 2 58.335 29.168 0.3164 3.9754 1.505 15.0 25.0 -1 1 3 61.533 30.767 0.3320 4.1727 1.418 8.0 14.0 0 2 2 65.785 32.892 0.3525 4.4298 1.409 11.0 20.0 -3 1 1 66.248 33.124 0.3547 4.4574 1.378 9.0 16.0 1 1 3 67.943 33.972 0.3627 4.5580 1.375 11.0 20.0 -2 2 0 68.089 34.045 0.3634 4.5666 1.303 5.0 10.0 3 1 1 72.427 36.214 0.3835 4.8191 1.264 5.0 10.0 0 0 4 75.029 37.515 0.3953 4.9673 1.262 6.0 12.0 -2 2 2 75.225 37.612 0.3962 4.9784 1.196 2.0 4.0 -2 0 4 80.180 40.090 0.4180 5.2531 1.169 3.0 6.0 -3 1 3 82.375 41.188 0.4275 5.3716 1.161 2.0 4.0 2 2 2 83.103 41.551 0.4306 5.4105 1.155 2.0 4.0 4 0 0 83.649 41.825 0.4329 5.4395 1.123 1.0 2.0 -4 0 2 86.567 43.283 0.4450 5.5925 1.092 2.0 5.0 -1 3 1 89.721 44.861 0.4579 5.7538 1.074 1.0 2.0 1 3 1 91.649 45.824 0.4655 5.8503 1.039 1.0 2.0 2 0 4 95.672 47.836 0.4811 6.0462 1.017 1.0 2.0 0 2 4 98.406 49.203 0.4914 6.1751 1.006 2.0 5.0 3 1 3 99.814 49.907 0.4966 6.2401 0.981 2.0 5.0 -1 1 5 103.389 51.695 0.5094 6.4010 0.980 2.0 5.0 -2 2 4 103.523 51.761 0.5098 6.4068 0.957 1.0 3.0 -4 2 0 107.086 53.543 0.5221 6.5607 0.943 1.0 3.0 -1 3 3 109.419 54.710 0.5298 6.6580 0.939 2.0 5.0 -4 2 2 110.164 55.082 0.5323 6.6885 0.933 1.0 3.0 -4 0 4 111.208 55.604 0.5356 6.7308 0.920 2.0 5.0 1 1 5 113.571 56.785 0.5431 6.8244 0.918 2.0 6.0 -3 3 1 113.972 56.986 0.5443 6.8400 0.909 1.0 3.0 1 3 3 115.678 57.839 0.5495 6.9054 0.903 1.0 3.0 -5 1 1 116.939 58.470 0.5533 6.9527 |
4樓2015-05-20 20:52:24
fatewu
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★ ★ ★ ★ ★
青若: 金幣+5, 謝謝回帖，歡迎常來(lái)無(wú)機(jī)物化版交流 2015-05-21 09:24:50
青若: 金幣+5, 謝謝回帖，歡迎常來(lái)無(wú)機(jī)物化版交流 2015-05-21 09:24:50
|
PDF#34-0425: QM=Star(+); d=Diffractometer; I=Diffractometer Copper Iron Oxide Cu Fe2 O4 (Blackish yellow-green) Radiation=CuKa1 Lambda=1.5405981 Filter= Calibration=Internal(Ag) d-Cutoff=22.1 I/Ic(RIR)= Ref= Natl. Bur. Stand. (U.S.) Monogr. 25, 20 47 (1984) Tetragonal - Powder Diffraction, I41/amd (141) Z=4 mp= Cell=5.8444x8.6304 Pearson=tI28 (?) Density(c)=5.390 Density(m)=5.52A Mwt=239.24 Vol=294.79 F(25)=85.0(.0098,30) Ref= Ibid. Strong Line: 2.50/X 2.58/5 1.49/4 2.99/3 1.59/2 2.07/2 4.84/2 1.46/2 2.42/1 2.92/1 NOTE: The sample was prepared at NBS, Gaithersburg, Maryland, USA. Stoichiometric amounts of CuO + Fe2 O3 were heated in a platinum boat in pure oxygen with intermittent grinding. 