| 2 | 1/1 | 返回列表 |
| 查看: 368 | 回復: 1 | |||
[求助]
求助單晶A類錯誤修改 已有1人參與
|
| 做有機的實在不會 對專業(yè)人事來說應該是so easy的事 |
捐助貴賓 (著名寫手)
|
之前的結(jié)構(gòu)中有幾個原子定錯了。 Bond precision: C-C = 0.0055 A Wavelength=0.71073 Cell: a=12.828(4) b=16.694(5) c=13.040(4) alpha=90 beta=101.773(6) gamma=90 Temperature: 296 K Calculated Reported Volume 2733.8(15) 2733.9(13) Space group P 21/n P2(1)/n Hall group -P 2yn ? Moiety formula C32 H33 N5 O2 ? Sum formula C32 H33 N5 O2 C32 H33 N5 O2 Mr 519.63 519.63 Dx,g cm-3 1.263 1.262 Z 4 4 Mu (mm-1) 0.081 0.081 F000 1104.0 1104.0 F000' 1104.41 h,k,lmax 15,19,15 15,19,15 Nref 4811 4803 Tmin,Tmax 0.982,0.986 0.983,0.986 Tmin' 0.982 Correction method= # Reported T Limits: Tmin=0.983 Tmax=0.986 AbsCorr = MULTI-SCAN Data completeness= 0.998 Theta(max)= 25.000 R(reflections)= 0.0598( 2058) wR2(reflections)= 0.1586( 4803) S = 0.943 Npar= 357 The following ALERTS were generated. Each ALERT has the format test-name_ALERT_alert-type_alert-level. Click on the hyperlinks for more details of the test. Alert level C PLAT026_ALERT_3_C Ratio Observed / Unique Reflections too Low .... 43 % PLAT340_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0055 Ang. |
| 2 | 1/1 | 返回列表 |
| 最具人氣熱帖推薦 [查看全部] | 作者 | 回/看 | 最后發(fā)表 | |
|---|---|---|---|---|
|
[考研] 266分,求材料冶金能源化工等調(diào)劑 +5 | 哇呼哼呼哼 2026-03-27 | 7/350 |
|
|---|---|---|---|---|
|
[考研] 085701環(huán)境工程,267求調(diào)劑 +11 | minht 2026-03-26 | 11/550 |
|
|
[考研]
|
18419759900 2026-03-25 | 8/400 |
|
|
[考研] 材料292調(diào)劑 +12 | 橘頌思美人 2026-03-23 | 12/600 |
|
|
[考研] 314求調(diào)劑 +3 | 溪云珂 2026-03-26 | 3/150 |
|
|
[論文投稿] Journal of Mechanical Science and Technology +3 | Russ_ss 2026-03-25 | 5/250 |
|
|
[考研] 求調(diào)劑323材料與化工 +7 | 1124361 2026-03-24 | 7/350 |
|
|
[考研] 316求調(diào)劑 +5 | 江辭666 2026-03-26 | 5/250 |
|
|
[考研] 324求調(diào)劑 +8 | hanamiko 2026-03-26 | 10/500 |
|
|
[考研] 349求調(diào)劑 +5 | 杰斯塔里斯 2026-03-21 | 5/250 |
|
|
[考研] 調(diào)劑 +4 | 柚柚yoyo 2026-03-26 | 4/200 |
|
|
[考研] 340求調(diào)劑 +3 | Amber00 2026-03-26 | 3/150 |
|
|
[考研] 材料考研求調(diào)劑 +3 | Dendel 2026-03-23 | 6/300 |
|
|
[考研] 一志愿天津大學339材料與化工求調(diào)劑 +3 | 江往賣魚 2026-03-26 | 3/150 |
|
|
[考研] 打過很多競賽,085406控制工程300分,求調(diào)劑 +3 | askeladz 2026-03-26 | 3/150 |
|
|
[考研] 296求調(diào)劑 +4 | 汪?! 2026-03-25 | 7/350 |
|
|
[考研] 一志愿南航材料專317分求調(diào)劑 +5 | 炸呀炸呀炸薯條 2026-03-23 | 5/250 |
|
|
[考研] 接收2026碩士調(diào)劑(學碩+專碩) +4 | allen-yin 2026-03-23 | 6/300 |
|
|
[考研] 280分求調(diào)劑 一志愿085802 +4 | PUMPT 2026-03-22 | 7/350 |
|
|
[考研] 285求調(diào)劑 +6 | ytter 2026-03-22 | 6/300 |
|