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junendure金蟲 (正式寫手)
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[求助]
求解Co-N配體單晶
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| 具體結構見附件,謝謝! |

銀蟲 (小有名氣)
用戶注銷 (知名作家)
精修問題可私信
用戶注銷 (知名作家)
精修問題可私信
捐助貴賓 (著名寫手)
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數(shù)據(jù)見附件 Bond precision: C-C = 0.0199 A Wavelength=0.71073 Cell: a=13.7104(11) b=15.7729(13) c=26.137(2) alpha=90 beta=90 gamma=90 Temperature: 273 K Calculated Reported Volume 5652.2(8) 5652.3(8) Space group P 21 21 21 P2(1)2(1)2( Hall group P 2ac 2ab ? Moiety formula C26 H22 Co N4 O4, C26 H24 Co N4 O4, Cl4 Co, C H2 Cl2 ? Sum formula C53 H48 Cl6 Co3 N8 O8 C53 H48 Cl6 Co3 N8 O8 Mr 1314.48 1314.48 Dx,g cm-3 1.545 1.545 Z 4 4 Mu (mm-1) 1.214 1.214 F000 2676.0 2676.0 F000' 2684.55 h,k,lmax 16,19,32 16,19,32 Nref 11155[ 6151] 11121 Tmin,Tmax 0.766,0.804 0.776,0.811 Tmin' 0.766 Correction method= # Reported T Limits: Tmin=0.776 Tmax=0.811 AbsCorr = MULTI-SCAN Data completeness= 1.81/1.00 Theta(max)= 26.030 R(reflections)= 0.0960( 7510) wR2(reflections)= 0.2613( 11121) S = 0.982 Npar= 725 The following ALERTS were generated. Each ALERT has the format test-name_ALERT_alert-type_alert-level. Click on the hyperlinks for more details of the test. Alert level B PLAT341_ALERT_3_B Low Bond Precision on C-C Bonds ............... 0.0199 Ang. Alert level C RFACR01_ALERT_3_C The value of the weighted R factor is > 0.25 Weighted R factor given 0.261 PLAT084_ALERT_3_C High wR2 Value (i.e. > 0.25) ................... 0.26 Report PLAT090_ALERT_3_C Poor Data / Parameter Ratio (Zmax > 18) ........ 8.48 Note PLAT166_ALERT_4_C S.U's Given on Coordinates for calc-flagged .... H11 |
金蟲 (正式寫手)

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