850 C for 18 hours; 875 C for 21 hours; 925 C for 23 hours; 975 C for 20 hours; 975 C for 20 hours; 5 weight of Cu O was then added; 900 C for 20 hours; 975 C for 26 hours. The sample contained traces of Cu O and an unidentified phase. A cubic phase has also been reported by Vervey and Heilman (1947). To replace 00-006-0545. It is a tetragonally distorted inverse spinel. The structure was determined by Prince and Treuting (1956). The 'a' dimension given by Prince and Treuting was divided by the square root of 2 to make it conform to the body-centered space group. d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d 4.839 17.0 9.0 1 0 1 18.319 9.159 0.1033 1.2984 2.985 32.0 27.0 1 1 2 29.907 14.954 0.1675 2.1048 2.923 13.0 11.0 2 0 0 30.558 15.279 0.1711 2.1495 2.581 53.0 51.0 1 0 3 34.718 17.359 0.1937 2.4337 2.502 100.0 100.0 2 1 1 35.861 17.931 0.1998 2.5112 2.419 14.0 14.0 2 0 2 37.121 18.561 0.2066 2.5964 2.158 11.0 13.0 0 0 4 41.825 20.912 0.2317 2.9116 2.066 22.0 27.0 2 2 0 43.767 21.883 0.2419 3.0403 1.934 1.0 1.0 2 1 3 46.929 23.464 0.2585 3.2479 1.736 5.0 7.0 2 0 4 52.682 26.341 0.2880 3.6193 1.699 10.0 15.0 3 1 2 53.922 26.961 0.2943 3.6982 1.655 12.0 18.0 1 0 5 55.476 27.738 0.3021 3.7965 1.613 11.0 17.0 3 0 3 57.033 28.517 0.3099 3.8943 1.593 24.0 38.0 3 2 1 57.827 28.914 0.3138 3.9439 1.492 40.0 67.0 2 2 4 62.156 31.078 0.3351 4.2107 1.461 16.0 27.0 4 0 0 63.630 31.815 0.3422 4.3002 1.411 1.0 2.0 3 2 3 66.125 33.063 0.3541 4.4501 1.358 2.0 4.0 1 1 6 69.097 34.549 0.3681 4.6259 1.311 2.0 4.0 3 3 2 71.918 35.959 0.3812 4.7899 1.306 2.0 4.0 4 2 0 72.239 36.120 0.3826 4.8083 1.292 5.0 10.0 3 0 5 73.182 36.591 0.3869 4.8624 1.290 4.0 8.0 2 0 6 73.329 36.664 0.3876 4.8708 1.271 9.0 18.0 4 1 3 74.584 37.292 0.3933 4.9421 1.250 4.0 8.0 4 2 2 76.035 38.017 0.3998 5.0239 1.209 5.0 10.0 4 0 4 79.092 39.546 0.4133 5.1935 |
5樓2015-05-20 20:53:21
fatewu
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6樓2015-05-20 20:54:11
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[考研] 301求調(diào)劑 +10 | yy要上岸呀 2026-03-17 | 10/500 |
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[考研] 083200學(xué)碩321分一志愿暨南大學(xué)求調(diào)劑 +3 | innocenceF 2026-03-17 | 3/150 |
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[考研] 初始318分求調(diào)劑（有工作經(jīng)驗(yàn)） +3 | 1911236844 2026-03-17 | 3/150 |
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[考研] 297求調(diào)劑 +9 | 戲精丹丹丹 2026-03-17 | 9/450 |
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[考研] 295材料求調(diào)劑，一志愿武漢理工085601專碩 +5 | Charlieyq 2026-03-19 | 5/250 |
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[考研] 266求調(diào)劑 +5 | 陽(yáng)陽(yáng)哇塞 2026-03-14 | 10/500 |
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胡辣湯放糖 2026-03-15 | 6/300 |
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[考研] 318求調(diào)劑 +3 | Yanyali 2026-03-15 | 3/150 |
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